CA1275224C - Process for manufacture of detergent powder - Google Patents
Process for manufacture of detergent powderInfo
- Publication number
- CA1275224C CA1275224C CA000517637A CA517637A CA1275224C CA 1275224 C CA1275224 C CA 1275224C CA 000517637 A CA000517637 A CA 000517637A CA 517637 A CA517637 A CA 517637A CA 1275224 C CA1275224 C CA 1275224C
- Authority
- CA
- Canada
- Prior art keywords
- weight
- phosphate
- detergency builder
- sugar
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000843 powder Substances 0.000 title claims abstract description 47
- 239000003599 detergent Substances 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 title claims description 18
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 239000000203 mixture Substances 0.000 claims abstract description 40
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 32
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 32
- 239000010452 phosphate Substances 0.000 claims abstract description 32
- 239000002002 slurry Substances 0.000 claims abstract description 20
- 235000000346 sugar Nutrition 0.000 claims abstract description 18
- 239000000344 soap Substances 0.000 claims abstract description 17
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000004094 surface-active agent Substances 0.000 claims abstract description 15
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 14
- 229910000323 aluminium silicate Inorganic materials 0.000 claims abstract description 13
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 11
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 10
- 229930006000 Sucrose Natural products 0.000 claims abstract description 10
- 239000005720 sucrose Substances 0.000 claims abstract description 10
- 238000001694 spray drying Methods 0.000 claims abstract description 9
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims abstract description 6
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims abstract description 6
- 239000000600 sorbitol Substances 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 239000007921 spray Substances 0.000 claims description 17
- 239000004615 ingredient Substances 0.000 claims description 8
- 229920002472 Starch Polymers 0.000 claims description 7
- 235000019698 starch Nutrition 0.000 claims description 7
- 239000008107 starch Substances 0.000 claims description 6
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 4
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 3
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims description 3
- GUBGYTABKSRVRQ-CUHNMECISA-N D-Cellobiose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-CUHNMECISA-N 0.000 claims description 3
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 3
- 229930091371 Fructose Natural products 0.000 claims description 3
- 239000005715 Fructose Substances 0.000 claims description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 3
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 3
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000008103 glucose Substances 0.000 claims description 3
- 150000004676 glycans Polymers 0.000 claims description 3
- 239000008101 lactose Substances 0.000 claims description 3
- 239000005017 polysaccharide Substances 0.000 claims description 3
- 150000004804 polysaccharides Polymers 0.000 claims description 3
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- 239000013078 crystal Substances 0.000 claims description 2
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- 239000004115 Sodium Silicate Substances 0.000 abstract description 14
- 229910052911 sodium silicate Inorganic materials 0.000 abstract description 14
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 abstract description 13
- 229910000288 alkali metal carbonate Inorganic materials 0.000 abstract description 2
- 150000008041 alkali metal carbonates Chemical class 0.000 abstract description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 9
- 229910052708 sodium Inorganic materials 0.000 description 9
- 239000011734 sodium Substances 0.000 description 9
- 239000010457 zeolite Substances 0.000 description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 7
- 238000009472 formulation Methods 0.000 description 7
- 229910021536 Zeolite Inorganic materials 0.000 description 6
- 229910000503 Na-aluminosilicate Inorganic materials 0.000 description 5
- 150000001720 carbohydrates Chemical group 0.000 description 5
- 125000004432 carbon atom Chemical group C* 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 230000000704 physical effect Effects 0.000 description 5
- -1 sodium alkyl benzene Chemical class 0.000 description 5
- 235000012217 sodium aluminium silicate Nutrition 0.000 description 5
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 4
- 239000001768 carboxy methyl cellulose Substances 0.000 description 4
- 239000000377 silicon dioxide Substances 0.000 description 4
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 4
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000005342 ion exchange Methods 0.000 description 3
- 150000003138 primary alcohols Chemical class 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 150000008163 sugars Chemical class 0.000 description 3
- 239000003760 tallow Substances 0.000 description 3
- 125000006539 C12 alkyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
- 229920002261 Corn starch Polymers 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- SRSXLGNVWSONIS-UHFFFAOYSA-M benzenesulfonate Chemical compound [O-]S(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-M 0.000 description 2
- 150000001719 carbohydrate derivatives Chemical class 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 235000019198 oils Nutrition 0.000 description 2
- 239000011368 organic material Substances 0.000 description 2
- 230000001376 precipitating effect Effects 0.000 description 2
- 150000003333 secondary alcohols Chemical class 0.000 description 2
- 239000000429 sodium aluminium silicate Substances 0.000 description 2
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 2
- DZCAZXAJPZCSCU-UHFFFAOYSA-K sodium nitrilotriacetate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CC([O-])=O DZCAZXAJPZCSCU-UHFFFAOYSA-K 0.000 description 2
- 235000019832 sodium triphosphate Nutrition 0.000 description 2
- 239000001117 sulphuric acid Substances 0.000 description 2
- 235000011149 sulphuric acid Nutrition 0.000 description 2
- RNAMYOYQYRYFQY-UHFFFAOYSA-N 2-(4,4-difluoropiperidin-1-yl)-6-methoxy-n-(1-propan-2-ylpiperidin-4-yl)-7-(3-pyrrolidin-1-ylpropoxy)quinazolin-4-amine Chemical compound N1=C(N2CCC(F)(F)CC2)N=C2C=C(OCCCN3CCCC3)C(OC)=CC2=C1NC1CCN(C(C)C)CC1 RNAMYOYQYRYFQY-UHFFFAOYSA-N 0.000 description 1
- 240000002791 Brassica napus Species 0.000 description 1
- 235000004977 Brassica sinapistrum Nutrition 0.000 description 1
- 229910021532 Calcite Inorganic materials 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 1
- 235000019759 Maize starch Nutrition 0.000 description 1
- 235000019483 Peanut oil Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- BCKXLBQYZLBQEK-KVVVOXFISA-M Sodium oleate Chemical compound [Na+].CCCCCCCC\C=C/CCCCCCCC([O-])=O BCKXLBQYZLBQEK-KVVVOXFISA-M 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 235000019486 Sunflower oil Nutrition 0.000 description 1
- BGRWYDHXPHLNKA-UHFFFAOYSA-N Tetraacetylethylenediamine Chemical compound CC(=O)N(C(C)=O)CCN(C(C)=O)C(C)=O BGRWYDHXPHLNKA-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 150000001279 adipic acids Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 150000004996 alkyl benzenes Chemical class 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 230000003466 anti-cipated effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- AYJRCSIUFZENHW-DEQYMQKBSA-L barium(2+);oxomethanediolate Chemical compound [Ba+2].[O-][14C]([O-])=O AYJRCSIUFZENHW-DEQYMQKBSA-L 0.000 description 1
- 150000001642 boronic acid derivatives Chemical class 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 229920003086 cellulose ether Polymers 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000002385 cottonseed oil Substances 0.000 description 1
- 235000012343 cottonseed oil Nutrition 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 150000002016 disaccharides Chemical class 0.000 description 1
- BNVZBQVIMPLFNA-UHFFFAOYSA-L disodium;2-(carboxymethoxy)butanedioate Chemical compound [Na+].[Na+].OC(=O)COC(C([O-])=O)CC([O-])=O BNVZBQVIMPLFNA-UHFFFAOYSA-L 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- 150000002311 glutaric acids Chemical class 0.000 description 1
- 125000005456 glyceride group Chemical group 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 229920000592 inorganic polymer Polymers 0.000 description 1
- 150000004682 monohydrates Chemical class 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 235000019865 palm kernel oil Nutrition 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229920001983 poloxamer Polymers 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- 229960001922 sodium perborate Drugs 0.000 description 1
- 229940048086 sodium pyrophosphate Drugs 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 229940074404 sodium succinate Drugs 0.000 description 1
- ZDQYSKICYIVCPN-UHFFFAOYSA-L sodium succinate (anhydrous) Chemical compound [Na+].[Na+].[O-]C(=O)CCC([O-])=O ZDQYSKICYIVCPN-UHFFFAOYSA-L 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- WYPBVHPKMJYUEO-NBTZWHCOSA-M sodium;(9z,12z)-octadeca-9,12-dienoate Chemical compound [Na+].CCCCC\C=C/C\C=C/CCCCCCCC([O-])=O WYPBVHPKMJYUEO-NBTZWHCOSA-M 0.000 description 1
- UNZSHUCNBUBSGW-IFNWOZJISA-M sodium;(9z,12z,15z)-octadeca-9,12,15-trienoate Chemical compound [Na+].CC\C=C/C\C=C/C\C=C/CCCCCCCC([O-])=O UNZSHUCNBUBSGW-IFNWOZJISA-M 0.000 description 1
- MZSDGDXXBZSFTG-UHFFFAOYSA-M sodium;benzenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C1=CC=CC=C1 MZSDGDXXBZSFTG-UHFFFAOYSA-M 0.000 description 1
- YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 150000003444 succinic acids Chemical class 0.000 description 1
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
- 239000000037 vitreous enamel Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/221—Mono, di- or trisaccharides or derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB8522621 | 1985-09-12 | ||
| GB858522621A GB8522621D0 (en) | 1985-09-12 | 1985-09-12 | Detergent powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1275224C true CA1275224C (en) | 1990-10-16 |
Family
ID=10585082
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000517637A Expired - Fee Related CA1275224C (en) | 1985-09-12 | 1986-09-05 | Process for manufacture of detergent powder |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4755318A (ref) |
| EP (1) | EP0215637B2 (ref) |
| JP (1) | JPH0637637B2 (ref) |
| KR (1) | KR870003188A (ref) |
| AU (1) | AU591520B2 (ref) |
| BR (1) | BR8604308A (ref) |
| CA (1) | CA1275224C (ref) |
| DE (1) | DE3682246D1 (ref) |
| ES (1) | ES2002322A6 (ref) |
| GB (2) | GB8522621D0 (ref) |
| IN (1) | IN165359B (ref) |
| ZA (1) | ZA866927B (ref) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MX170188B (es) * | 1989-02-10 | 1993-08-10 | Ciba Geigy | Agentes de lavado para el lavado posterior de materiales textiles en el estampado y teñido con colores reactivos |
| US5024937A (en) * | 1989-04-06 | 1991-06-18 | Dow Corning Corporation | Method for processing aqueous fermentation broths |
| US5078888A (en) * | 1989-04-06 | 1992-01-07 | Dow Corning Corporation | Method for processing aqueous fermentation broths |
| FR2653442A1 (fr) * | 1989-10-23 | 1991-04-26 | Roquette Freres | Composition pour produits de lavage, son procede de preparation et produit de lavage la contenant. |
| US5151212A (en) * | 1990-03-21 | 1992-09-29 | The Belzak Corporation | Peroxygen compound activation |
| FR2659979B1 (fr) * | 1990-03-23 | 1994-04-29 | Roquette Freres | Produit de lavage a teneur reduite ou nulle en phosphates. |
| DE4102745A1 (de) * | 1991-01-30 | 1992-08-06 | Henkel Kgaa | Pulverfoermige tensidmischung |
| DE4134914A1 (de) * | 1991-10-23 | 1993-04-29 | Henkel Kgaa | Wasch- und reinigungsmittel mit ausgewaehlten builder-systemen |
| DE4216453A1 (de) * | 1992-05-19 | 1993-11-25 | Henkel Kgaa | Verfahren zur Herstellung pastenförmiger Waschmittel |
| EP0618286A1 (en) * | 1993-03-30 | 1994-10-05 | AUSIMONT S.p.A. | Process for decreasing the build up of inorganic incrustations on textiles and detergent composition used in such process |
| US5610131A (en) * | 1993-04-30 | 1997-03-11 | The Procter & Gamble Company | Structuring liquid nonionic surfactants prior to granulation process |
| EP0622454A1 (en) * | 1993-04-30 | 1994-11-02 | The Procter & Gamble Company | Structuring liquid nonionic surfactants prior to granulation process |
| US5415801A (en) * | 1993-08-27 | 1995-05-16 | The Procter & Gamble Company | Concentrated light duty liquid or gel dishwashing detergent compositions containing sugar |
| US5474710A (en) * | 1993-08-27 | 1995-12-12 | Ofosu-Asanta; Kofi | Process for preparing concentrated surfactant mixtures containing magnesium |
| DE4329988A1 (de) * | 1993-09-04 | 1995-03-09 | Henkel Kgaa | Sprühgetrocknetes Granulat mit hohem Schüttgewicht |
| US5756445A (en) * | 1993-11-11 | 1998-05-26 | The Proctor & Gamble Company | Granular detergent composition comprising a low bulk density component |
| EP0765378A1 (en) * | 1994-06-13 | 1997-04-02 | The Procter & Gamble Company | Detergent composition containing anionic surfactants and water-soluble saccharides |
| US5650014A (en) * | 1995-04-21 | 1997-07-22 | Tauber; Julius | Sugar additive to reduce caking |
| DE69531207T2 (de) | 1995-09-18 | 2004-04-22 | The Procter & Gamble Company, Cincinnati | Verfahren zur Herstellung von körnigen Reinigungsmitteln |
| US5914320A (en) * | 1996-07-19 | 1999-06-22 | The Procter & Gamble Company | Co-milled mixtures comprising polyol and method of making |
| CN1120231C (zh) * | 1996-08-26 | 2003-09-03 | 普罗格特-甘布尔公司 | 涉及预混修饰的聚胺制备洗涤剂组合物的喷雾干燥法 |
| GB9711359D0 (en) * | 1997-05-30 | 1997-07-30 | Unilever Plc | Detergent powder composition |
| WO1998054289A1 (en) | 1997-05-30 | 1998-12-03 | Unilever Plc | Free-flowing particulate detergent compositions |
| DE19936726A1 (de) * | 1999-08-06 | 2001-02-08 | Henkel Kgaa | Verfahren zur Herstellung cobuilder-haltiger Zubereitungen |
| KR100334733B1 (ko) * | 1999-08-09 | 2002-05-04 | 안용찬 | 고밀도분말세제의 제조방법 |
| KR20040019483A (ko) * | 2002-08-28 | 2004-03-06 | 정근식 | 분말세제 조성물 및 그 제조방법 |
| KR101087405B1 (ko) * | 2005-12-08 | 2011-11-25 | 애경산업(주) | 주방용 액체 세제 조성물 |
| DE102006054436A1 (de) | 2006-11-16 | 2008-05-21 | Henkel Kgaa | Feste, textil- und/oder hautpflegende Zusammensetzung |
| CN106893638A (zh) * | 2017-01-20 | 2017-06-27 | 西安那片森林农业科技有限公司 | 一种天然葡萄清洗粉及其制备方法 |
| WO2024138657A1 (en) * | 2022-12-30 | 2024-07-04 | The Procter & Gamble Company | Spray-dried particulate composition |
Family Cites Families (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3615811A (en) * | 1968-02-29 | 1971-10-26 | Chemical Products Corp | Carbonate compositions and process |
| SE352652B (ref) * | 1969-10-01 | 1973-01-08 | Hentschel V | |
| DE2148279A1 (de) * | 1970-09-30 | 1972-04-06 | Unilever N V , Rotterdam (Nieder lande) | Geruststoffe fur Detergensmittel |
| US3701735A (en) * | 1971-04-12 | 1972-10-31 | Colgate Palmolive Co | Automatic dishwashing compositions |
| SE391343B (sv) * | 1971-06-17 | 1977-02-14 | Hentschel V S E | Tvett-, disk- och rengoringsmedel med vattenavherdare och tvetteffektforsterkare |
| GB1383407A (en) * | 1971-07-29 | 1974-02-12 | Colgate Palmolive Co | Detergent compositions |
| BE789685A (fr) * | 1971-10-05 | 1973-02-01 | Diamalt Ag | Produits de lavage |
| CA991942A (en) * | 1972-04-28 | 1976-06-29 | Lawrence Benjamin | Detergent composition containing crystallization seed and soap |
| US3816352A (en) * | 1972-11-01 | 1974-06-11 | V Loureiro | Spray dried alpha-olefin sulfonate detergent compositions |
| US4076653A (en) * | 1973-08-08 | 1978-02-28 | Lever Brothers Company | Detergent compositions |
| GB1481685A (en) * | 1973-08-15 | 1977-08-03 | Unilever Ltd | Detergent ingredient |
| US4054541A (en) * | 1974-11-04 | 1977-10-18 | Witco Chemical Corporation | Spray dried alcohol ether sulfate detergent compositions |
| GB1481585A (en) * | 1975-06-10 | 1977-08-03 | Tsnii Travmatol I Ortoped Im N | Apparatus for surgical treatment of fractured bones or of bone joints |
| JPS5294304A (en) * | 1976-02-03 | 1977-08-08 | Yuken Kagaku Kougiyou Kk | Detergent composition |
| ZA774818B (en) * | 1976-08-17 | 1979-03-28 | Colgate Palmolive Co | Disintegrable detergent builder agglomerates |
| US4414130A (en) * | 1976-08-17 | 1983-11-08 | Colgate Palmolive Company | Readily disintegrable agglomerates of insoluble detergent builders and detergent compositions containing them |
| FR2401987A1 (fr) * | 1977-08-31 | 1979-03-30 | Colgate Palmolive Co | Agglomerats d'auxiliaire de detergence aisement desintegrables et compositions en contenant |
| JPS5512120A (en) * | 1978-07-10 | 1980-01-28 | Asahi Denka Kogyo Kk | Cloth cleaning material |
| DE2912486A1 (de) * | 1979-03-29 | 1980-10-09 | Henkel Kgaa | Verfahren zum reinigen von kaltwasserloeslichen celluloseethern und verwendung der gereinigten produkte, insbesondere in wasch- und reinigungsmitteln |
| GB2051117B (en) * | 1979-05-30 | 1983-05-18 | Unilever Ltd | Reducing friability of detergent powders |
| US4314953A (en) | 1980-06-13 | 1982-02-09 | Lever Brothers Company | Process for reducing friability of detergent powders |
| EP0050015A3 (en) * | 1980-10-14 | 1982-06-09 | Yuken Industries Co. Ltd. | Cleaning composition |
| US4379080A (en) * | 1981-04-22 | 1983-04-05 | The Procter & Gamble Company | Granular detergent compositions containing film-forming polymers |
| PH18527A (en) * | 1982-12-17 | 1985-08-02 | Unilever Nv | Detergent composition for washing fabric |
| DE3301577A1 (de) * | 1983-01-19 | 1984-07-19 | Henkel KGaA, 4000 Düsseldorf | Wasch- und reinigungsmittel |
| US4536319A (en) * | 1983-10-04 | 1985-08-20 | The Procter & Gamble Company | Compositions comprising alkylpolysaccharide detergent surfactant |
| GB8415302D0 (en) * | 1984-06-15 | 1984-07-18 | Unilever Plc | Fabric washing process |
| GB2174712B (en) * | 1985-05-10 | 1988-10-19 | Unilever Plc | Detergent granules |
-
1985
- 1985-09-12 GB GB858522621A patent/GB8522621D0/en active Pending
-
1986
- 1986-09-05 CA CA000517637A patent/CA1275224C/en not_active Expired - Fee Related
- 1986-09-08 US US06/904,743 patent/US4755318A/en not_active Expired - Fee Related
- 1986-09-08 KR KR1019860007487A patent/KR870003188A/ko not_active Withdrawn
- 1986-09-08 AU AU62494/86A patent/AU591520B2/en not_active Ceased
- 1986-09-09 BR BR8604308A patent/BR8604308A/pt not_active IP Right Cessation
- 1986-09-09 IN IN253/BOM/86A patent/IN165359B/en unknown
- 1986-09-10 GB GB8621846A patent/GB2180254B/en not_active Expired - Fee Related
- 1986-09-10 DE DE8686306979T patent/DE3682246D1/de not_active Expired - Fee Related
- 1986-09-10 EP EP86306979A patent/EP0215637B2/en not_active Expired - Lifetime
- 1986-09-11 JP JP61214994A patent/JPH0637637B2/ja not_active Expired - Lifetime
- 1986-09-11 ZA ZA866927A patent/ZA866927B/xx unknown
- 1986-09-11 ES ES8601826A patent/ES2002322A6/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| EP0215637B1 (en) | 1991-10-30 |
| GB2180254B (en) | 1990-01-24 |
| IN165359B (ref) | 1989-09-23 |
| GB8522621D0 (en) | 1985-10-16 |
| DE3682246D1 (de) | 1991-12-05 |
| ZA866927B (en) | 1988-05-25 |
| KR870003188A (ko) | 1987-04-15 |
| JPH0637637B2 (ja) | 1994-05-18 |
| GB8621846D0 (en) | 1986-10-15 |
| ES2002322A6 (es) | 1988-08-01 |
| EP0215637A2 (en) | 1987-03-25 |
| JPS6262900A (ja) | 1987-03-19 |
| EP0215637B2 (en) | 1994-10-05 |
| AU591520B2 (en) | 1989-12-07 |
| GB2180254A (en) | 1987-03-25 |
| US4755318A (en) | 1988-07-05 |
| BR8604308A (pt) | 1987-05-05 |
| EP0215637A3 (en) | 1988-09-14 |
| AU6249486A (en) | 1987-03-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKLA | Lapsed |