CA2834856C - Lignin production from lignocellulosic biomass - Google Patents

Lignin production from lignocellulosic biomass Download PDF

Info

Publication number
CA2834856C
CA2834856C CA2834856A CA2834856A CA2834856C CA 2834856 C CA2834856 C CA 2834856C CA 2834856 A CA2834856 A CA 2834856A CA 2834856 A CA2834856 A CA 2834856A CA 2834856 C CA2834856 C CA 2834856C
Authority
CA
Canada
Prior art keywords
lignin
pressure
temperature
degree
bar
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA2834856A
Other languages
English (en)
French (fr)
Other versions
CA2834856A1 (en
Inventor
Krishnan V. Iyer
Michel A. Simard
Kiran Kadam
Original Assignee
Renmatix Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Renmatix Inc filed Critical Renmatix Inc
Publication of CA2834856A1 publication Critical patent/CA2834856A1/en
Application granted granted Critical
Publication of CA2834856C publication Critical patent/CA2834856C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/16—Sulfur-containing compounds
    • C04B24/18—Lignin sulfonic acid or derivatives thereof, e.g. sulfite lye
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
    • C07G1/00—Low-molecular-weight derivatives of lignin
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H6/00—Macromolecular compounds derived from lignin, e.g. tannins, humic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H8/00—Macromolecular compounds derived from lignocellulosic materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L97/00—Compositions of lignin-containing materials
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1014—Biomass of vegetal origin
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Ceramic Engineering (AREA)
  • Structural Engineering (AREA)
  • Processing Of Solid Wastes (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Paper (AREA)
  • Dry Formation Of Fiberboard And The Like (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
CA2834856A 2011-05-04 2012-05-04 Lignin production from lignocellulosic biomass Expired - Fee Related CA2834856C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161482425P 2011-05-04 2011-05-04
US61/482,425 2011-05-04
PCT/US2012/036566 WO2012151509A2 (en) 2011-05-04 2012-05-04 Lignin production from lignocellulosic biomass

Publications (2)

Publication Number Publication Date
CA2834856A1 CA2834856A1 (en) 2012-11-08
CA2834856C true CA2834856C (en) 2020-04-07

Family

ID=47090420

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2834856A Expired - Fee Related CA2834856C (en) 2011-05-04 2012-05-04 Lignin production from lignocellulosic biomass

Country Status (13)

Country Link
US (2) US8317928B1 (cg-RX-API-DMAC10.html)
EP (1) EP2705074B1 (cg-RX-API-DMAC10.html)
JP (1) JP5905570B2 (cg-RX-API-DMAC10.html)
KR (1) KR101425765B1 (cg-RX-API-DMAC10.html)
CN (1) CN103502320B (cg-RX-API-DMAC10.html)
AU (1) AU2012250560B2 (cg-RX-API-DMAC10.html)
BR (1) BR112013028146A2 (cg-RX-API-DMAC10.html)
CA (1) CA2834856C (cg-RX-API-DMAC10.html)
PH (1) PH12013502197A1 (cg-RX-API-DMAC10.html)
RU (1) RU2508301C1 (cg-RX-API-DMAC10.html)
SG (1) SG194704A1 (cg-RX-API-DMAC10.html)
WO (1) WO2012151509A2 (cg-RX-API-DMAC10.html)
ZA (1) ZA201309031B (cg-RX-API-DMAC10.html)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2597588C2 (ru) 2010-01-19 2016-09-10 Ренмэтикс, Инк. Производство сбраживаемых сахаров и лигнина из биомассы, использующее сверхкритические текучие среды
BR112013010659A8 (pt) 2010-11-01 2017-12-26 Reac Fuel Ab Processo para uma conversão controlada de uma matéria-prima da biomassa
KR20140039215A (ko) 2011-05-04 2014-04-01 렌매틱스, 인코포레이티드. 목질계 바이오매스로부터의 리그닌 제조
US8801859B2 (en) 2011-05-04 2014-08-12 Renmatix, Inc. Self-cleaning apparatus and method for thick slurry pressure control
KR20140092380A (ko) * 2011-11-08 2014-07-23 리엑 퓰 에이비 낮은 pH에서 바이오매스의 액화
US8759498B2 (en) 2011-12-30 2014-06-24 Renmatix, Inc. Compositions comprising lignin
FI20125362L (fi) * 2012-03-29 2013-09-30 Upm Kymmene Corp Ligniini sekä menetelmä ja järjestelmä ligniinin käsittelemiseksi
BR112014025714A8 (pt) * 2012-04-30 2018-02-06 Renmatix Inc Processo que envolve a liquefação de uma calda de biomassa por meio de tratamento em água comprimida quente (hcw)
US9222040B2 (en) * 2012-06-07 2015-12-29 General Electric Company System and method for slurry handling
US10018416B2 (en) 2012-12-04 2018-07-10 General Electric Company System and method for removal of liquid from a solids flow
CN105026525B (zh) * 2013-01-25 2017-10-10 雷恩生物燃料公司 用于精炼的生物质材料的组合物
US9255187B2 (en) * 2013-03-15 2016-02-09 Synergy Horizon Limited Method for production of dry hydrolytic lignin
NZ731063A (en) 2013-03-15 2018-09-28 Renmatix Inc High purity lignin, lignin compositions, and higher structured lignin
KR101479676B1 (ko) * 2013-05-23 2015-01-08 씨제이제일제당 주식회사 저분자 리그닌 유도체의 제조방법
US9702372B2 (en) 2013-12-11 2017-07-11 General Electric Company System and method for continuous solids slurry depressurization
US9784121B2 (en) 2013-12-11 2017-10-10 General Electric Company System and method for continuous solids slurry depressurization
CA2962604C (en) 2014-09-26 2018-10-02 Renmatix, Inc. Methods for preparing and collecting polyaromatic compounds, and products comprising polyaromatic compounds
SG11201701740VA (en) 2014-09-26 2017-04-27 Renmatix Inc Cellulose-containing compositions and methods of making same
AU2014411407B2 (en) * 2014-11-12 2020-06-18 Renmatix, Inc. Method of coalescing a substance
FI127960B (fi) 2015-05-29 2019-06-14 Upm Kymmene Corp Menetelmä raakaligniinin pesemiseksi, liukoinen hiilihydraattia sisältävä fraktio, kiintoainefraktio ja niiden käyttö
FI127740B (en) 2015-05-29 2019-01-15 Upm Kymmene Corp A method and an apparatus for forming a lignin fraction, a lignin composition and its use
GB2546243B (en) * 2015-12-23 2018-07-11 Aerothermal Green Energy Ltd Biomass, thermal pressure hydrolysis and anaerobic digestion
US11821047B2 (en) 2017-02-16 2023-11-21 Apalta Patent OÜ High pressure zone formation for pretreatment
US11873384B2 (en) 2017-09-07 2024-01-16 Renmatix, Inc. Antioxidant stabilizer in polymers
BR112022012348A2 (pt) 2019-12-22 2022-09-13 Sweetwater Energy Inc Métodos de fazer lignina especializada e produtos de lignina da biomassa

Family Cites Families (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2156159A (en) 1938-05-17 1939-04-25 Northwood Chemical Company Process of making lignin
US2994633A (en) 1958-08-21 1961-08-01 Crossett Company Process for separating lignin solids from used neutral sulfite pulping liquors
US2997466A (en) 1958-11-04 1961-08-22 West Virginia Pulp & Paper Co Decantation of lignin
DE2737118A1 (de) 1977-08-17 1979-03-01 Projektierung Chem Verfahrenst Verfahren zur gewinnung von zuckern, gegebenenfalls cellulose und gegebenenfalls lignin aus lignocellulosischen pflanzlichen rohstoffen
CA1100266A (en) 1977-08-31 1981-05-05 Laszlo Paszner Organosolv delignification and saccharification process for lignocellulosic plant materials
US4470851A (en) 1981-03-26 1984-09-11 Laszlo Paszner High efficiency organosolv saccharification process
SU1086046A1 (ru) * 1982-07-12 1984-04-15 Ленинградская Ордена Ленина Лесотехническая Академия Им.С.М.Кирова Способ делигнификации древесины
DE3428661A1 (de) 1983-08-09 1985-03-07 Krupp Industrietechnik GmbH Werk Buckau Wolf, 4048 Grevenbroich Verfahren zur hydrolyse von lignocellulosehaltiger biomasse
CA1198703A (en) 1984-08-02 1985-12-31 Edward A. De Long Method of producing level off d p microcrystalline cellulose and glucose from lignocellulosic material
US4764596A (en) 1985-11-05 1988-08-16 Repap Technologies Inc. Recovery of lignin
CA1284637C (en) 1987-08-24 1991-06-04 George S. Faass Biomass fractionation process
US5041192A (en) * 1988-09-16 1991-08-20 University Of South Florida Supercritical delignification of wood
US6180845B1 (en) * 1999-10-07 2001-01-30 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Transforming biomass to hydrocarbon mixtures in near-critical or supercritical water
DK176540B1 (da) * 2004-09-24 2008-07-21 Cambi Bioethanol Aps Fremgangsmåde til behandling af biomasse og organisk affald med henblik på at udvinde önskede biologisk baserede produkter
JP2006255676A (ja) * 2005-03-18 2006-09-28 Kri Inc リグニン物質分離方法
JP2006288676A (ja) * 2005-04-11 2006-10-26 Takahiko Katayama 飲料入り容器の陳列方法
CA2615844C (en) * 2005-07-19 2015-04-21 Holm Christensen Biosystemer Aps Method and apparatus for conversion of cellulosic material to ethanol
US20090176286A1 (en) 2005-11-23 2009-07-09 O'connor Ryan P Process for Fractionating Lignocellulosic Biomass into Liquid and Solid Products
BRPI0621525B1 (pt) * 2006-03-29 2016-06-14 Virginia Tech Intell Prop processos para fracionar biomssa lignocelulosica baseado em celulose-solvente com condições reacionais moderadas e reciclagem dos reagentes
WO2008017145A1 (en) * 2006-08-07 2008-02-14 Emicellex Energy Corporation Process for recovery of holocellulose and near-native lignin from biomass
RU2338769C1 (ru) * 2007-05-22 2008-11-20 Институт физической химии и электрохимии им. А.Н. Фрумкина Российской академии наук Способ переработки растительного сырья
WO2009021216A2 (en) 2007-08-08 2009-02-12 Bountiful Applied Research Corp. Lignin dewatering process
CN102239184B (zh) * 2008-07-16 2014-07-23 瑞恩麦特克斯股份有限公司 使用一种或多种超临界流体从生物质萃取糠醛和葡萄糖的方法
US8282738B2 (en) 2008-07-16 2012-10-09 Renmatix, Inc. Solvo-thermal fractionation of biomass
JP5339341B2 (ja) * 2008-08-13 2013-11-13 宜章 大木 亜臨界状態による木材の繊維を線維固形分としての分離方法
JP5410060B2 (ja) * 2008-10-02 2014-02-05 株式会社Kri イオン液体によるリグノセルロース系バイオマスのセルロースとリグニンの分離化方法
KR101657100B1 (ko) * 2008-10-29 2016-09-19 삼성전자주식회사 리그노셀룰로오스계 바이오매스의 분별방법 및 분별장치
EP2421911B1 (en) 2009-04-23 2014-06-18 Greenfield Ethanol Inc. Separation of reactive cellulose from lignocellulosic biomass with high lignin content
MX2012000591A (es) * 2009-07-13 2012-06-01 Beta Renewables Spa Procedimiento para la separacion de lignina a alta temperatura.
CN101974161B (zh) * 2010-09-30 2012-10-31 中国科学院西双版纳热带植物园 一种溶解和快速水解木质纤维素生物质的方法及其设备和应用

Also Published As

Publication number Publication date
US20120282467A1 (en) 2012-11-08
AU2012250560A1 (en) 2013-11-07
JP5905570B2 (ja) 2016-04-20
BR112013028146A2 (pt) 2017-04-25
NZ616924A (en) 2015-10-30
CN103502320A (zh) 2014-01-08
EP2705074B1 (en) 2017-11-01
CN103502320B (zh) 2016-03-30
SG194704A1 (en) 2013-12-30
JP2014513740A (ja) 2014-06-05
KR20140027376A (ko) 2014-03-06
CA2834856A1 (en) 2012-11-08
WO2012151509A3 (en) 2013-03-21
US8317928B1 (en) 2012-11-27
RU2508301C1 (ru) 2014-02-27
WO2012151509A2 (en) 2012-11-08
US8404051B2 (en) 2013-03-26
US20120282466A1 (en) 2012-11-08
EP2705074A2 (en) 2014-03-12
AU2012250560B2 (en) 2015-11-19
KR101425765B1 (ko) 2014-08-01
ZA201309031B (en) 2015-03-25
EP2705074A4 (en) 2014-12-03
PH12013502197A1 (en) 2014-01-13

Similar Documents

Publication Publication Date Title
US8317928B1 (en) Lignin production from lignocellulosic biomass
US9624449B2 (en) Biorefinery process for extraction, separation and recovery of fermentable saccharides, other useful compounds, and yield of improved lignocellulosic material from plant biomass
US9777223B2 (en) Process and apparatus for producing liquid hydrocarbon
US8759498B2 (en) Compositions comprising lignin
EP3848437A1 (en) Process and apparatus for producing liquid hydrocarbons
US12559779B2 (en) Processes for improving performance and energy efficiency in biomass conversion to sugars, biochemicals, biofuels, and/or biomaterials
US20180179704A1 (en) Method for processing a cellulosic feedstock at high consistency
WO2015164948A1 (en) Liquid co-extraction process for production of sucrose, xylo-oligosaccharides and xylose from feedstock
US20240301455A1 (en) Methods and systems for optimized feeding of lignocellulosic biomass in the production of sugars, biochemicals, biofuels, and/or biomaterials
NZ616924B2 (en) Lignin production from lignocellulosic biomass

Legal Events

Date Code Title Description
EEER Examination request

Effective date: 20170501

MKLA Lapsed

Effective date: 20210504