CA2553011A1 - Procede de production d'adipodinitrile par hydrocyanuration de 1,3-butadiene - Google Patents

Procede de production d'adipodinitrile par hydrocyanuration de 1,3-butadiene Download PDF

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Publication number
CA2553011A1
CA2553011A1 CA002553011A CA2553011A CA2553011A1 CA 2553011 A1 CA2553011 A1 CA 2553011A1 CA 002553011 A CA002553011 A CA 002553011A CA 2553011 A CA2553011 A CA 2553011A CA 2553011 A1 CA2553011 A1 CA 2553011A1
Authority
CA
Canada
Prior art keywords
catalyst
stream
nickel
pentenenitrile
process step
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA002553011A
Other languages
English (en)
Inventor
Michael Bartsch
Robert Baumann
Gerd Haderlein
Miguel Angel Flores
Tim Jungkamp
Hermann Luyken
Jens Scheidel
Wolfgang Siegel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=34801259&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CA2553011(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Individual filed Critical Individual
Publication of CA2553011A1 publication Critical patent/CA2553011A1/fr
Abandoned legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00Preparation of carboxylic acid nitriles
    • C07C253/08Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds
    • C07C253/10Preparation of carboxylic acid nitriles by addition of hydrogen cyanide or salts thereof to unsaturated compounds to compounds containing carbon-to-carbon double bonds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00Preparation of carboxylic acid nitriles
    • C07C253/30Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00Preparation of carboxylic acid nitriles
    • C07C253/32Separation; Purification; Stabilisation; Use of additives
    • C07C253/34Separation; Purification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00Carboxylic acid nitriles
    • C07C255/01Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/02Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms of an acyclic and saturated carbon skeleton
    • C07C255/04Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms of an acyclic and saturated carbon skeleton containing two cyano groups bound to the carbon skeleton

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CA002553011A 2004-01-29 2005-01-26 Procede de production d'adipodinitrile par hydrocyanuration de 1,3-butadiene Abandoned CA2553011A1 (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102004004682A DE102004004682A1 (de) 2004-01-29 2004-01-29 Verfahren zur Herstellung von Adipodinitril durch Hydrocyanierung von 1,3-Butadien
DE102004004682.4 2004-01-29
PCT/EP2005/000717 WO2005073167A1 (fr) 2004-01-29 2005-01-26 Procede de production d'adipodinitrile par hydrocyanuration de 1,3-butadiene

Publications (1)

Publication Number Publication Date
CA2553011A1 true CA2553011A1 (fr) 2005-08-11

Family

ID=34801259

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002553011A Abandoned CA2553011A1 (fr) 2004-01-29 2005-01-26 Procede de production d'adipodinitrile par hydrocyanuration de 1,3-butadiene

Country Status (14)

Country Link
US (1) US7528275B2 (fr)
EP (1) EP1713759B1 (fr)
JP (1) JP4509124B2 (fr)
KR (1) KR101146403B1 (fr)
CN (1) CN100564353C (fr)
AR (1) AR048151A1 (fr)
AT (1) ATE486844T1 (fr)
BR (1) BRPI0507184B1 (fr)
CA (1) CA2553011A1 (fr)
DE (2) DE102004004682A1 (fr)
ES (1) ES2355732T3 (fr)
MY (1) MY144096A (fr)
TW (1) TW200530160A (fr)
WO (1) WO2005073167A1 (fr)

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DE10136488A1 (de) * 2001-07-27 2003-02-06 Basf Ag Ni(O) enthaltendes Katalysatorsystem
FR2850966B1 (fr) * 2003-02-10 2005-03-18 Rhodia Polyamide Intermediates Procede de fabrication de composes dinitriles
FR2854891B1 (fr) 2003-05-12 2006-07-07 Rhodia Polyamide Intermediates Procede de preparation de dinitriles
FR2878848B1 (fr) * 2004-12-07 2007-01-05 Rhodia Chimie Sa Procede de fabrication de composes dinitriles
EP1948591A1 (fr) 2005-10-18 2008-07-30 INVISTA Technologies S.à.r.l. Procede de preparation de 3-aminopentanenitrile
US7629484B2 (en) 2006-03-17 2009-12-08 Invista North America S.A.R.L. Method for the purification of triorganophosphites by treatment with a basic additive
US7709674B2 (en) * 2006-07-14 2010-05-04 Invista North America S.A R.L Hydrocyanation process with reduced yield losses
US7919646B2 (en) 2006-07-14 2011-04-05 Invista North America S.A R.L. Hydrocyanation of 2-pentenenitrile
US7880028B2 (en) * 2006-07-14 2011-02-01 Invista North America S.A R.L. Process for making 3-pentenenitrile by hydrocyanation of butadiene
WO2008017626A1 (fr) * 2006-08-08 2008-02-14 Basf Se Procédé de préparation de 3-pentènenitrile par hydrocyanuration de 1,3-butadiène
WO2009075692A2 (fr) 2007-05-14 2009-06-18 Invista Technologies S.A.R.L. Réacteur et procédé à haut rendement
WO2008157218A1 (fr) 2007-06-13 2008-12-24 Invista Technologies S.A.R.L. Procédé pour améliorer la qualité de l'adiponitrile
US7977502B2 (en) * 2008-01-15 2011-07-12 Invista North America S.A R.L. Process for making and refining 3-pentenenitrile, and for refining 2-methyl-3-butenenitrile
CN101918356B (zh) * 2008-01-15 2013-09-25 因温斯特技术公司 戊烯腈的氢氰化
FR2926549B1 (fr) * 2008-01-18 2015-05-01 Rhodia Operations Procede de fabrication de composes nitriles
JP2011515411A (ja) * 2008-03-19 2011-05-19 インビスタ テクノロジーズ エス エイ アール エル シクロドデカトリエンの製造方法およびラウロラクトンの製造方法
US8247621B2 (en) 2008-10-14 2012-08-21 Invista North America S.A.R.L. Process for making 2-secondary-alkyl-4,5-di-(normal-alkyl)phenols
KR20120047251A (ko) 2009-08-07 2012-05-11 인비스타 테크놀러지스 에스.에이.알.엘. 디에스테르를 형성하기 위한 수소화 및 에스테르화
US8815186B2 (en) * 2009-12-18 2014-08-26 Invista North America S.A.R.L. Nickel compositions for preparing nickel metal and nickel complexes
FR2960236B1 (fr) * 2010-05-21 2012-05-11 Rhodia Operations Procede de fabrication de composes comprenant des fonctions nitriles
WO2012005916A1 (fr) 2010-07-07 2012-01-12 Invista Technologies S.A.R.L. Méthode de production de nitriles
EP2614070B1 (fr) 2010-09-07 2017-07-26 Invista Technologies S.à r.l. Compositions de nickel pour préparer un métal nickel et des complexes à base de nickel
KR20140039268A (ko) 2011-06-10 2014-04-01 인비스타 테크놀러지스 에스.에이 알.엘. 유동층 반응기를 포함하는 하소 및 환원 방법
CN103732323B (zh) 2011-06-10 2016-09-14 因温斯特技术公司 用于催化镍-配体配合物的制备的镍形式
US9133226B2 (en) 2011-12-21 2015-09-15 Invista North America S.A.R.L. Extraction solvent control for reducing stable emulsions
JP2015512862A (ja) 2011-12-21 2015-04-30 インヴィスタ テクノロジーズ エスアエルエル 安定なエマルジョンを減じるための抽出溶媒制御
EP2794048B1 (fr) 2011-12-21 2022-01-05 INVISTA Textiles (U.K.) Limited Contrôle de solvant d'extraction pour réduire des emulsions stables
EP2657224A1 (fr) * 2012-04-27 2013-10-30 Basf Se Procédé d'isomérisation de cis-2-pentènenitrile en 3-pentènenitrile
CN103965056B (zh) 2012-12-18 2017-04-12 英威达科技公司 用于生产六亚甲基二胺的一体化方法
CN107082752B (zh) * 2013-07-17 2021-06-15 英威达纺织(英国)有限公司 通过蒸馏将溶剂与镍催化剂分离
CN103664691B (zh) * 2013-12-27 2016-01-20 安徽省安庆市曙光化工股份有限公司 制备己二腈的方法
SI3102562T1 (en) 2014-02-07 2018-05-31 Basf Se Method for purification of adipodinitrile (ADN)
CN103804229B (zh) * 2014-02-17 2016-08-24 重庆中平紫光科技发展有限公司 丁二烯法合成己二腈中抑制含磷配体降解的方法
EP2998290A1 (fr) 2014-09-16 2016-03-23 Basf Se Procédé de fabrication continue d'adipodinitrile
CN108640854A (zh) * 2018-04-28 2018-10-12 山东豪迈化工技术有限公司 一种己二腈的合成方法
CN108997167B (zh) * 2018-08-09 2021-05-07 大连微凯化学有限公司 一种利用丁二烯氢氰化制备己二腈和甲基戊二腈的方法
CN111995547B (zh) * 2020-01-19 2021-07-09 浙江新和成股份有限公司 己二腈的制备方法和装置
US20230047439A1 (en) * 2020-01-31 2023-02-16 Inv Nylon Chemicals Americas, Llc Impurity formation reduction during product refining
CN112794948B (zh) 2020-12-31 2022-08-26 浙江大学 多孔聚合物及其制备方法、催化剂以及己二腈的制备方法

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3496215A (en) 1965-11-23 1970-02-17 Du Pont Hydrocyanation of olefins using selected nickel phosphite catalysts
GB1112539A (en) 1965-11-26 1968-05-08 Du Pont Preparation of organic nitriles
US3496217A (en) 1967-05-23 1970-02-17 Du Pont Hydrocyanation of olefins
US3773809A (en) 1972-06-28 1973-11-20 Du Pont Separation of organic phosphorus compounds and their metal complexes from organic nitriles in the hydrocyanation of olefins
US3850973A (en) 1973-09-26 1974-11-26 Du Pont Hydrocyanation of conjugated diolefins
US4774353A (en) 1986-06-05 1988-09-27 E. I. Du Pont De Nemours And Company Triorganotin catalyst promoters for hydrocyanation
US4874884A (en) 1988-03-31 1989-10-17 E. I. Du Pont De Nemours And Company Promoter synergism in pentenenitrile hydrocyanation
US5693843A (en) 1995-12-22 1997-12-02 E. I. Du Pont De Nemours And Company Process for hydrocyanation of diolefins and isomerization of nonconjugated 2 alkyl-3-monoalkenenitriles
MY124170A (en) 1997-07-29 2006-06-30 Invista Tech Sarl Hydrocyanation processes and multidentate phosphite ligand and nickel catalyst compositions therefor
DE19733682A1 (de) * 1997-08-04 1999-02-11 Basf Ag Verfahren zur Herstellung von Gemischen monoolefinischer C¶5¶-Mononitrile durch katalytische Hydrocyanierung in Gegenwart eines katalysators, umfassend wenigstens einen Metallocenphosphor(III)-Nickel(0)-Komplex
DE19740180A1 (de) 1997-09-12 1999-03-18 Basf Ag Katalysator, umfassend wenigstens einen Nickel(0)Komplex auf Basis eines Phosphonitliganden und Verfahren zur Herstellung von Nitrilen
US6380421B1 (en) 1999-09-20 2002-04-30 E. I. Du Pont De Nemours And Company Multidentate phosphite ligands, catalytic compositions containing such ligands and catalytic processes utilizing such catalytic compositions
DE10046025A1 (de) * 2000-09-18 2002-03-28 Basf Ag Verfahren zur Herstellung von Adipinsäuredinitril
FR2815344B1 (fr) 2000-10-13 2004-01-30 Rhodia Polyamide Intermediates Procede d'hydrocyanation de composes organiques a insaturation ethylenique
FR2819250B1 (fr) * 2001-01-05 2004-12-03 Rhodia Polyamide Intermediates Procede de fabrication de composes nitriles a partir de composes a insaturation ethylenique
DE10136488A1 (de) * 2001-07-27 2003-02-06 Basf Ag Ni(O) enthaltendes Katalysatorsystem
FR2830530B1 (fr) * 2001-10-08 2004-07-02 Rhodia Polyamide Intermediates Procede de transformation, d'une part, de composes a insaturation ethylenique en nitriles et, d'autre part, de nitriles branches en nitriles lineaires
DE10351002A1 (de) 2003-10-30 2005-05-25 Basf Ag Einsatz von azeotrop-getrockneten Nickel(II)-halogeniden
DE102004004671A1 (de) 2004-01-29 2005-08-18 Basf Ag Verfahren zur Herstellung von linearem Pentennitril
DE102004004683A1 (de) 2004-01-29 2005-08-18 Basf Ag Verfahren zur Herstellung von Dinitrilen

Also Published As

Publication number Publication date
MY144096A (en) 2011-08-15
US7528275B2 (en) 2009-05-05
JP2007519663A (ja) 2007-07-19
AR048151A1 (es) 2006-04-05
ATE486844T1 (de) 2010-11-15
DE502005010476D1 (de) 2010-12-16
TW200530160A (en) 2005-09-16
US20080221351A1 (en) 2008-09-11
BRPI0507184B1 (pt) 2014-06-24
CN100564353C (zh) 2009-12-02
CN1914160A (zh) 2007-02-14
EP1713759B1 (fr) 2010-11-03
DE102004004682A1 (de) 2005-08-18
EP1713759A1 (fr) 2006-10-25
BRPI0507184A (pt) 2007-06-26
KR20070011279A (ko) 2007-01-24
ES2355732T3 (es) 2011-03-30
JP4509124B2 (ja) 2010-07-21
KR101146403B1 (ko) 2012-05-17
WO2005073167A1 (fr) 2005-08-11

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Legal Events

Date Code Title Description
EEER Examination request
FZDE Discontinued