CN112840049B - 用于制备高纯度水合硫酸镍的方法 - Google Patents

用于制备高纯度水合硫酸镍的方法 Download PDF

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Publication number
CN112840049B
CN112840049B CN201980063456.3A CN201980063456A CN112840049B CN 112840049 B CN112840049 B CN 112840049B CN 201980063456 A CN201980063456 A CN 201980063456A CN 112840049 B CN112840049 B CN 112840049B
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nickel
organic phase
cobalt
rich
depleted
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Chinese (zh)
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CN112840049A (zh
Inventor
卡雷尔·约翰·奥斯滕
罗萨诺·安东尼奥·格拉西
阿图罗·古铁雷斯·克劳斯朵夫
里安·科林·哈里森
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Eggo Ltd
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Eggo Ltd
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C22B3/24Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/01Preparation or separation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00Compounds of nickel
    • C01G53/10Sulfates
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00Obtaining nickel or cobalt
    • C22B23/04Obtaining nickel or cobalt by wet processes
    • C22B23/0453Treatment or purification of solutions, e.g. obtained by leaching
    • C22B23/0461Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00Obtaining nickel or cobalt
    • C22B23/04Obtaining nickel or cobalt by wet processes
    • C22B23/0476Separation of nickel from cobalt
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/16Extraction of metal compounds from ores or concentrates by wet processes by leaching in organic solutions
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32Carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32Carboxylic acids
    • C22B3/326Ramified chain carboxylic acids or derivatives thereof, e.g. "versatic" acids
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
CN201980063456.3A 2018-09-27 2019-09-26 用于制备高纯度水合硫酸镍的方法 Active CN112840049B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
AU2018903643A AU2018903643A0 (en) 2018-09-27 Method for preparing a high-purity hydrated nickel sulphate
AU2018903643 2018-09-27
AU2019901760 2019-05-23
AU2019901760A AU2019901760A0 (en) 2019-05-23 Method for preparing a high-purity hydrated nickel sulphate
PCT/AU2019/051044 WO2020061639A1 (en) 2018-09-27 2019-09-26 Method for preparing a high-purity hydrated nickel sulphate

Publications (2)

Publication Number Publication Date
CN112840049A CN112840049A (zh) 2021-05-25
CN112840049B true CN112840049B (zh) 2024-09-13

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CN201980063456.3A Active CN112840049B (zh) 2018-09-27 2019-09-26 用于制备高纯度水合硫酸镍的方法

Country Status (8)

Country Link
US (1) US11993520B2 (https=)
EP (1) EP3856941A4 (https=)
JP (1) JP7459060B2 (https=)
KR (1) KR102820068B1 (https=)
CN (1) CN112840049B (https=)
AU (1) AU2019348192B2 (https=)
CA (1) CA3110398C (https=)
WO (1) WO2020061639A1 (https=)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7360091B2 (ja) * 2019-12-27 2023-10-12 住友金属鉱山株式会社 溶媒抽出方法およびコバルト水溶液の製造方法
JP7348130B2 (ja) * 2020-04-24 2023-09-20 Jx金属株式会社 金属含有溶液中のマグネシウムイオン除去方法及び、金属回収方法
US10995014B1 (en) 2020-07-10 2021-05-04 Northvolt Ab Process for producing crystallized metal sulfates
CN114134341B (zh) * 2020-09-04 2023-01-13 苏州博萃循环科技有限公司 一种含镍钴锰的料液中镍钴锰的回收方法
CN116745236A (zh) 2020-11-03 2023-09-12 哈茨有限公司 用于结晶金属硫酸盐的处理工艺
PH12023551304A1 (en) 2020-11-12 2023-11-20 Hatch Ltd Processes and methods for production of crystallized metal sulfates
CN112553478A (zh) * 2020-12-02 2021-03-26 金川集团镍盐有限公司 一种氢氧化镍钴硫酸体系快速浸出的方法
KR20230145474A (ko) 2021-02-18 2023-10-17 해치 리미티드 리튬 및 배터리 화학물질 생성 시 황산나트륨 부산물 가공
JP7832303B2 (ja) * 2021-07-29 2026-03-17 ユミコア 金属を分離するための結晶化方法
KR102601662B1 (ko) * 2022-01-20 2023-11-10 포항공과대학교 산학협력단 2 서킷 공정에 의한 양극재용 고순도 니켈/코발트 혼합용액 제조방법
CN115058597B (zh) * 2022-06-30 2024-06-04 盛隆资源再生(无锡)有限公司 一种含钙、铁、钴、镍的电镀污泥的回收处理方法
WO2024073810A1 (en) * 2022-10-07 2024-04-11 Igo Limited Method for preparing high-purity mixed nickel and cobalt sulphate
WO2024213973A1 (en) * 2023-04-11 2024-10-17 Bactech Environmental Corporation A process for treating a material containing iron and sulphur
US12286360B2 (en) * 2023-07-26 2025-04-29 Pt Qmb New Energy Materials Cobalt-manganese sulfate solution from low nickel matte
WO2025020125A1 (zh) * 2023-07-26 2025-01-30 青美邦新能源材料有限公司 一种低冰镍制备电池级硫酸镍钴锰晶体的方法
JP2025530957A (ja) 2023-08-25 2025-09-19 コリア・ジンク・カンパニー・リミテッド ニッケルを含有する原料からニッケル酸化物を回収するためのオールインワンニッケル製錬方法
AU2024213150B2 (en) 2023-08-25 2025-06-26 Kemco All-in-one nickel recovering method for nickel metal recovery from raw materials containing nickel
JP2025530955A (ja) 2023-08-25 2025-09-19 コリア・ジンク・カンパニー・リミテッド ニッケルを含有する原料からニッケル水酸化物を回収するためのオールインワンニッケル製錬方法
JP2025530958A (ja) 2023-08-25 2025-09-19 コリア・ジンク・カンパニー・リミテッド ニッケルを含有する原料から硫酸ニッケル水溶液を製造する方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104379779A (zh) * 2012-02-14 2015-02-25 Bhp比利通Ssm开发有限公司 高等级镍产品的制备
CN105200235A (zh) * 2015-07-27 2015-12-30 江西睿锋环保有限公司 从电镀污泥中回收有价金属制备阴极铜和电池级硫酸镍的方法

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3276863A (en) 1964-01-21 1966-10-04 Gen Mills Inc Separation of nickel and cobalt values using alpha-hydroxy oximes
US3869257A (en) * 1972-08-17 1975-03-04 Int Nickel Co Production of nickel sulfate
NL169958C (nl) * 1977-03-09 1982-09-16 Stamicarbon Werkwijze voor het selectief extraheren van metaalionen uit waterige oplossingen daarvan.
US4108752A (en) 1977-05-31 1978-08-22 Diamond Shamrock Corporation Electrolytic cell bank having spring loaded intercell connectors
US4541868A (en) * 1983-07-22 1985-09-17 California Nickel Corporation Recovery of nickel and cobalt by controlled sulfuric acid leaching
US5399322A (en) * 1992-10-15 1995-03-21 Hazen Research, Inc. Selective recovery of dissolved metals and preparation of metal salt products
US5855858A (en) 1993-07-29 1999-01-05 Cominco Engineering Services Ltd. Process for the recovery of nickel and/or cobalt from an ore or concentrate
AUPN191395A0 (en) * 1995-03-22 1995-04-27 M.I.M. Holdings Limited Atmospheric mineral leaching process
US6149885A (en) * 1997-04-30 2000-11-21 Sumitomo Metal Mining Co., Ltd. Method for purifying a nickel sulfate solution by solvent extraction
US6231823B1 (en) * 2000-03-27 2001-05-15 Dynatec Corporation Solvent extraction process for the separation of cobalt from nickel in aqueous sulphate-containing solutions
US6267800B1 (en) * 2000-04-11 2001-07-31 Sherritt International Corporation Process for producing cobalt metal powder from nickel-cobalt sulphides
BRPI0507138A (pt) * 2004-01-28 2007-06-19 Commw Scient Ind Res Org processo de extração por solvente para separação de cobalto e/ou nìquel de impureza em soluções de lixìvia
WO2006029439A1 (en) * 2004-09-13 2006-03-23 Canopean Pty. Ltd Process for preparing nickel loaded organic extractant solution
EA013353B1 (ru) 2005-10-03 2010-04-30 Ототек Оюй Способ переработки никельсодержащего сырьевого материала в выщелачивающем растворе на основе хлорида
DE102011089574B4 (de) * 2011-12-22 2015-10-01 Continental Automotive Gmbh Elektrische Vorrichtung mit Filter zum Unterdrücken von Störsignalen
KR101191042B1 (ko) * 2011-12-27 2012-10-15 강호길 니켈정광, 니켈매트로부터 고순도 황산니켈을 제조하는 방법
CN103224259A (zh) * 2013-05-15 2013-07-31 大冶有色金属有限责任公司 一种粗硫酸镍精制并回收有价金属的方法
US11149328B2 (en) * 2013-11-01 2021-10-19 Colorado School Of Mines Method of leaching arsenic from ore comprising copper
JP6489378B2 (ja) * 2016-06-20 2019-03-27 住友金属鉱山株式会社 硫酸ニッケルと硫酸コバルトの低塩素濃度混合水溶液の製造方法
CN108002408B (zh) * 2016-10-31 2021-06-04 湖南金源新材料股份有限公司 电池废料制备硫酸镍、锰、锂、钴及四氧化三钴的方法
TWI667056B (zh) * 2018-04-30 2019-08-01 Chaoyang University Of Technology 錯合反應協同溶劑萃取回收金屬之方法
CN108570555A (zh) * 2018-05-03 2018-09-25 北京矿冶科技集团有限公司 一种从镍钴富集物中直接生产电池级硫酸镍的方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104379779A (zh) * 2012-02-14 2015-02-25 Bhp比利通Ssm开发有限公司 高等级镍产品的制备
CN105200235A (zh) * 2015-07-27 2015-12-30 江西睿锋环保有限公司 从电镀污泥中回收有价金属制备阴极铜和电池级硫酸镍的方法

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Publication number Publication date
CA3110398C (en) 2024-01-16
KR102820068B1 (ko) 2025-06-12
EP3856941A1 (en) 2021-08-04
US11993520B2 (en) 2024-05-28
JP7459060B2 (ja) 2024-04-01
JP2022502564A (ja) 2022-01-11
CA3110398A1 (en) 2020-04-02
AU2019348192A1 (en) 2021-03-18
US20210354997A1 (en) 2021-11-18
WO2020061639A1 (en) 2020-04-02
EP3856941A4 (en) 2022-06-15
AU2019348192B2 (en) 2024-07-11
CN112840049A (zh) 2021-05-25
KR20210065144A (ko) 2021-06-03

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