KR102820068B1 - 고순도 수화 황산 니켈의 제조 방법 - Google Patents

고순도 수화 황산 니켈의 제조 방법 Download PDF

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KR102820068B1
KR102820068B1 KR1020217011969A KR20217011969A KR102820068B1 KR 102820068 B1 KR102820068 B1 KR 102820068B1 KR 1020217011969 A KR1020217011969 A KR 1020217011969A KR 20217011969 A KR20217011969 A KR 20217011969A KR 102820068 B1 KR102820068 B1 KR 102820068B1
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South Korea
Prior art keywords
nickel
organic phase
cobalt
rich
lean
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KR1020217011969A
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Korean (ko)
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KR20210065144A (ko
Inventor
카렐 존 오스텐
로사노 안토니오 그라시
아르투로 구티에레즈 클라우스도르프
리안 콜린 헤리슨
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이고 리미티드
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    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C22B3/24—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/01—Preparation or separation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/10—Sulfates
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B23/0461—Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0476—Separation of nickel from cobalt
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/16—Extraction of metal compounds from ores or concentrates by wet processes by leaching in organic solutions
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32—Carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32—Carboxylic acids
    • C22B3/326—Ramified chain carboxylic acids or derivatives thereof, e.g. "versatic" acids
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
KR1020217011969A 2018-09-27 2019-09-26 고순도 수화 황산 니켈의 제조 방법 Active KR102820068B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
AU2018903643A AU2018903643A0 (en) 2018-09-27 Method for preparing a high-purity hydrated nickel sulphate
AU2018903643 2018-09-27
AU2019901760 2019-05-23
AU2019901760A AU2019901760A0 (en) 2019-05-23 Method for preparing a high-purity hydrated nickel sulphate
PCT/AU2019/051044 WO2020061639A1 (en) 2018-09-27 2019-09-26 Method for preparing a high-purity hydrated nickel sulphate

Publications (2)

Publication Number Publication Date
KR20210065144A KR20210065144A (ko) 2021-06-03
KR102820068B1 true KR102820068B1 (ko) 2025-06-12

Family

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KR1020217011969A Active KR102820068B1 (ko) 2018-09-27 2019-09-26 고순도 수화 황산 니켈의 제조 방법

Country Status (8)

Country Link
US (1) US11993520B2 (https=)
EP (1) EP3856941A4 (https=)
JP (1) JP7459060B2 (https=)
KR (1) KR102820068B1 (https=)
CN (1) CN112840049B (https=)
AU (1) AU2019348192B2 (https=)
CA (1) CA3110398C (https=)
WO (1) WO2020061639A1 (https=)

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JP7360091B2 (ja) * 2019-12-27 2023-10-12 住友金属鉱山株式会社 溶媒抽出方法およびコバルト水溶液の製造方法
JP7348130B2 (ja) * 2020-04-24 2023-09-20 Ｊｘ金属株式会社 金属含有溶液中のマグネシウムイオン除去方法及び、金属回収方法
US10995014B1 (en) 2020-07-10 2021-05-04 Northvolt Ab Process for producing crystallized metal sulfates
CN114134341B (zh) * 2020-09-04 2023-01-13 苏州博萃循环科技有限公司 一种含镍钴锰的料液中镍钴锰的回收方法
CN116745236A (zh) 2020-11-03 2023-09-12 哈茨有限公司 用于结晶金属硫酸盐的处理工艺
PH12023551304A1 (en) 2020-11-12 2023-11-20 Hatch Ltd Processes and methods for production of crystallized metal sulfates
CN112553478A (zh) * 2020-12-02 2021-03-26 金川集团镍盐有限公司 一种氢氧化镍钴硫酸体系快速浸出的方法
KR20230145474A (ko) 2021-02-18 2023-10-17 해치 리미티드 리튬 및 배터리 화학물질 생성 시 황산나트륨 부산물 가공
JP7832303B2 (ja) * 2021-07-29 2026-03-17 ユミコア 金属を分離するための結晶化方法
KR102601662B1 (ko) * 2022-01-20 2023-11-10 포항공과대학교 산학협력단 2 서킷 공정에 의한 양극재용 고순도 니켈/코발트 혼합용액 제조방법
CN115058597B (zh) * 2022-06-30 2024-06-04 盛隆资源再生（无锡）有限公司 一种含钙、铁、钴、镍的电镀污泥的回收处理方法
WO2024073810A1 (en) * 2022-10-07 2024-04-11 Igo Limited Method for preparing high-purity mixed nickel and cobalt sulphate
WO2024213973A1 (en) * 2023-04-11 2024-10-17 Bactech Environmental Corporation A process for treating a material containing iron and sulphur
US12286360B2 (en) * 2023-07-26 2025-04-29 Pt Qmb New Energy Materials Cobalt-manganese sulfate solution from low nickel matte
WO2025020125A1 (zh) * 2023-07-26 2025-01-30 青美邦新能源材料有限公司 一种低冰镍制备电池级硫酸镍钴锰晶体的方法
JP2025530957A (ja) 2023-08-25 2025-09-19 コリア・ジンク・カンパニー・リミテッド ニッケルを含有する原料からニッケル酸化物を回収するためのオールインワンニッケル製錬方法
AU2024213150B2 (en) 2023-08-25 2025-06-26 Kemco All-in-one nickel recovering method for nickel metal recovery from raw materials containing nickel
JP2025530955A (ja) 2023-08-25 2025-09-19 コリア・ジンク・カンパニー・リミテッド ニッケルを含有する原料からニッケル水酸化物を回収するためのオールインワンニッケル製錬方法
JP2025530958A (ja) 2023-08-25 2025-09-19 コリア・ジンク・カンパニー・リミテッド ニッケルを含有する原料から硫酸ニッケル水溶液を製造する方法

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Also Published As

Publication number Publication date
CN112840049B (zh) 2024-09-13
CA3110398C (en) 2024-01-16
EP3856941A1 (en) 2021-08-04
US11993520B2 (en) 2024-05-28
JP7459060B2 (ja) 2024-04-01
JP2022502564A (ja) 2022-01-11
CA3110398A1 (en) 2020-04-02
AU2019348192A1 (en) 2021-03-18
US20210354997A1 (en) 2021-11-18
WO2020061639A1 (en) 2020-04-02
EP3856941A4 (en) 2022-06-15
AU2019348192B2 (en) 2024-07-11
CN112840049A (zh) 2021-05-25
KR20210065144A (ko) 2021-06-03

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