CA2552000A1 - Process for preparing fluorochemical monoisocyanates - Google Patents
Process for preparing fluorochemical monoisocyanates Download PDFInfo
- Publication number
- CA2552000A1 CA2552000A1 CA002552000A CA2552000A CA2552000A1 CA 2552000 A1 CA2552000 A1 CA 2552000A1 CA 002552000 A CA002552000 A CA 002552000A CA 2552000 A CA2552000 A CA 2552000A CA 2552000 A1 CA2552000 A1 CA 2552000A1
- Authority
- CA
- Canada
- Prior art keywords
- fluorochemical
- solvent
- alcohol
- monoisocyanate
- mdi
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract 10
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 claims abstract 8
- 239000002904 solvent Substances 0.000 claims abstract 7
- 238000000034 method Methods 0.000 claims 16
- 239000000203 mixture Substances 0.000 claims 9
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 3
- 239000012948 isocyanate Substances 0.000 claims 3
- 150000002513 isocyanates Chemical class 0.000 claims 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- DJXNLVJQMJNEMN-UHFFFAOYSA-N 2-[difluoro(methoxy)methyl]-1,1,1,2,3,3,3-heptafluoropropane Chemical compound COC(F)(F)C(F)(C(F)(F)F)C(F)(F)F DJXNLVJQMJNEMN-UHFFFAOYSA-N 0.000 claims 1
- FNUBKINEQIEODM-UHFFFAOYSA-N 3,3,4,4,5,5,5-heptafluoropentanal Chemical compound FC(F)(F)C(F)(F)C(F)(F)CC=O FNUBKINEQIEODM-UHFFFAOYSA-N 0.000 claims 1
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical group CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 239000012975 dibutyltin dilaurate Substances 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 125000002768 hydroxyalkyl group Chemical group 0.000 claims 1
- 239000012454 non-polar solvent Substances 0.000 claims 1
- 239000003208 petroleum Substances 0.000 claims 1
- 150000003512 tertiary amines Chemical class 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
- C07C303/40—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reactions not involving the formation of sulfonamide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
- C07C311/01—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms
- C07C311/02—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
- C07C311/09—Sulfonamides having sulfur atoms of sulfonamide groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton the carbon skeleton being further substituted by at least two halogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyurethanes Or Polyureas (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/751,142 | 2003-12-31 | ||
| US10/751,142 US7081545B2 (en) | 2003-12-31 | 2003-12-31 | Process for preparing fluorochemical monoisocyanates |
| PCT/US2004/041743 WO2005065164A2 (en) | 2003-12-31 | 2004-12-14 | Process for preparing fluorochemical monoisocyanates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2552000A1 true CA2552000A1 (en) | 2005-07-21 |
Family
ID=34701272
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002552000A Abandoned CA2552000A1 (en) | 2003-12-31 | 2004-12-14 | Process for preparing fluorochemical monoisocyanates |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US7081545B2 (enExample) |
| EP (1) | EP1699755B1 (enExample) |
| JP (1) | JP4965264B2 (enExample) |
| KR (1) | KR20060107836A (enExample) |
| CN (1) | CN100471834C (enExample) |
| AT (1) | ATE525348T1 (enExample) |
| CA (1) | CA2552000A1 (enExample) |
| WO (1) | WO2005065164A2 (enExample) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1709089B1 (en) * | 2003-12-31 | 2008-03-05 | 3M Innovative Properties Company | Water-and oil-repellent fluoroacrylates |
| US20060142530A1 (en) * | 2004-12-28 | 2006-06-29 | Moore George G | Water- and oil-repellent fluorourethanes and fluoroureas |
| US7345123B2 (en) * | 2004-12-28 | 2008-03-18 | 3M Innovative Properties Company | Fluoroacrylate-multifunctional acrylate copolymer compositions |
| US7411020B2 (en) | 2004-12-28 | 2008-08-12 | 3M Innovative Properties Company | Water-based release coating containing fluorochemical |
| US7253241B2 (en) | 2004-12-28 | 2007-08-07 | 3M Innovative Properties Company | Fluorochemical containing low adhesion backsize |
| US7291688B2 (en) * | 2004-12-28 | 2007-11-06 | 3M Innovative Properties Company | Fluoroacrylate-mercaptofunctional copolymers |
| MX2008000251A (es) * | 2005-06-29 | 2008-03-18 | 3M Innovative Properties Co | Poliuretanos derivados de fluoroacrilatos oligomericos. |
| US7279210B2 (en) * | 2005-09-07 | 2007-10-09 | 3M Innovative Properties Company | Curable compositions, methods of making and using the same, and articles therefrom |
| US7560166B2 (en) * | 2005-12-28 | 2009-07-14 | 3M Innovative Properties Company | Adhesive article, composite article, and methods of making the same |
| US7981988B2 (en) * | 2006-05-25 | 2011-07-19 | 3M Innovative Properties Company | Ultraviolet radiation-polymerizable compositions |
| US20080075951A1 (en) * | 2006-09-27 | 2008-03-27 | 3M Innovative Properties Company | Fluoroacrylates and hardcoat compositions including the same |
| US8530054B2 (en) * | 2006-09-27 | 2013-09-10 | 3M Innovative Properties Company | Solar control multilayer film |
| US20080229976A1 (en) * | 2006-12-29 | 2008-09-25 | 3M Innovative Properties Company | Stain and fouling resistant polyurea and polyurethane coatings |
| JP5706886B2 (ja) | 2009-06-12 | 2015-04-22 | スリーエム イノベイティブ プロパティズ カンパニー | フッ素化芳香族ビス（アシル）含有化合物及びそれから調製されるポリエステル |
| CN102686561B (zh) | 2009-12-22 | 2014-03-05 | 3M创新有限公司 | 氟化的含亚芳基化合物、方法以及由其制得的聚合物 |
| CN104927024A (zh) * | 2014-03-20 | 2015-09-23 | 江南大学 | 一种氟改性光固化聚氨酯丙烯酸酯树脂的制备方法及其作为光固化涂层疏水填料的应用 |
Family Cites Families (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2803656A (en) | 1956-01-23 | 1957-08-20 | Minnesota Mining & Mfg | Fluorocarbonsulfonamidoalkanols and sulfates thereof |
| US3776805A (en) | 1971-09-07 | 1973-12-04 | Minnesota Mining & Mfg | Solar control products |
| US4321404A (en) | 1980-05-20 | 1982-03-23 | Minnesota Mining And Manufacturing Company | Compositions for providing abherent coatings |
| US4540497A (en) * | 1982-11-09 | 1985-09-10 | Minnesota Mining And Manufacturing Company | Fluoroaliphatic radical-containing, substituted guanidines and fibrous substrates treated therewith |
| US4566981A (en) * | 1984-03-30 | 1986-01-28 | Minnesota Mining And Manufacturing Company | Fluorochemicals and fibrous substrates treated therewith: compositions of cationic and non-ionic fluorochemicals |
| US4668726A (en) * | 1984-03-30 | 1987-05-26 | Minnesota Mining And Manufacturing Company | Cationic and non-ionic fluorochemicals and fibrous substrates treated therewith |
| DE3521762A1 (de) * | 1985-06-19 | 1987-01-02 | Bayer Ag | Ionisch modifizierte pur-streichpasten und ihre verwendung |
| FR2588555B1 (fr) | 1985-10-16 | 1987-12-11 | Atochem | Monomeres acryliques fluores, polymeres en derivant et leur application au traitement hydrofuge et oleofuge de substrats divers |
| US5144056A (en) | 1985-12-03 | 1992-09-01 | Atochem | Fluorinated acrylic monomers as hydrophobic and oleophobic agents |
| FR2590895B1 (fr) | 1985-12-03 | 1988-01-15 | Atochem | Monomeres acryliques fluores, polymeres en derivant et leur application comme agents hydrophobes et oleophobes |
| CA2048232A1 (en) | 1990-09-05 | 1992-03-06 | Jerry W. Williams | Energy curable pressure-sensitive compositions |
| JPH0689462A (ja) | 1992-09-07 | 1994-03-29 | Three Bond Co Ltd | 光ディスク |
| TW312700B (enExample) | 1994-05-17 | 1997-08-11 | Sony Co Ltd | |
| US5446118A (en) | 1994-08-11 | 1995-08-29 | W. L. Gore & Associates, Inc. | Fluorinated acrylic monomers containing urethane groups and their polymers |
| US6017603A (en) | 1995-04-28 | 2000-01-25 | Nippon Kayaku Kabushiki Kaisha | Ultraviolet-curing adhesive composition and article |
| US5688884A (en) | 1995-08-31 | 1997-11-18 | E. I. Du Pont De Nemours And Company | Polymerization process |
| DE19541174C2 (de) | 1995-11-04 | 1998-11-26 | Spraying Systems Deutschland G | Hochleistungsstrahldüse |
| JPH09291258A (ja) | 1996-04-26 | 1997-11-11 | Lintec Corp | 粘着剤組成物およびこれを用いた粘着シート |
| JP3835857B2 (ja) | 1996-06-18 | 2006-10-18 | 日本化薬株式会社 | 光ディスク用接着剤組成物、硬化物、物品及び接着方法 |
| JPH1025453A (ja) | 1996-07-08 | 1998-01-27 | Nippon Kayaku Co Ltd | 陰極線管用接着剤及びその硬化物 |
| JP3911728B2 (ja) | 1996-08-07 | 2007-05-09 | 住友化学株式会社 | ディジタルビデオディスクの保護コート兼接着用樹脂組成物 |
| JPH10140090A (ja) | 1996-11-08 | 1998-05-26 | Daicel U C B Kk | 陰極線管用接着剤およびその硬化物 |
| EP0960355A1 (en) | 1997-02-13 | 1999-12-01 | Dsm N.V. | Photocurable resin composition |
| TW430672B (en) | 1997-07-03 | 2001-04-21 | Sumitomo Chemical Co | A photo-curing resin composition for DVD |
| US5959775A (en) | 1997-12-23 | 1999-09-28 | 3M Innovative Properties Company | Urethane/acrylate bead bond for retroreflective articles |
| US6180200B1 (en) | 1998-06-01 | 2001-01-30 | Dsm N. V. | Cationic and hybrid radiation curable pressure sensitive adhesives for bonding of optical discs |
| JP4855616B2 (ja) * | 1999-10-27 | 2012-01-18 | スリーエム イノベイティブ プロパティズ カンパニー | フルオロケミカルスルホンアミド界面活性剤 |
| DE19962272A1 (de) | 1999-12-23 | 2001-06-28 | Basf Ag | Isocyanatgruppen aufweisende Bausteine sowie ihre Verwendung zur Funktionalisierung oder Modifizierung von Verbindungen oder Oberflächen |
| EP1142912A1 (en) | 2000-04-05 | 2001-10-10 | Dsm N.V. | Radiation curable compositions |
| US6949297B2 (en) | 2001-11-02 | 2005-09-27 | 3M Innovative Properties Company | Hybrid adhesives, articles, and methods |
| EP1709089B1 (en) * | 2003-12-31 | 2008-03-05 | 3M Innovative Properties Company | Water-and oil-repellent fluoroacrylates |
-
2003
- 2003-12-31 US US10/751,142 patent/US7081545B2/en not_active Expired - Fee Related
-
2004
- 2004-12-14 CA CA002552000A patent/CA2552000A1/en not_active Abandoned
- 2004-12-14 WO PCT/US2004/041743 patent/WO2005065164A2/en not_active Ceased
- 2004-12-14 JP JP2006547104A patent/JP4965264B2/ja not_active Expired - Fee Related
- 2004-12-14 KR KR1020067013191A patent/KR20060107836A/ko not_active Withdrawn
- 2004-12-14 EP EP04813986A patent/EP1699755B1/en not_active Expired - Lifetime
- 2004-12-14 AT AT04813986T patent/ATE525348T1/de not_active IP Right Cessation
- 2004-12-14 CN CNB2004800396658A patent/CN100471834C/zh not_active Expired - Fee Related
-
2006
- 2006-07-12 US US11/457,037 patent/US7361782B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| WO2005065164A3 (en) | 2005-09-09 |
| ATE525348T1 (de) | 2011-10-15 |
| CN1902164A (zh) | 2007-01-24 |
| EP1699755B1 (en) | 2011-09-21 |
| US7361782B2 (en) | 2008-04-22 |
| US20050143595A1 (en) | 2005-06-30 |
| WO2005065164A2 (en) | 2005-07-21 |
| EP1699755A2 (en) | 2006-09-13 |
| JP4965264B2 (ja) | 2012-07-04 |
| KR20060107836A (ko) | 2006-10-16 |
| JP2007517033A (ja) | 2007-06-28 |
| CN100471834C (zh) | 2009-03-25 |
| US20060247460A1 (en) | 2006-11-02 |
| EP1699755A4 (en) | 2007-11-07 |
| US7081545B2 (en) | 2006-07-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| FZDE | Discontinued |
Effective date: 20131018 |