BR112021022558A2 - Método para produzir uma zeólita - Google Patents

Método para produzir uma zeólita

Info

Publication number
BR112021022558A2
BR112021022558A2 BR112021022558A BR112021022558A BR112021022558A2 BR 112021022558 A2 BR112021022558 A2 BR 112021022558A2 BR 112021022558 A BR112021022558 A BR 112021022558A BR 112021022558 A BR112021022558 A BR 112021022558A BR 112021022558 A2 BR112021022558 A2 BR 112021022558A2
Authority
BR
Brazil
Prior art keywords
ammonium
zeolite
type
producing
contact
Prior art date
Application number
BR112021022558A
Other languages
English (en)
Inventor
Akihiro Kanno
Junki Tomita
Katsuhiko Hayashi
Takahiro Kogawa
Yuichi Senoo
Original Assignee
Mitsui Mining & Smelting Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Mining & Smelting Co Ltd filed Critical Mitsui Mining & Smelting Co Ltd
Publication of BR112021022558A2 publication Critical patent/BR112021022558A2/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/18—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the mordenite type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/26—Mordenite type
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/16—After treatment, characterised by the effect to be obtained to increase the Si/Al ratio; Dealumination
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/38—Base treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)

Abstract

método para produzir uma zeólita. um método para produzir uma zeólita com si/al melhorado de acordo com a presente invenção inclui as etapas de: submeter uma zeólita sintetizada sem usar um agente orgânico direcionador de estrutura para troca iônica, assim obtendo uma zeólita de tipo sódio, de tipo próton, ou de tipo amônio; e colocar a zeólita submetida à troca iônica em contato com uma solução de sal de amônio, assim desaluminizando a zeólita. é preferível que o sal de amônio seja qualquer um dentre oxalato de amônio, fluoreto de amônio, fluorossilicato de amônio, fluoroborato de amônio, fluorofosfato de amônio, fluorotitanato de amônio e fluorozirconato de amônio. também é preferível que a zeólita após troca iônica seja exposta a vapor d?água, sendo, então, colocada em contato com a solução de sal de amônio.
BR112021022558A 2019-07-03 2020-06-29 Método para produzir uma zeólita BR112021022558A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2019124817 2019-07-03
PCT/JP2020/025524 WO2021002324A1 (ja) 2019-07-03 2020-06-29 ゼオライトの製造方法

Publications (1)

Publication Number Publication Date
BR112021022558A2 true BR112021022558A2 (pt) 2022-01-11

Family

ID=74100610

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112021022558A BR112021022558A2 (pt) 2019-07-03 2020-06-29 Método para produzir uma zeólita

Country Status (6)

Country Link
US (1) US20220212941A1 (pt)
EP (1) EP3995450A4 (pt)
JP (1) JPWO2021002324A1 (pt)
CN (1) CN113950460A (pt)
BR (1) BR112021022558A2 (pt)
WO (1) WO2021002324A1 (pt)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT201900022509A1 (it) * 2019-11-29 2021-05-29 Getters Spa Imballaggio alimentare per il controllo o la rimozione di ammine

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0082211B2 (en) * 1981-12-20 1993-07-28 Union Carbide Corporation Silicon substituted zeolite compositions and process for preparing same
JPS58110420A (ja) * 1981-12-21 1983-07-01 ユニオン・カ−バイド・コ−ポレ−シヨン 珪素置換ゼオライト組成物及びその調製方法
JPS58217425A (ja) 1982-06-11 1983-12-17 Toyo Soda Mfg Co Ltd モルデナイトの製造法
JP4904417B2 (ja) 2009-07-27 2012-03-28 日本化学工業株式会社 ベータ型ゼオライト及びその製造方法
JP5504446B2 (ja) * 2010-05-14 2014-05-28 国立大学法人大阪大学 疎水性ゼオライトの製造方法及びその方法で得られた疎水性ゼオライト
CN104203824B (zh) * 2011-11-25 2017-10-17 UniZeo株式会社 沸石及所述沸石的制造方法以及石蜡的接触分解催化剂
JP5988743B2 (ja) 2012-07-18 2016-09-07 ユニゼオ株式会社 Ｆｅ（ＩＩ）置換ベータ型ゼオライト、それを含むガス吸着剤及びその製造方法、並びに一酸化窒素及びハイドロカーボンの除去方法
CN102992343A (zh) * 2012-12-09 2013-03-27 浙江大学 无有机模板固相法合成沸石分子筛的方法
CN104588073B (zh) * 2013-11-03 2017-01-25 中国石油化工股份有限公司 一种加氢脱芳烃催化剂及其制备方法
CN105621431B (zh) * 2014-11-03 2017-12-22 中国石油化工股份有限公司 改性β分子筛及其制备方法

Also Published As

Publication number Publication date
EP3995450A1 (en) 2022-05-11
WO2021002324A1 (ja) 2021-01-07
EP3995450A4 (en) 2022-08-17
US20220212941A1 (en) 2022-07-07
JPWO2021002324A1 (pt) 2021-01-07
CN113950460A (zh) 2022-01-18

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Legal Events

Date Code Title Description
B11A Dismissal acc. art.33 of ipl - examination not requested within 36 months of filing
B11Y Definitive dismissal - extension of time limit for request of examination expired [chapter 11.1.1 patent gazette]