BR112016001388B8 - processo contínuo e uso de dihidrogenofosfato de potássio - Google Patents
processo contínuo e uso de dihidrogenofosfato de potássioInfo
- Publication number
- BR112016001388B8 BR112016001388B8 BR112016001388A BR112016001388A BR112016001388B8 BR 112016001388 B8 BR112016001388 B8 BR 112016001388B8 BR 112016001388 A BR112016001388 A BR 112016001388A BR 112016001388 A BR112016001388 A BR 112016001388A BR 112016001388 B8 BR112016001388 B8 BR 112016001388B8
- Authority
- BR
- Brazil
- Prior art keywords
- liquid feed
- feed stream
- continuous process
- dihydrogen phosphate
- potassium dihydrogen
- Prior art date
Links
- 238000010924 continuous production Methods 0.000 title abstract 2
- 229910000402 monopotassium phosphate Inorganic materials 0.000 title abstract 2
- 235000019796 monopotassium phosphate Nutrition 0.000 title abstract 2
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 title abstract 2
- 239000007788 liquid Substances 0.000 abstract 5
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 abstract 3
- 238000006735 epoxidation reaction Methods 0.000 abstract 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 abstract 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 abstract 2
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 abstract 2
- ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 abstract 2
- 229910000396 dipotassium phosphate Inorganic materials 0.000 abstract 2
- 235000019797 dipotassium phosphate Nutrition 0.000 abstract 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 1
- 229910021536 Zeolite Inorganic materials 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000001294 propane Substances 0.000 abstract 1
- 229910052719 titanium Inorganic materials 0.000 abstract 1
- 239000010936 titanium Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 239000010457 zeolite Substances 0.000 abstract 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/06—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of zinc, cadmium or mercury
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/14—Phosphorus; Compounds thereof
- B01J27/16—Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr
- B01J27/18—Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr with metals other than Al or Zr
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
- B01J29/7049—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing rare earth elements, titanium, zirconium, hafnium, zinc, cadmium, mercury, gallium, indium, thallium, tin or lead
- B01J29/7088—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/19—Catalysts containing parts with different compositions
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
- B01J37/0027—Powdering
- B01J37/0045—Drying a slurry, e.g. spray drying
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/08—Heat treatment
- B01J37/10—Heat treatment in the presence of water, e.g. steam
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/36—Use of additives, e.g. for stabilisation
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/10—After treatment, characterised by the effect to be obtained
- B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
- B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/30—After treatment, characterised by the means used
- B01J2229/42—Addition of matrix or binder particles
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Epoxy Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
um processo para o preparo de óxido de propileno um processo contínuo para a preparação de óxido de propileno, compreendendo (i) prover uma corrente de alimentação de líquido compreendendo propeno, peróxido de hidrogênio, acetonitrila, água, dihidrogenofosfato de potássio dissolvido e, opcionalmente, propano; (ii) passar a corrente de alimentação de líquido provida em (i) em um reator de epoxidação compreendendo um catalisador, compreendendo um zeólito de titânio do tipo estrutura mww e sujeitar a corrente de alimentação de líquido a condições de reação de epoxidação; (iii) remover uma corrente de efluentes do reator a epoxidação; em que a concentração do hidrogenofosfato de potássio dissolvido na corrente de alimentação de líquido é pelo menos 10% do limite de solubilidade do hidrogenofosfato de potássio na corrente de alimentação de líquido.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP13177903.5 | 2013-07-24 | ||
EP13177903 | 2013-07-24 | ||
PCT/EP2014/065249 WO2015010992A1 (en) | 2013-07-24 | 2014-07-16 | A process for the preparation of propylene oxide |
Publications (3)
Publication Number | Publication Date |
---|---|
BR112016001388A2 BR112016001388A2 (pt) | 2019-12-17 |
BR112016001388B1 BR112016001388B1 (pt) | 2020-12-01 |
BR112016001388B8 true BR112016001388B8 (pt) | 2020-12-22 |
Family
ID=48832824
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112016001388A BR112016001388B8 (pt) | 2013-07-24 | 2014-07-16 | processo contínuo e uso de dihidrogenofosfato de potássio |
Country Status (10)
Country | Link |
---|---|
US (1) | US9688648B2 (pt) |
EP (1) | EP3024580B1 (pt) |
KR (1) | KR102302531B1 (pt) |
CN (1) | CN105813741B (pt) |
BR (1) | BR112016001388B8 (pt) |
ES (1) | ES2687470T3 (pt) |
MX (1) | MX2016001027A (pt) |
RU (1) | RU2673676C2 (pt) |
SG (1) | SG11201600519XA (pt) |
WO (1) | WO2015010992A1 (pt) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SG10201803770YA (en) | 2013-07-24 | 2018-06-28 | Basf Se | A process for preparing propylene oxide |
EP3206756B1 (de) | 2014-10-14 | 2018-09-19 | Basf Se | Verwendung von hexadeca-8,15-dienal als aromachemikalie |
CN107848822B (zh) | 2015-02-12 | 2021-03-02 | 巴斯夫欧洲公司 | 用于制备具有bea骨架结构的脱铝沸石材料的方法 |
CN107646032B (zh) | 2015-04-09 | 2019-07-12 | 利安德化学技术有限公司 | 在丙烯环氧化中改进的催化剂性能 |
US9643943B2 (en) | 2015-04-09 | 2017-05-09 | Lyondell Chemical Technology, L.P. | Process for forming propylene oxide from oxidation of methyl benzyl alcohol |
WO2016177814A1 (en) | 2015-05-04 | 2016-11-10 | Basf Se | Process for the preparation of melonal |
JP2018522007A (ja) | 2015-07-15 | 2018-08-09 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | アリールプロペンの調製方法 |
CN107848930A (zh) | 2015-07-15 | 2018-03-27 | 巴斯夫欧洲公司 | 制备芳基丙烯的方法 |
RU2732326C2 (ru) | 2015-07-22 | 2020-09-15 | Басф Се | Способ получения фуран-2,5-дикарбоновой кислоты |
CN113461474A (zh) * | 2021-06-30 | 2021-10-01 | 中国石油化工股份有限公司 | 一种丙烷工业化连续制备环氧丙烷的系统及方法 |
Family Cites Families (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3936854A1 (de) | 1989-11-06 | 1991-05-08 | Basf Ag | Verfahren zur herstellung von methylformiat |
US5646314A (en) * | 1994-11-16 | 1997-07-08 | Arco Chemical Technology, L.P. | Process for titanium silicalite-catalyzed epoxidation |
DE19936547A1 (de) * | 1999-08-04 | 2001-02-15 | Basf Ag | Verfahren zur Umsetzung einer organischen Verbindung mit einem Hydroperoxid |
US6114551A (en) | 1999-10-04 | 2000-09-05 | Mobil Oil Corporation | Olefin epoxidation catalysts |
EP1122249A1 (fr) | 2000-02-02 | 2001-08-08 | SOLVAY (Société Anonyme) | Procédé de fabrication d'un oxiranne |
DE10015246A1 (de) * | 2000-03-28 | 2001-10-04 | Basf Ag | Verfahren zur Umsetzung einer organischen Verbindung mit einem Hydroperoxid |
DE10044787A1 (de) | 2000-09-11 | 2002-04-04 | Basf Ag | Verfahren zur Herstellung eines Epoxides |
US6498259B1 (en) * | 2001-10-19 | 2002-12-24 | Arco Chemical Technology L.P. | Direct epoxidation process using a mixed catalyst system |
DE10320635A1 (de) | 2003-05-08 | 2004-11-18 | Basf Ag | Verfahren zur Herstellung von Propylenoxid |
US7273826B2 (en) * | 2005-07-26 | 2007-09-25 | Lyondell Chemical Technology, L.P. | Epoxidation catalyst |
BRPI0813576A2 (pt) | 2007-07-10 | 2014-12-23 | Sumitomo Chemical Co | Método para a produção de óxido de propileno |
MY156574A (en) | 2009-07-16 | 2016-03-15 | Basf Se | Method for the separation of acetonitrile from water |
JP2011246423A (ja) | 2010-05-31 | 2011-12-08 | Sumitomo Chemical Co Ltd | オレフィンオキサイドの製造方法 |
JP2012116758A (ja) * | 2010-11-29 | 2012-06-21 | Sumitomo Chemical Co Ltd | オレフィンオキサイドの製造方法 |
US8785670B2 (en) * | 2010-12-07 | 2014-07-22 | Basf Se | Process for the production of propylene oxide |
JP2012236177A (ja) * | 2011-05-13 | 2012-12-06 | Sumitomo Chemical Co Ltd | チタノシリケート含有触媒の製造方法 |
CN102558100A (zh) * | 2012-01-20 | 2012-07-11 | 中国天辰工程有限公司 | 以钛硅分子筛为催化剂催化丙烯环氧化反应的方法 |
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2014
- 2014-07-16 BR BR112016001388A patent/BR112016001388B8/pt active IP Right Grant
- 2014-07-16 WO PCT/EP2014/065249 patent/WO2015010992A1/en active Application Filing
- 2014-07-16 RU RU2016105803A patent/RU2673676C2/ru active
- 2014-07-16 ES ES14739190.8T patent/ES2687470T3/es active Active
- 2014-07-16 MX MX2016001027A patent/MX2016001027A/es active IP Right Grant
- 2014-07-16 EP EP14739190.8A patent/EP3024580B1/en active Active
- 2014-07-16 CN CN201480052333.7A patent/CN105813741B/zh active Active
- 2014-07-16 SG SG11201600519XA patent/SG11201600519XA/en unknown
- 2014-07-16 KR KR1020167004186A patent/KR102302531B1/ko active IP Right Grant
- 2014-07-16 US US14/906,852 patent/US9688648B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
SG11201600519XA (en) | 2016-02-26 |
BR112016001388B1 (pt) | 2020-12-01 |
US20160185741A1 (en) | 2016-06-30 |
RU2016105803A3 (pt) | 2018-04-27 |
ES2687470T3 (es) | 2018-10-25 |
CN105813741B (zh) | 2019-02-19 |
MX2016001027A (es) | 2016-08-03 |
CN105813741A (zh) | 2016-07-27 |
RU2016105803A (ru) | 2017-08-28 |
RU2673676C2 (ru) | 2018-11-29 |
EP3024580A1 (en) | 2016-06-01 |
US9688648B2 (en) | 2017-06-27 |
BR112016001388A2 (pt) | 2019-12-17 |
EP3024580B1 (en) | 2018-06-13 |
KR102302531B1 (ko) | 2021-09-16 |
KR20160041939A (ko) | 2016-04-18 |
WO2015010992A1 (en) | 2015-01-29 |
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B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
B06U | Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 16/07/2014, OBSERVADAS AS CONDICOES LEGAIS. |
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