CN112840049B - 用于制备高纯度水合硫酸镍的方法 - Google Patents
用于制备高纯度水合硫酸镍的方法 Download PDFInfo
- Publication number
- CN112840049B CN112840049B CN201980063456.3A CN201980063456A CN112840049B CN 112840049 B CN112840049 B CN 112840049B CN 201980063456 A CN201980063456 A CN 201980063456A CN 112840049 B CN112840049 B CN 112840049B
- Authority
- CN
- China
- Prior art keywords
- nickel
- organic phase
- cobalt
- rich
- depleted
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
- C22B3/24—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/01—Preparation or separation involving a liquid-liquid extraction, an adsorption or an ion-exchange
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/10—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B23/00—Obtaining nickel or cobalt
- C22B23/04—Obtaining nickel or cobalt by wet processes
- C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
- C22B23/0461—Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B23/00—Obtaining nickel or cobalt
- C22B23/04—Obtaining nickel or cobalt by wet processes
- C22B23/0476—Separation of nickel from cobalt
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/16—Extraction of metal compounds from ores or concentrates by wet processes by leaching in organic solutions
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/32—Carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/32—Carboxylic acids
- C22B3/326—Ramified chain carboxylic acids or derivatives thereof, e.g. "versatic" acids
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AU2018903643A AU2018903643A0 (en) | 2018-09-27 | Method for preparing a high-purity hydrated nickel sulphate | |
| AU2018903643 | 2018-09-27 | ||
| AU2019901760 | 2019-05-23 | ||
| AU2019901760A AU2019901760A0 (en) | 2019-05-23 | Method for preparing a high-purity hydrated nickel sulphate | |
| PCT/AU2019/051044 WO2020061639A1 (en) | 2018-09-27 | 2019-09-26 | Method for preparing a high-purity hydrated nickel sulphate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN112840049A CN112840049A (zh) | 2021-05-25 |
| CN112840049B true CN112840049B (zh) | 2024-09-13 |
Family
ID=69949184
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201980063456.3A Active CN112840049B (zh) | 2018-09-27 | 2019-09-26 | 用于制备高纯度水合硫酸镍的方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US11993520B2 (https=) |
| EP (1) | EP3856941A4 (https=) |
| JP (1) | JP7459060B2 (https=) |
| KR (1) | KR102820068B1 (https=) |
| CN (1) | CN112840049B (https=) |
| AU (1) | AU2019348192B2 (https=) |
| CA (1) | CA3110398C (https=) |
| WO (1) | WO2020061639A1 (https=) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP7360091B2 (ja) * | 2019-12-27 | 2023-10-12 | 住友金属鉱山株式会社 | 溶媒抽出方法およびコバルト水溶液の製造方法 |
| JP7348130B2 (ja) * | 2020-04-24 | 2023-09-20 | Jx金属株式会社 | 金属含有溶液中のマグネシウムイオン除去方法及び、金属回収方法 |
| US10995014B1 (en) | 2020-07-10 | 2021-05-04 | Northvolt Ab | Process for producing crystallized metal sulfates |
| CN114134341B (zh) * | 2020-09-04 | 2023-01-13 | 苏州博萃循环科技有限公司 | 一种含镍钴锰的料液中镍钴锰的回收方法 |
| CN116745236A (zh) | 2020-11-03 | 2023-09-12 | 哈茨有限公司 | 用于结晶金属硫酸盐的处理工艺 |
| PH12023551304A1 (en) | 2020-11-12 | 2023-11-20 | Hatch Ltd | Processes and methods for production of crystallized metal sulfates |
| CN112553478A (zh) * | 2020-12-02 | 2021-03-26 | 金川集团镍盐有限公司 | 一种氢氧化镍钴硫酸体系快速浸出的方法 |
| KR20230145474A (ko) | 2021-02-18 | 2023-10-17 | 해치 리미티드 | 리튬 및 배터리 화학물질 생성 시 황산나트륨 부산물 가공 |
| JP7832303B2 (ja) * | 2021-07-29 | 2026-03-17 | ユミコア | 金属を分離するための結晶化方法 |
| KR102601662B1 (ko) * | 2022-01-20 | 2023-11-10 | 포항공과대학교 산학협력단 | 2 서킷 공정에 의한 양극재용 고순도 니켈/코발트 혼합용액 제조방법 |
| CN115058597B (zh) * | 2022-06-30 | 2024-06-04 | 盛隆资源再生(无锡)有限公司 | 一种含钙、铁、钴、镍的电镀污泥的回收处理方法 |
| WO2024073810A1 (en) * | 2022-10-07 | 2024-04-11 | Igo Limited | Method for preparing high-purity mixed nickel and cobalt sulphate |
| WO2024213973A1 (en) * | 2023-04-11 | 2024-10-17 | Bactech Environmental Corporation | A process for treating a material containing iron and sulphur |
| US12286360B2 (en) * | 2023-07-26 | 2025-04-29 | Pt Qmb New Energy Materials | Cobalt-manganese sulfate solution from low nickel matte |
| WO2025020125A1 (zh) * | 2023-07-26 | 2025-01-30 | 青美邦新能源材料有限公司 | 一种低冰镍制备电池级硫酸镍钴锰晶体的方法 |
| JP2025530957A (ja) | 2023-08-25 | 2025-09-19 | コリア・ジンク・カンパニー・リミテッド | ニッケルを含有する原料からニッケル酸化物を回収するためのオールインワンニッケル製錬方法 |
| AU2024213150B2 (en) | 2023-08-25 | 2025-06-26 | Kemco | All-in-one nickel recovering method for nickel metal recovery from raw materials containing nickel |
| JP2025530955A (ja) | 2023-08-25 | 2025-09-19 | コリア・ジンク・カンパニー・リミテッド | ニッケルを含有する原料からニッケル水酸化物を回収するためのオールインワンニッケル製錬方法 |
| JP2025530958A (ja) | 2023-08-25 | 2025-09-19 | コリア・ジンク・カンパニー・リミテッド | ニッケルを含有する原料から硫酸ニッケル水溶液を製造する方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104379779A (zh) * | 2012-02-14 | 2015-02-25 | Bhp比利通Ssm开发有限公司 | 高等级镍产品的制备 |
| CN105200235A (zh) * | 2015-07-27 | 2015-12-30 | 江西睿锋环保有限公司 | 从电镀污泥中回收有价金属制备阴极铜和电池级硫酸镍的方法 |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3276863A (en) | 1964-01-21 | 1966-10-04 | Gen Mills Inc | Separation of nickel and cobalt values using alpha-hydroxy oximes |
| US3869257A (en) * | 1972-08-17 | 1975-03-04 | Int Nickel Co | Production of nickel sulfate |
| NL169958C (nl) * | 1977-03-09 | 1982-09-16 | Stamicarbon | Werkwijze voor het selectief extraheren van metaalionen uit waterige oplossingen daarvan. |
| US4108752A (en) | 1977-05-31 | 1978-08-22 | Diamond Shamrock Corporation | Electrolytic cell bank having spring loaded intercell connectors |
| US4541868A (en) * | 1983-07-22 | 1985-09-17 | California Nickel Corporation | Recovery of nickel and cobalt by controlled sulfuric acid leaching |
| US5399322A (en) * | 1992-10-15 | 1995-03-21 | Hazen Research, Inc. | Selective recovery of dissolved metals and preparation of metal salt products |
| US5855858A (en) | 1993-07-29 | 1999-01-05 | Cominco Engineering Services Ltd. | Process for the recovery of nickel and/or cobalt from an ore or concentrate |
| AUPN191395A0 (en) * | 1995-03-22 | 1995-04-27 | M.I.M. Holdings Limited | Atmospheric mineral leaching process |
| US6149885A (en) * | 1997-04-30 | 2000-11-21 | Sumitomo Metal Mining Co., Ltd. | Method for purifying a nickel sulfate solution by solvent extraction |
| US6231823B1 (en) * | 2000-03-27 | 2001-05-15 | Dynatec Corporation | Solvent extraction process for the separation of cobalt from nickel in aqueous sulphate-containing solutions |
| US6267800B1 (en) * | 2000-04-11 | 2001-07-31 | Sherritt International Corporation | Process for producing cobalt metal powder from nickel-cobalt sulphides |
| BRPI0507138A (pt) * | 2004-01-28 | 2007-06-19 | Commw Scient Ind Res Org | processo de extração por solvente para separação de cobalto e/ou nìquel de impureza em soluções de lixìvia |
| WO2006029439A1 (en) * | 2004-09-13 | 2006-03-23 | Canopean Pty. Ltd | Process for preparing nickel loaded organic extractant solution |
| EA013353B1 (ru) | 2005-10-03 | 2010-04-30 | Ототек Оюй | Способ переработки никельсодержащего сырьевого материала в выщелачивающем растворе на основе хлорида |
| DE102011089574B4 (de) * | 2011-12-22 | 2015-10-01 | Continental Automotive Gmbh | Elektrische Vorrichtung mit Filter zum Unterdrücken von Störsignalen |
| KR101191042B1 (ko) * | 2011-12-27 | 2012-10-15 | 강호길 | 니켈정광, 니켈매트로부터 고순도 황산니켈을 제조하는 방법 |
| CN103224259A (zh) * | 2013-05-15 | 2013-07-31 | 大冶有色金属有限责任公司 | 一种粗硫酸镍精制并回收有价金属的方法 |
| US11149328B2 (en) * | 2013-11-01 | 2021-10-19 | Colorado School Of Mines | Method of leaching arsenic from ore comprising copper |
| JP6489378B2 (ja) * | 2016-06-20 | 2019-03-27 | 住友金属鉱山株式会社 | 硫酸ニッケルと硫酸コバルトの低塩素濃度混合水溶液の製造方法 |
| CN108002408B (zh) * | 2016-10-31 | 2021-06-04 | 湖南金源新材料股份有限公司 | 电池废料制备硫酸镍、锰、锂、钴及四氧化三钴的方法 |
| TWI667056B (zh) * | 2018-04-30 | 2019-08-01 | Chaoyang University Of Technology | 錯合反應協同溶劑萃取回收金屬之方法 |
| CN108570555A (zh) * | 2018-05-03 | 2018-09-25 | 北京矿冶科技集团有限公司 | 一种从镍钴富集物中直接生产电池级硫酸镍的方法 |
-
2019
- 2019-09-26 EP EP19866230.6A patent/EP3856941A4/en active Pending
- 2019-09-26 AU AU2019348192A patent/AU2019348192B2/en active Active
- 2019-09-26 CN CN201980063456.3A patent/CN112840049B/zh active Active
- 2019-09-26 JP JP2021511629A patent/JP7459060B2/ja active Active
- 2019-09-26 CA CA3110398A patent/CA3110398C/en active Active
- 2019-09-26 US US17/280,962 patent/US11993520B2/en active Active
- 2019-09-26 KR KR1020217011969A patent/KR102820068B1/ko active Active
- 2019-09-26 WO PCT/AU2019/051044 patent/WO2020061639A1/en not_active Ceased
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104379779A (zh) * | 2012-02-14 | 2015-02-25 | Bhp比利通Ssm开发有限公司 | 高等级镍产品的制备 |
| CN105200235A (zh) * | 2015-07-27 | 2015-12-30 | 江西睿锋环保有限公司 | 从电镀污泥中回收有价金属制备阴极铜和电池级硫酸镍的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CA3110398C (en) | 2024-01-16 |
| KR102820068B1 (ko) | 2025-06-12 |
| EP3856941A1 (en) | 2021-08-04 |
| US11993520B2 (en) | 2024-05-28 |
| JP7459060B2 (ja) | 2024-04-01 |
| JP2022502564A (ja) | 2022-01-11 |
| CA3110398A1 (en) | 2020-04-02 |
| AU2019348192A1 (en) | 2021-03-18 |
| US20210354997A1 (en) | 2021-11-18 |
| WO2020061639A1 (en) | 2020-04-02 |
| EP3856941A4 (en) | 2022-06-15 |
| AU2019348192B2 (en) | 2024-07-11 |
| CN112840049A (zh) | 2021-05-25 |
| KR20210065144A (ko) | 2021-06-03 |
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