BR112019023942A2 - processo para preparar compostos mono-hidróxi - Google Patents

processo para preparar compostos mono-hidróxi Download PDF

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Publication number
BR112019023942A2
BR112019023942A2 BR112019023942A BR112019023942A BR112019023942A2 BR 112019023942 A2 BR112019023942 A2 BR 112019023942A2 BR 112019023942 A BR112019023942 A BR 112019023942A BR 112019023942 A BR112019023942 A BR 112019023942A BR 112019023942 A2 BR112019023942 A2 BR 112019023942A2
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BR
Brazil
Prior art keywords
hydrogenation
compounds
contained
monohydroxy
monohydroxy compounds
Prior art date
Application number
BR112019023942A
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English (en)
Inventor
Lange De Oliveira Armin
Breitscheidel Boris
Papp Rainer
Zuend Stephan
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BR112019023942A2 publication Critical patent/BR112019023942A2/pt

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/72—Copper
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
    • C07C29/149—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/02—Monohydroxylic acyclic alcohols
    • C07C31/12—Monohydroxylic acyclic alcohols containing four carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/49—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide
    • C07C45/50—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide by oxo-reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

a invenção refere-se a um método para produzir compostos mono-hidróxi-c4 a c13 a partir de uma fração de fundo que é obtida durante a destilação de uma mistura bruta de oxoaldeídos c4- a c13- a partir da hidroformilação catalisada por cobalto ou ródio, ou durante a destilação de uma mistura bruta de oxoálcoois c4- a c13-. o método é distinguido em que a fração de fundo, na presença de hidrogênio, é colocada em contato com um catalisador contendo óxido de cobre e óxido de alumínio a uma temperatura de 150°c a 300°c e uma pressão de 20 bar a 300 bar, o produto obtido de hidrogenação bruto é destilado, e a quantidade de compostos mono-hidróxi c4 a c13 que está contida no produto de hidrogenação bruto após a hidrogenação é maior do que a quantidade de compostos mono-hidróxi c4 a c13 que resultam estequiometricamente a partir da hidrogenação dos compostos éster e aldeído contidos na fração de fundo, incluindo os compostos mono-hidróxi c4 a c13 contidos na fração de fundo antes da hidrogenação.
BR112019023942A 2017-05-16 2018-05-14 processo para preparar compostos mono-hidróxi BR112019023942A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP17171250 2017-05-16
PCT/EP2018/062328 WO2018210720A1 (de) 2017-05-16 2018-05-14 HYDROFORMYLIERUNGSVERFAHREN DIENEN DER GROßTECHNISCHEN HERSTELLUNG VON ALDEHYDEN UND/ODER ALKOHOLEN

Publications (1)

Publication Number Publication Date
BR112019023942A2 true BR112019023942A2 (pt) 2020-06-09

Family

ID=58709882

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112019023942A BR112019023942A2 (pt) 2017-05-16 2018-05-14 processo para preparar compostos mono-hidróxi

Country Status (8)

Country Link
US (1) US11014863B2 (pt)
EP (1) EP3625199B1 (pt)
KR (1) KR102641656B1 (pt)
CN (1) CN110637003B (pt)
BR (1) BR112019023942A2 (pt)
PL (1) PL3625199T3 (pt)
TW (1) TWI780153B (pt)
WO (1) WO2018210720A1 (pt)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3770145A1 (en) 2019-07-24 2021-01-27 Basf Se A process for the continuous production of either acrolein or acrylic acid as the target product from propene
WO2021247177A1 (en) * 2020-06-05 2021-12-09 SCION Holdings LLC Alcohols production
WO2021247516A1 (en) 2020-06-05 2021-12-09 SCION Holdings LLC Branched alcohols
US20220194886A1 (en) 2020-12-17 2022-06-23 SCION Holdings LLC Branched Products
CN112844398B (zh) * 2021-02-10 2023-05-30 中国海洋石油集团有限公司 一种用于碳四叠合产物加氢的催化剂及其制备方法

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US3501537A (en) * 1964-04-01 1970-03-17 Eastman Kodak Co Process for separating high-boilers of the oxo process
US3935285A (en) * 1968-12-27 1976-01-27 Ruhrchemie Ag Recovery of alcohols from esters formed during an oxo-synthesis
DE2445303C3 (de) 1974-09-21 1979-04-05 Basf Ag, 6700 Ludwigshafen Basisches, zur Herstellung eines Kupfer enthaltenden Katalysators geeignetes Carbonat
US4148830A (en) 1975-03-07 1979-04-10 Union Carbide Corporation Hydroformylation of olefins
DE2628987C3 (de) 1976-06-28 1981-10-22 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von C↓3↓-C↓5↓-Alkanolen
DE2740216C2 (de) 1977-09-07 1979-10-11 Chemische Werke Huels Ag, 4370 Marl Verfahren zur Aufarbeitung von Destillationsruckständen der Propen-Hydroformylierung
ATE13874T1 (de) 1981-08-20 1985-07-15 Davy Mckee London Hydrierungsverfahren.
US5004845A (en) * 1981-08-20 1991-04-02 Davy Mckee (London) Limited Hydrogenation of aldehydes
DE3228881C2 (de) 1982-08-03 1985-06-13 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von C↓3↓-C↓5↓-Alkoholen
GB9324753D0 (en) * 1993-12-02 1994-01-19 Davy Mckee London Process
DE19530698A1 (de) 1995-08-21 1997-02-27 Basf Ag Verfahren zur Aufarbeitung eines flüssigen Hydroformylierungsaustrags
CA2250132A1 (en) 1996-03-21 1997-09-25 Mallinckrodt Chemical, Inc. Preparation and use of non-chrome catalysts for cu/cr catalyst applications
DE19739773A1 (de) 1997-09-10 1999-03-11 Basf Ag Verfahren und Katalysator zur Dampfreformierung von Methanol
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Also Published As

Publication number Publication date
TWI780153B (zh) 2022-10-11
EP3625199A1 (de) 2020-03-25
US11014863B2 (en) 2021-05-25
WO2018210720A1 (de) 2018-11-22
EP3625199B1 (de) 2021-09-22
CN110637003A (zh) 2019-12-31
TW201900587A (zh) 2019-01-01
KR20200007910A (ko) 2020-01-22
CN110637003B (zh) 2022-11-04
KR102641656B1 (ko) 2024-02-29
US20210078925A1 (en) 2021-03-18
PL3625199T3 (pl) 2022-02-07

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B11A Dismissal acc. art.33 of ipl - examination not requested within 36 months of filing
B350 Update of information on the portal [chapter 15.35 patent gazette]
B11Y Definitive dismissal - extension of time limit for request of examination expired [chapter 11.1.1 patent gazette]