BR112013028830A2 - composição, método para produzir uma composição e artigo - Google Patents
composição, método para produzir uma composição e artigoInfo
- Publication number
- BR112013028830A2 BR112013028830A2 BR112013028830A BR112013028830A BR112013028830A2 BR 112013028830 A2 BR112013028830 A2 BR 112013028830A2 BR 112013028830 A BR112013028830 A BR 112013028830A BR 112013028830 A BR112013028830 A BR 112013028830A BR 112013028830 A2 BR112013028830 A2 BR 112013028830A2
- Authority
- BR
- Brazil
- Prior art keywords
- polymer
- composition
- copolymer
- isocyanate
- molecule
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G81/00—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers
- C08G81/02—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers at least one of the polymers being obtained by reactions involving only carbon-to-carbon unsaturated bonds
- C08G81/024—Block or graft polymers containing sequences of polymers of C08C or C08F and of polymers of C08G
- C08G81/025—Block or graft polymers containing sequences of polymers of C08C or C08F and of polymers of C08G containing polyether sequences
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/2805—Compounds having only one group containing active hydrogen
- C08G18/288—Compounds containing at least one heteroatom other than oxygen or nitrogen
- C08G18/289—Compounds containing at least one heteroatom other than oxygen or nitrogen containing silicon
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
- C08G18/632—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers onto polyethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/71—Monoisocyanates or monoisothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/71—Monoisocyanates or monoisothiocyanates
- C08G18/718—Monoisocyanates or monoisothiocyanates containing silicon
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7614—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
- C08G18/7621—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring being toluene diisocyanate including isomer mixtures
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
- C08L75/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/10—Materials in mouldable or extrudable form for sealing or packing joints or covers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Materials Engineering (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Polyurethanes Or Polyureas (AREA)
- Sealing Material Composition (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
resumo “composição, método para produzir uma composição e artigo” é provido um polímero terminado por silano reticulável carregado com copolímero tendo pelo menos um grupo silila reticulável em cada molécula. o polímero terminado por silano reticulável carregado com copolímero é o produto de reação de um poliol carregado com copolímero e um polímero hidrossililado capeado com isocianato. o polímero hidrossililado capeado com isocianato é o produto de reação de pelo menos um isocianato e um polímero hidrossililado. o polímero hidrossililado é o produto de reação de um polímero tendo pelo menos um grupo insaturado e pelo menos um grupo hidroxila alcoólico em cada molécula e um composto tendo uma ligação hidrogênio-silício e um grupo silila reticulável em cada molécula. os polímeros terminados por silano reticuláveis carregados com copolímero exibem propriedades de módulo e carga de ruptura melhorados enquanto que mantendo propriedades de alongamento. 1
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161503501P | 2011-06-30 | 2011-06-30 | |
PCT/US2012/042385 WO2013003053A1 (en) | 2011-06-30 | 2012-06-14 | Silane terminated polymer for coating, adhesives, sealant and elastomer applications |
Publications (1)
Publication Number | Publication Date |
---|---|
BR112013028830A2 true BR112013028830A2 (pt) | 2017-01-31 |
Family
ID=46384492
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112013028830A BR112013028830A2 (pt) | 2011-06-30 | 2012-06-14 | composição, método para produzir uma composição e artigo |
Country Status (10)
Country | Link |
---|---|
US (1) | US8907014B2 (pt) |
EP (1) | EP2726524B1 (pt) |
JP (2) | JP2014520911A (pt) |
KR (1) | KR101951495B1 (pt) |
CN (1) | CN103635499B (pt) |
BR (1) | BR112013028830A2 (pt) |
DK (1) | DK2726524T3 (pt) |
ES (1) | ES2546261T3 (pt) |
RU (1) | RU2014102979A (pt) |
WO (1) | WO2013003053A1 (pt) |
Families Citing this family (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2955209A1 (de) | 2014-06-11 | 2015-12-16 | HILTI Aktiengesellschaft | Dämmschichtbildende Zusammensetzung und deren Verwendung |
EP2957589A1 (de) | 2014-06-18 | 2015-12-23 | HILTI Aktiengesellschaft | Brandschutz-Zusammensetzung und deren Verwendung |
EP3095809A1 (de) | 2015-05-21 | 2016-11-23 | HILTI Aktiengesellschaft | Schäumbare, dämmschichtbildende mehrkomponenten-zusammensetzung und deren verwendung |
WO2016205405A1 (en) * | 2015-06-19 | 2016-12-22 | Ndsu Research Foundation | Coordination polymer |
US20180244828A1 (en) * | 2015-09-10 | 2018-08-30 | Dow Global Technologies Llc | Moisture curable systems based on polysilylated polyethers and titanium (iv) catalysts and/or zinc/cyclic amidine catalyst mixtures |
CN105238256B (zh) * | 2015-11-11 | 2017-12-29 | 科顺防水科技股份有限公司 | 一种烯丙基醚改性单组份聚氨酯防水涂料及其制备方法 |
CN106978059B (zh) * | 2017-03-09 | 2020-01-10 | 上海台安实业集团有限公司 | 硅烷封端剂改性双组份聚氨酯防水涂料及其制备方法 |
EP3412736A1 (de) | 2017-06-06 | 2018-12-12 | HILTI Aktiengesellschaft | Brandschutz-zusammensetzung, mehrkomponentensystem und deren verwendung |
CA3068871A1 (en) * | 2017-06-26 | 2019-01-03 | Dow Silicones Corporation | Silicone-polyether copolymer, isocyanate-functional silicone-polyether copolymer formed therewith, silicone-polyether-urethane copolymer, sealants comprising same, and related methods |
CN107419666A (zh) * | 2017-08-08 | 2017-12-01 | 合肥安力电力工程有限公司 | 一种高铁桥梁泄水管的施工工艺 |
CN109666115B (zh) * | 2017-10-16 | 2021-09-07 | 万华化学集团股份有限公司 | 一种氨基硅烷封端改性聚氨酯树脂及其制备方法 |
EP3549987A1 (en) | 2018-04-05 | 2019-10-09 | HILTI Aktiengesellschaft | Airless-sprayable firestop coating composition |
CN110614122B (zh) * | 2018-06-20 | 2023-03-24 | 万华化学集团股份有限公司 | 一种负载型硅氢加成催化剂的制备方法 |
BE1027545B1 (nl) | 2019-09-02 | 2021-03-31 | Fourny Nv | Adhesief en applicator voor het aanbrengen van dit adhesief |
IT201900022356A1 (it) * | 2019-11-28 | 2021-05-28 | Dow Global Technologies Llc | Composizione adesiva |
EP3838962A1 (en) * | 2019-12-20 | 2021-06-23 | Repsol, S.A. | Stable modified polymer polyol dispersions |
EP3945118A1 (en) | 2020-07-28 | 2022-02-02 | Hilti Aktiengesellschaft | Fire-protection coating composition and use thereof |
BE1028534B1 (nl) | 2020-08-07 | 2022-03-08 | Fourny Nv | Applicator voor het aanbrengen van een adhesief |
EP3981842A1 (en) | 2020-10-09 | 2022-04-13 | Hilti Aktiengesellschaft | Fire-protection coating composition and use thereof |
EP4335908A1 (en) | 2022-09-09 | 2024-03-13 | Hilti Aktiengesellschaft | Intumescent composition and use of the intumescent composition to increase char stability of coatings in the event of fire |
EP4335907A1 (en) | 2022-09-09 | 2024-03-13 | Hilti Aktiengesellschaft | Use of alkoxy-functional organic polymers to enhance water resistance of intumescent coatings |
CN116023628B (zh) * | 2023-02-21 | 2023-09-12 | 广州海豚新材料有限公司 | 一种生物基含硅聚氨酯及其制备方法和超纤革 |
Family Cites Families (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3931092A (en) | 1974-04-29 | 1976-01-06 | Basf Wyandotte Corporation | Finely-divided polymeric solids having improved physical properties |
US4521546A (en) | 1981-12-21 | 1985-06-04 | Olin Corporation | Graft copolymers from vinyl monomers and polyurethane oligomers and polyurethanes prepared therefrom |
JPS60133019A (ja) * | 1983-12-20 | 1985-07-16 | Sanyo Chem Ind Ltd | ポリウレタンの製造法 |
US4522976A (en) | 1984-05-17 | 1985-06-11 | Basf Wyandotte Corporation | Graft polymer dispersion in a mixture of low molecular weight polyols and polyether polyols and polyurethane foams prepared therefrom |
JPH05125176A (ja) * | 1991-11-01 | 1993-05-21 | Asahi Glass Co Ltd | ポリエーテル重合体及びその製造方法 |
JP3037579B2 (ja) * | 1995-03-17 | 2000-04-24 | サンスター技研株式会社 | 湿気硬化性ポリマー組成物およびその製造法 |
EP1080126B1 (en) | 1998-04-27 | 2003-10-22 | Essex Specialty Products, Inc. | Method of bonding a window to a substrate using a silane functional adhesive composition |
US6121354A (en) * | 1998-11-19 | 2000-09-19 | Bostik, Inc. | High performance single-component sealant |
EP1299476A2 (en) | 2000-05-15 | 2003-04-09 | The Dow Chemical Company | Polyurethanes containing reinforcing polymers |
TWI315730B (en) | 2001-08-15 | 2009-10-11 | Dow Global Technologies Inc | Process to manufacture polyurethane products |
US10023683B2 (en) * | 2006-06-12 | 2018-07-17 | Evonik Degussa Gmbh | Catalyst compositions for improving polyurethane foam performance |
US20090281206A1 (en) | 2006-07-05 | 2009-11-12 | Dow Global Technologies Inc. | Copolymer polyols and a process for the production thereof |
WO2008018389A1 (fr) * | 2006-08-07 | 2008-02-14 | Mitsui Chemicals Polyurethanes, Inc. | Résine durcissable et composition durcissable |
US20090314656A1 (en) | 2006-08-08 | 2009-12-24 | Takayuki Nakano | Method of purifying water and apparatus therefor |
MX2009010553A (es) | 2008-02-01 | 2009-10-22 | Dow Global Technologies Inc | Polioles de copolimero basados en aceite natural y productos de poliuretano preparados a partir de los mismos. |
DE102008020979A1 (de) * | 2008-04-25 | 2009-10-29 | Henkel Ag & Co. Kgaa | Härtbare Zusammensetzungen enthaltend silylierte Polyurethane |
US8394868B2 (en) * | 2008-06-12 | 2013-03-12 | Dow Global Technologies Llc | Polyol prepolymers of natural oil based polyols |
US8668804B2 (en) * | 2008-08-22 | 2014-03-11 | Dow Global Technologies Llc | Adhesive composition adapted for bonding large mass parts to structures |
EP2576657B1 (en) | 2010-05-27 | 2017-01-18 | Dow Global Technologies LLC | Methods for producing crosslinkable silyl group-containing polyoxyalkylene polymers |
EP2588511B1 (en) * | 2010-06-30 | 2020-03-18 | Dow Global Technologies LLC | Low viscosity silyl-modified polymers |
EP2588510B1 (en) * | 2010-06-30 | 2015-04-15 | Dow Global Technologies LLC | Tin free silyl-terminated polymers |
JP5918230B2 (ja) * | 2010-06-30 | 2016-05-18 | ダウ グローバル テクノロジーズ エルエルシー | シリル末端ポリマー |
-
2012
- 2012-06-14 EP EP12730105.9A patent/EP2726524B1/en active Active
- 2012-06-14 WO PCT/US2012/042385 patent/WO2013003053A1/en active Application Filing
- 2012-06-14 RU RU2014102979/04A patent/RU2014102979A/ru not_active Application Discontinuation
- 2012-06-14 CN CN201280031551.3A patent/CN103635499B/zh not_active Expired - Fee Related
- 2012-06-14 JP JP2014518614A patent/JP2014520911A/ja active Pending
- 2012-06-14 DK DK12730105.9T patent/DK2726524T3/da active
- 2012-06-14 KR KR1020137034321A patent/KR101951495B1/ko active IP Right Grant
- 2012-06-14 ES ES12730105.9T patent/ES2546261T3/es active Active
- 2012-06-14 BR BR112013028830A patent/BR112013028830A2/pt not_active IP Right Cessation
- 2012-06-14 US US14/113,318 patent/US8907014B2/en not_active Expired - Fee Related
-
2017
- 2017-01-12 JP JP2017002999A patent/JP6232509B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
RU2014102979A (ru) | 2015-08-10 |
KR20140039236A (ko) | 2014-04-01 |
US20140309372A1 (en) | 2014-10-16 |
CN103635499A (zh) | 2014-03-12 |
EP2726524A1 (en) | 2014-05-07 |
JP2014520911A (ja) | 2014-08-25 |
EP2726524B1 (en) | 2015-07-22 |
WO2013003053A1 (en) | 2013-01-03 |
JP6232509B2 (ja) | 2017-11-15 |
CN103635499B (zh) | 2015-12-23 |
US8907014B2 (en) | 2014-12-09 |
KR101951495B1 (ko) | 2019-02-22 |
JP2017106022A (ja) | 2017-06-15 |
ES2546261T3 (es) | 2015-09-22 |
DK2726524T3 (da) | 2015-10-05 |
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