CA1081880A - Process and device for the manufacture of polymer dispersions with low monomer content - Google Patents

Process and device for the manufacture of polymer dispersions with low monomer content

Info

Publication number
CA1081880A
CA1081880A CA232,194A CA232194A CA1081880A CA 1081880 A CA1081880 A CA 1081880A CA 232194 A CA232194 A CA 232194A CA 1081880 A CA1081880 A CA 1081880A
Authority
CA
Canada
Prior art keywords
vessel
dispersion
wall
spray
outlet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA232,194A
Other languages
English (en)
French (fr)
Inventor
Franz Botsch
Christoph Heinze
Horst Wolff
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Application granted granted Critical
Publication of CA1081880A publication Critical patent/CA1081880A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/001—Removal of residual monomers by physical means
    • C08F6/003—Removal of residual monomers by physical means from polymer solutions, suspensions, dispersions or emulsions without recovery of the polymer therefrom
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/06—Flash distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/343—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances the substance being a gas
    • B01D3/346—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances the substance being a gas the gas being used for removing vapours, e.g. transport gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/02—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor of the thin-film type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Polymerisation Methods In General (AREA)
CA232,194A 1974-07-25 1975-07-24 Process and device for the manufacture of polymer dispersions with low monomer content Expired CA1081880A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE2435704A DE2435704C3 (de) 1974-07-25 1974-07-25 Verfahren und Vorrichtung zur kontinuierlichen Entfernung von Restgehalten an Monomeren aus wäßrigen Dispersionen von Polymerisaten des Vinylchlorids
DEP2435704.8 1974-07-25

Publications (1)

Publication Number Publication Date
CA1081880A true CA1081880A (en) 1980-07-15

Family

ID=5921434

Family Applications (1)

Application Number Title Priority Date Filing Date
CA232,194A Expired CA1081880A (en) 1974-07-25 1975-07-24 Process and device for the manufacture of polymer dispersions with low monomer content

Country Status (15)

Country Link
JP (1) JPS5137175A (xx)
AT (1) AT341772B (xx)
BE (1) BE831744A (xx)
CA (1) CA1081880A (xx)
CH (1) CH614962A5 (xx)
DE (1) DE2435704C3 (xx)
ES (1) ES439556A1 (xx)
FR (1) FR2279766A1 (xx)
GB (1) GB1508813A (xx)
HU (1) HU175479B (xx)
IT (1) IT1040006B (xx)
NL (1) NL168848C (xx)
SE (1) SE420734B (xx)
YU (2) YU39029B (xx)
ZA (1) ZA754769B (xx)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10272354B2 (en) 2014-10-16 2019-04-30 Rvt Process Equipment Gmbh Liquid distributor of a process-technology column

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL7607736A (nl) * 1974-07-25 1977-01-20 Hoechst Ag Werkwijze en inrichting voor het bereiden van polymeerdispersies met een laag monomeerge- halte.
JPS5128890A (ja) * 1974-09-04 1976-03-11 Mitsui Toatsu Chemicals Mihannoenkabinirumonomaa no jokyohoho
JPS5147075A (en) * 1974-10-19 1976-04-22 Shinetsu Chemical Co Jugoshuryogono mihannotanryotaijokyohoho
JPS51127187A (en) * 1975-04-26 1976-11-05 Kureha Chem Ind Co Ltd A process and an apparatus for recovering monomers
JPS52147689A (en) * 1976-06-02 1977-12-08 Mitsui Toatsu Chem Inc Continuous removal of unreacted vinyl chloride monometer
DE2701147C2 (de) * 1977-01-13 1987-01-02 Wacker-Chemie GmbH, 8000 München Verfahren zur Herstellung von Vinylchlorid-Copolymerisaten mit niedrigem Restmonomergehalt
DE2832972A1 (de) * 1978-07-27 1980-02-07 Wacker Chemie Gmbh Verfahren zur druck- und restentgasung eines pvc-wasser-gemisches im polymerisationsautoklaven bei hoechstmoeglichem abscheidegrad des uebertriebs in einem nachgeschalteten abscheider und rueckfuehrung des uebertriebs zur restentgasung in den polymerisationsautoklaven
IT1121511B (it) * 1979-05-28 1986-04-02 Montedison Spa Procedimento per l'estrazione del cloruro di vinile monomero dai lattici di cloruro di polivinile ed apparecchiatura per la sua realizzazione
GB2247415A (en) * 1990-08-29 1992-03-04 Shell Int Research Discharge device for reducing foam
DE19517680C2 (de) * 1995-05-13 1997-06-12 Buna Sow Leuna Olefinverb Gmbh Verfahren zur Reduzierung der Schaumentwicklung
NZ511502A (en) * 2001-05-04 2002-03-01 Wen Sen Shih Two-chamber water distillation apparatus
DE102011119341A1 (de) 2011-11-25 2013-05-29 Heraeus Quarzglas Gmbh & Co. Kg Verfahren zur Herstellung von synthetischem Quarzglas nach der Sootmethode
DE102011119374A1 (de) 2011-11-25 2013-05-29 Heraeus Quarzglas Gmbh & Co. Kg Verfahren zur Herstellung von synthetischem Quarzglas
DE102011119373A1 (de) 2011-11-25 2013-05-29 Heraeus Quarzglas Gmbh & Co. Kg Verfahren zur Herstellung von synthetischem Quarzglas
DE102011119339A1 (de) 2011-11-25 2013-05-29 Heraeus Quarzglas Gmbh & Co. Kg Zerstäubungsverfahren zur Herstellung von synthetischem Quarzglas
DE102013209673B3 (de) * 2013-05-24 2014-05-22 Heraeus Quarzglas Gmbh & Co. Kg Verfahren und Verdampfer zur Herstellung von synthetischem Quarzglas
WO2020241252A1 (ja) * 2019-05-31 2020-12-03 昭和電工株式会社 精製クロロプレン系重合体ラテックスの製造方法
WO2020241251A1 (ja) 2019-05-31 2020-12-03 昭和電工株式会社 クロロプレン系重合体ラテックスの製造方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1799467A (en) * 1927-03-07 1931-04-07 Thomas B Jarvies Vapor-heating system
NL79746C (xx) * 1953-11-06
GB1090976A (en) * 1964-02-12 1967-11-15 Dunlop Rubber Co Improvements in or relating to volatilization of residual liquid monomers
DE1495177A1 (de) * 1964-05-05 1969-03-13 Basf Ag Verfahren und Vorrichtung zum kontinuierlichen Entfernen fluechtiger Anteile aus Polyamiden
BE709965A (xx) * 1967-01-27 1968-05-30
JPS546269B1 (xx) * 1970-12-18 1979-03-27
DE2130616A1 (de) * 1971-06-21 1972-12-28 Franz Froitzheim Verfahren zum Verdampfen von Fluessigkeiten
DE2259740C3 (de) * 1972-12-04 1981-10-08 Siemens AG, 1000 Berlin und 8000 München Vorrichtung zum Entgasen von Flüssigkeiten

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10272354B2 (en) 2014-10-16 2019-04-30 Rvt Process Equipment Gmbh Liquid distributor of a process-technology column

Also Published As

Publication number Publication date
GB1508813A (en) 1978-04-26
NL7508630A (nl) 1976-01-27
AT341772B (de) 1978-02-27
ES439556A1 (es) 1977-02-16
SE420734B (sv) 1981-10-26
SE7508274L (sv) 1976-01-26
DE2435704B2 (de) 1979-09-27
FR2279766A1 (fr) 1976-02-20
HU175479B (hu) 1980-08-28
CH614962A5 (en) 1979-12-28
YU188875A (en) 1982-05-31
FR2279766B1 (xx) 1980-07-25
YU171981A (en) 1983-09-30
IT1040006B (it) 1979-12-20
ZA754769B (en) 1976-08-25
DE2435704C3 (de) 1987-06-19
NL168848B (nl) 1981-12-16
NL168848C (nl) 1984-05-16
BE831744A (fr) 1976-01-26
DE2435704A1 (de) 1976-02-05
YU39029B (en) 1984-02-29
ATA572175A (de) 1977-06-15
YU41460B (en) 1987-06-30
JPS5137175A (xx) 1976-03-29

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Legal Events

Date Code Title Description
MKEX Expiry