CA3013250C - Molybdenum disulfide powders and methods and apparatus for producing the same - Google Patents
Molybdenum disulfide powders and methods and apparatus for producing the same Download PDFInfo
- Publication number
- CA3013250C CA3013250C CA3013250A CA3013250A CA3013250C CA 3013250 C CA3013250 C CA 3013250C CA 3013250 A CA3013250 A CA 3013250A CA 3013250 A CA3013250 A CA 3013250A CA 3013250 C CA3013250 C CA 3013250C
- Authority
- CA
- Canada
- Prior art keywords
- oil
- molybdenum disulfide
- product
- housing
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000843 powder Substances 0.000 title claims abstract description 197
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 title claims abstract description 136
- 229910052982 molybdenum disulfide Inorganic materials 0.000 title claims abstract description 128
- 238000000034 method Methods 0.000 title claims description 117
- 239000000463 material Substances 0.000 claims abstract description 144
- 238000003801 milling Methods 0.000 claims abstract description 118
- 239000002245 particle Substances 0.000 claims abstract description 116
- 239000002243 precursor Substances 0.000 claims abstract description 96
- 239000002253 acid Substances 0.000 claims abstract description 71
- 238000000576 coating method Methods 0.000 claims abstract description 9
- 239000011248 coating agent Substances 0.000 claims abstract description 8
- 238000010902 jet-milling Methods 0.000 claims abstract description 8
- 238000005549 size reduction Methods 0.000 claims abstract description 6
- 230000000694 effects Effects 0.000 claims abstract description 3
- 239000003921 oil Substances 0.000 claims description 262
- 230000008569 process Effects 0.000 claims description 89
- 238000002347 injection Methods 0.000 claims description 56
- 239000007924 injection Substances 0.000 claims description 56
- 239000012530 fluid Substances 0.000 claims description 14
- 230000002093 peripheral effect Effects 0.000 claims description 12
- 238000011144 upstream manufacturing Methods 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- 230000003254 anti-foaming effect Effects 0.000 claims description 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 229930195729 fatty acid Natural products 0.000 claims description 2
- -1 fatty-acid ester Chemical class 0.000 claims description 2
- 229920001296 polysiloxane Polymers 0.000 claims description 2
- 239000010690 paraffinic oil Substances 0.000 claims 4
- 150000001875 compounds Chemical class 0.000 claims 2
- 229920003229 poly(methyl methacrylate) Polymers 0.000 claims 1
- 239000004926 polymethyl methacrylate Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 10
- 239000000047 product Substances 0.000 description 153
- 239000007789 gas Substances 0.000 description 102
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 95
- 238000000227 grinding Methods 0.000 description 10
- 229910052961 molybdenite Inorganic materials 0.000 description 8
- 238000010951 particle size reduction Methods 0.000 description 8
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 7
- 229910052750 molybdenum Inorganic materials 0.000 description 7
- 239000011733 molybdenum Substances 0.000 description 7
- 238000009826 distribution Methods 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 5
- 238000003556 assay Methods 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 3
- 230000000712 assembly Effects 0.000 description 3
- 238000000429 assembly Methods 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 230000003213 activating effect Effects 0.000 description 2
- 238000010923 batch production Methods 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000012159 carrier gas Substances 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 238000009291 froth flotation Methods 0.000 description 2
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 230000037361 pathway Effects 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 description 1
- PNKJRKPMPSMDKD-UHFFFAOYSA-N [Mo](=S)=S.[Cu]=S Chemical compound [Mo](=S)=S.[Cu]=S PNKJRKPMPSMDKD-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000003466 anti-cipated effect Effects 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- OMZSGWSJDCOLKM-UHFFFAOYSA-N copper(II) sulfide Chemical compound [S-2].[Cu+2] OMZSGWSJDCOLKM-UHFFFAOYSA-N 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000000994 depressogenic effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000005188 flotation Methods 0.000 description 1
- 239000010438 granite Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 238000005456 ore beneficiation Methods 0.000 description 1
- 238000011946 reduction process Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010301 surface-oxidation reaction Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910001868 water Inorganic materials 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/06—Jet mills
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/06—Jet mills
- B02C19/068—Jet mills of the fluidised-bed type
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/02—Feeding devices
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G39/00—Compounds of molybdenum
- C01G39/06—Sulfides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/19—Oil-absorption capacity, e.g. DBP values
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
Landscapes
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Disintegrating Or Milling (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Glanulating (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161439571P | 2011-02-04 | 2011-02-04 | |
| US61/439,571 | 2011-02-04 | ||
| CA2824399A CA2824399C (en) | 2011-02-04 | 2012-02-03 | Molybdenum disulfide powders and methods and apparatus for producing the same |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2824399A Division CA2824399C (en) | 2011-02-04 | 2012-02-03 | Molybdenum disulfide powders and methods and apparatus for producing the same |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA3013250A1 CA3013250A1 (en) | 2012-08-09 |
| CA3013250C true CA3013250C (en) | 2020-10-27 |
Family
ID=46600819
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA3013250A Active CA3013250C (en) | 2011-02-04 | 2012-02-03 | Molybdenum disulfide powders and methods and apparatus for producing the same |
| CA2824399A Active CA2824399C (en) | 2011-02-04 | 2012-02-03 | Molybdenum disulfide powders and methods and apparatus for producing the same |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2824399A Active CA2824399C (en) | 2011-02-04 | 2012-02-03 | Molybdenum disulfide powders and methods and apparatus for producing the same |
Country Status (5)
| Country | Link |
|---|---|
| US (3) | US8808661B2 (enExample) |
| EP (3) | EP2805917B1 (enExample) |
| JP (4) | JP6273146B2 (enExample) |
| CA (2) | CA3013250C (enExample) |
| WO (1) | WO2012106592A2 (enExample) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA3058215C (en) * | 2018-10-12 | 2023-09-26 | Disa, Llc | High slurry density hydraulic disassociation system |
| CN109806531B (zh) * | 2019-01-30 | 2020-04-24 | 河南理工大学 | 一种低碳气体水合物粉碎抑爆装置 |
| CN112024087A (zh) * | 2020-08-06 | 2020-12-04 | 包头永真静平磁性材料科技有限公司 | 一种用于钕铁硼生产的气流磨装置 |
| CN117043112B (zh) * | 2021-03-24 | 2025-08-01 | Dic株式会社 | 二硫化钼颗粒和润滑组合物 |
| CN117065900A (zh) * | 2023-09-14 | 2023-11-17 | 广东长信精密设备有限公司 | 金属粉体生产系统 |
| CN118513546B (zh) * | 2024-06-27 | 2025-05-27 | 天津大学 | 一种金属粉末制备装置及金属粉末制备方法 |
| CN119869707B (zh) * | 2025-03-13 | 2025-10-17 | 湖南泰通能源管理股份有限公司 | 基于气体压缩技术的正极材料磨料系统及加工方法 |
Family Cites Families (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3125413A (en) * | 1964-03-17 | Method of prepamng molybdenum | ||
| US2367946A (en) * | 1942-12-15 | 1945-01-23 | Westinghouse Electric & Mfg Co | Process of producing metallic disulphides, tellurides, and selenides |
| US2686156A (en) * | 1951-12-08 | 1954-08-10 | Westinghouse Electric Corp | Preparation of stable molybdenum disulfide lubricants |
| US2892741A (en) | 1954-09-01 | 1959-06-30 | Alpha Molykote Corp | Method of preparing lubricative crystalline molybdenum disulfide |
| US2983453A (en) * | 1958-03-13 | 1961-05-09 | Socony Mobil Oil Co Inc | Method of pulverization |
| GB926516A (en) * | 1958-10-29 | 1963-05-22 | American Metal Climax Inc | Method of producing molybdenum disulphide powder suitable for use as a lubricant |
| US3156420A (en) | 1959-08-17 | 1964-11-10 | Acheson Ind Inc | Method for making molybdenum disulfide |
| US3062741A (en) | 1959-08-17 | 1962-11-06 | Acheson Ind Inc | Molybdenum disulfide lubricant and method for making same |
| US3082065A (en) * | 1960-07-11 | 1963-03-19 | American Metal Climax Inc | Method of preparing pulverized molybdenum disulfide |
| US3073779A (en) * | 1960-07-20 | 1963-01-15 | American Metal Climax Inc | Method of preparing molybdenum disulfide powder |
| GB1126482A (en) * | 1964-09-25 | 1968-09-05 | British Petroleum Co | Separation of straight chain hydrocarbons from mixtures |
| GB1282875A (en) * | 1968-09-27 | 1972-07-26 | British Petroleum Co | Oleophilic metal sulphides |
| US3842009A (en) * | 1970-10-19 | 1974-10-15 | American Metal Climax Inc | Molybdenum disulfide containing lubricant |
| US3661508A (en) | 1970-12-14 | 1972-05-09 | Sylvania Electric Prod | Process for producing molybdenum disulfide |
| US4243554A (en) | 1979-06-11 | 1981-01-06 | Union Carbide Corporation | Molybdenum disulfide catalyst and the preparation thereof |
| US4284244A (en) | 1979-09-19 | 1981-08-18 | Amax, Inc. | Process for producing high grade molybdenum disulfide powder |
| JPS5918107A (ja) * | 1982-07-19 | 1984-01-30 | Central Glass Co Ltd | 改質されたフッ化黒鉛からなる固体潤滑剤 |
| JPS6064647A (ja) | 1983-09-19 | 1985-04-13 | フロイント産業株式会社 | コ−チング方法および装置 |
| US4606817A (en) * | 1985-01-31 | 1986-08-19 | Amax Inc. | Recovery of molybdenite |
| GB8628586D0 (en) * | 1986-11-29 | 1987-01-07 | Tioxide Group Plc | Mill |
| GB8720904D0 (en) * | 1987-09-05 | 1987-10-14 | Tioxide Group Plc | Mill |
| JPH01176006A (ja) * | 1987-12-29 | 1989-07-12 | Sekometsukusu Kk | 防爆射出成形用金属の製造方法および防爆射出成形用金属 |
| JPH0664909A (ja) | 1991-06-14 | 1994-03-08 | Nippon Steel Chem Co Ltd | 炭素質原料混練粉砕方法 |
| GB9226994D0 (en) * | 1992-12-24 | 1993-02-17 | Tioxide Group Services Ltd | Method of milling |
| US5512406A (en) * | 1993-10-14 | 1996-04-30 | Canon Kabushiki Kaisha | Toners of different size for electrophotography |
| JPH10118479A (ja) | 1996-10-15 | 1998-05-12 | Yasuo Kobayashi | 表面改質粉体およびその製造方法並びに粉体表面改質 装置 |
| US7237732B2 (en) * | 2000-06-01 | 2007-07-03 | Daikin Industries, Ltd. | Process for preparing ground resin particles and apparatus for preparing the same |
| JP3931564B2 (ja) * | 2001-01-25 | 2007-06-20 | 住友金属工業株式会社 | 耐焼付き性及び防錆性に優れた鋼管用ねじ継手 |
| EP2080558A1 (en) | 2002-12-13 | 2009-07-22 | Syngeta Participations AG | Device for coating a finely milled solid |
| US6962006B2 (en) | 2002-12-19 | 2005-11-08 | Acusphere, Inc. | Methods and apparatus for making particles using spray dryer and in-line jet mill |
| JP4380983B2 (ja) * | 2002-12-26 | 2009-12-09 | 日立金属株式会社 | Ｒ−Ｆｅ−Ｂ系焼結磁石の製造方法 |
| US7866581B2 (en) * | 2004-02-10 | 2011-01-11 | Kao Corporation | Method of manufacturing toner |
| US7560218B2 (en) * | 2004-10-01 | 2009-07-14 | Kao Corporation | Process for preparing toner |
| US7276102B2 (en) | 2004-10-21 | 2007-10-02 | Climax Engineered Materials, Llc | Molybdenum metal powder and production thereof |
| DE102005039118A1 (de) * | 2005-08-18 | 2007-02-22 | Wacker Chemie Ag | Verfahren und Vorrichtung zum Zerkleinern von Silicium |
| MX2008009032A (es) * | 2006-01-12 | 2008-09-26 | Univ Arkansas | Composiciones de nanoparticulas y metodos para fabricarlas y utilizarlas. |
| US7789331B2 (en) * | 2006-09-06 | 2010-09-07 | Integrated Photovoltaics, Inc. | Jet mill producing fine silicon powder |
| CA2706726C (en) | 2007-11-29 | 2013-11-12 | Dow Global Technologies Inc. | Compounds and methods of forming compounds useful as a toner |
| DE102008051784B4 (de) | 2008-10-17 | 2012-02-02 | H.C. Starck Gmbh | Verfahren zur Herstellung von Molybdän-Metallpulver, Molybdän-Metallpulver und dessen Verwendung |
| US8507090B2 (en) * | 2011-04-27 | 2013-08-13 | Climax Engineered Materials, Llc | Spherical molybdenum disulfide powders, molybdenum disulfide coatings, and methods for producing same |
-
2012
- 2012-02-03 EP EP14178636.8A patent/EP2805917B1/en not_active Not-in-force
- 2012-02-03 CA CA3013250A patent/CA3013250C/en active Active
- 2012-02-03 WO PCT/US2012/023757 patent/WO2012106592A2/en not_active Ceased
- 2012-02-03 EP EP12741656.8A patent/EP2670532B1/en active Active
- 2012-02-03 JP JP2013552672A patent/JP6273146B2/ja not_active Expired - Fee Related
- 2012-02-03 EP EP14178637.6A patent/EP2805918B1/en not_active Not-in-force
- 2012-02-03 US US13/365,697 patent/US8808661B2/en active Active
- 2012-02-03 CA CA2824399A patent/CA2824399C/en active Active
-
2014
- 2014-06-25 US US14/314,828 patent/US9878332B2/en active Active
- 2014-06-25 US US14/314,838 patent/US10549286B2/en not_active Expired - Fee Related
- 2014-10-01 JP JP2014202952A patent/JP6247187B2/ja not_active Expired - Fee Related
- 2014-10-01 JP JP2014202953A patent/JP6118299B2/ja not_active Expired - Fee Related
-
2017
- 2017-10-12 JP JP2017198167A patent/JP6581164B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JP6581164B2 (ja) | 2019-09-25 |
| CA2824399C (en) | 2018-09-18 |
| US8808661B2 (en) | 2014-08-19 |
| JP6273146B2 (ja) | 2018-01-31 |
| JP6247187B2 (ja) | 2017-12-13 |
| EP2805917B1 (en) | 2018-04-11 |
| EP2805917A3 (en) | 2015-01-21 |
| CA3013250A1 (en) | 2012-08-09 |
| US20120202063A1 (en) | 2012-08-09 |
| JP6118299B2 (ja) | 2017-04-19 |
| WO2012106592A3 (en) | 2012-10-18 |
| US20140306043A1 (en) | 2014-10-16 |
| JP2018048077A (ja) | 2018-03-29 |
| US10549286B2 (en) | 2020-02-04 |
| US20140308443A1 (en) | 2014-10-16 |
| JP2015044736A (ja) | 2015-03-12 |
| EP2670532A4 (en) | 2015-01-21 |
| EP2805918A2 (en) | 2014-11-26 |
| US9878332B2 (en) | 2018-01-30 |
| EP2805917A2 (en) | 2014-11-26 |
| WO2012106592A2 (en) | 2012-08-09 |
| CA2824399A1 (en) | 2012-08-09 |
| EP2670532A2 (en) | 2013-12-11 |
| EP2805918B1 (en) | 2016-02-03 |
| JP2014511323A (ja) | 2014-05-15 |
| EP2670532B1 (en) | 2019-09-11 |
| JP2015038033A (ja) | 2015-02-26 |
| EP2805918A3 (en) | 2015-01-28 |
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