BR112013024121A2 - processo para a cristalização de um composto solúvel em água - Google Patents

processo para a cristalização de um composto solúvel em água

Info

Publication number
BR112013024121A2
BR112013024121A2 BR112013024121A BR112013024121A BR112013024121A2 BR 112013024121 A2 BR112013024121 A2 BR 112013024121A2 BR 112013024121 A BR112013024121 A BR 112013024121A BR 112013024121 A BR112013024121 A BR 112013024121A BR 112013024121 A2 BR112013024121 A2 BR 112013024121A2
Authority
BR
Brazil
Prior art keywords
water
soluble compound
solvent
vapor phase
crystallization
Prior art date
Application number
BR112013024121A
Other languages
English (en)
Other versions
BR112013024121B1 (pt
Inventor
Johannes Cornelis Franciscus Van Bon Jeroen
Pieter Marinus Sanders Johan
Elisabeth Bruins Marieke
Original Assignee
Univ Wageningen
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Wageningen filed Critical Univ Wageningen
Publication of BR112013024121A2 publication Critical patent/BR112013024121A2/pt
Publication of BR112013024121B1 publication Critical patent/BR112013024121B1/pt

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
    • F02B—INTERNAL-COMBUSTION PISTON ENGINES; COMBUSTION ENGINES IN GENERAL
    • F02B43/00—Engines characterised by operating on gaseous fuels; Plants including such engines
    • F02B43/10—Engines or plants characterised by use of other specific gases, e.g. acetylene, oxyhydrogen
    • F02B43/12—Methods of operating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
    • B01D9/0054—Use of anti-solvent
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
    • C07H3/04—Disaccharides
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P5/00—Preparation of hydrocarbons or halogenated hydrocarbons
    • C12P5/02—Preparation of hydrocarbons or halogenated hydrocarbons acyclic
    • C12P5/023—Methane
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/06—Ethanol, i.e. non-beverage
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/16—Butanols
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
    • C13B30/02—Crystallisation; Crystallising apparatus
    • C13B30/021—Crystallisation; Crystallising apparatus using chemicals
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
    • C13B30/02—Crystallisation; Crystallising apparatus
    • C13B30/022—Continuous processes, apparatus therefor
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02T—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION
    • Y02T10/00—Road transport of goods or passengers
    • Y02T10/10—Internal combustion engine [ICE] based vehicles
    • Y02T10/30—Use of alternative fuels, e.g. biofuels

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Biotechnology (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Molecular Biology (AREA)
  • Microbiology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Mechanical Engineering (AREA)
  • Combustion & Propulsion (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)

Abstract

processo para a cristalização de um composto solúvel em água a invenção se refere a um processo para a cristalização de um composto solúvel em água a partir de uma solução compreendendo as seguintes etapas; a) fornecer, em um recipiente de cristalização, uma solução do composto solúvel em água em uma mistura de água e um solvente no qual o composto solúvel em água tem uma solubilidade menor do que na água; b) passar a fase de vapor da mistura através de uma zona de sorção contendo um adsorvente de vapor de água para seletivamente adsorver água a partir da fase de vapor para obter uma fase de vapor empobrecida em água e enriquecida no solvente e adsorvente de vapor de água saturado em água; c) enriquecer a mistura no recipiente de cristalização no solvente pela reciclagem de pelo menos parte da fase de vapor empobrecida em água e enriquecida no solvente para o recipiente de cristalização ou retirar a fase de vapor empobrecida em água do processo e adicionar solvente a partir de uma fonte externa para o recipiente de cristalização; d) permitir que cristais sólidos do composto solúvel em água se precipitem a partir da solução no recipiente de cristalização em uma temperatura de cristalização; e e) descarregar os cristais sólidos precipitados do composto solúvel em água a partir do recipiente de cristalização e descarregar uma solução do composto solúvel em água não cristalizado na mistura de água-solvente a partir do recipiente de cristalização. a invenção se refere adicionalmente a um processo para a fabricação de sacarose cristalina a partir do suco de açúcar de palmeira ou biomassa contendo sacarose compreendendo tal processo de cristalização.
BR112013024121A 2011-03-22 2012-03-19 processo para a cristalização de um composto solúvel em água BR112013024121B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NL2006447A NL2006447C2 (en) 2011-03-22 2011-03-22 Process for the crystallisation of a water-soluble compound.
PCT/NL2012/050169 WO2012128624A1 (en) 2011-03-22 2012-03-19 Process for the crystallisation of a water-soluble compound

Publications (2)

Publication Number Publication Date
BR112013024121A2 true BR112013024121A2 (pt) 2017-06-06
BR112013024121B1 BR112013024121B1 (pt) 2019-12-10

Family

ID=45928985

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112013024121A BR112013024121B1 (pt) 2011-03-22 2012-03-19 processo para a cristalização de um composto solúvel em água

Country Status (14)

Country Link
US (2) US9255301B2 (pt)
EP (1) EP2689039B1 (pt)
AU (1) AU2012231892B2 (pt)
BR (1) BR112013024121B1 (pt)
CA (1) CA2830644C (pt)
CO (1) CO6811871A2 (pt)
DK (1) DK2689039T3 (pt)
ES (1) ES2543441T3 (pt)
HR (1) HRP20150561T1 (pt)
HU (1) HUE025320T2 (pt)
NL (1) NL2006447C2 (pt)
PL (1) PL2689039T3 (pt)
PT (1) PT2689039E (pt)
WO (1) WO2012128624A1 (pt)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL2020952B1 (en) 2018-05-17 2019-11-25 Stichting Wageningen Res Method for producing inositol and inorganic phosphate
DE102020210071A1 (de) * 2020-08-07 2022-02-10 Südzucker AG Verbesserte Rübenzucker-Saccharosepräparation

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3503803A (en) * 1968-03-22 1970-03-31 Whiting Corp Continuous production of crystalline sucrose
GB8406734D0 (en) * 1984-03-15 1984-04-18 Tate & Lyle Plc Sugar process
ES2158419T3 (es) * 1996-10-14 2001-09-01 Bayer Ag Procedimiento de obtencion de esteres o de alcoholatos con separacion de agua.
BR0103406A (pt) * 2001-08-15 2004-05-04 Getec Guanabara Quimica Ind S Processo de produção de frutose cristalina de elevada pureza utilizando xarope com baixo teor de frutose originária de sacarose, e produto obtido
BRPI0705181A2 (pt) * 2007-10-16 2009-06-16 Dedini Sa Ind De Base processo e equipamento para cristalização de açúcar por resfriamento controlado

Also Published As

Publication number Publication date
EP2689039B1 (en) 2015-05-13
AU2012231892B2 (en) 2017-04-13
US20160097321A1 (en) 2016-04-07
CO6811871A2 (es) 2013-12-16
AU2012231892A1 (en) 2013-09-26
DK2689039T3 (en) 2015-06-29
US9810144B2 (en) 2017-11-07
US20140087437A1 (en) 2014-03-27
HRP20150561T1 (hr) 2015-08-14
CA2830644A1 (en) 2012-09-27
ES2543441T3 (es) 2015-08-19
PT2689039E (pt) 2015-08-17
NL2006447C2 (en) 2012-09-25
PL2689039T3 (pl) 2015-10-30
HUE025320T2 (en) 2016-02-29
WO2012128624A9 (en) 2013-01-10
CA2830644C (en) 2020-02-18
BR112013024121B1 (pt) 2019-12-10
WO2012128624A1 (en) 2012-09-27
US9255301B2 (en) 2016-02-09
EP2689039A1 (en) 2014-01-29

Similar Documents

Publication Publication Date Title
RU2018119914A (ru) Способ получения d-псикозы высокой чистоты
AR068287A1 (es) Procedimiento y equipo para cristalizacion de azucar por enfriamiento controlado
PE20131026A1 (es) Proceso para la recuperacion de compuestos oleaginosos a partir de biomasa
HRP20211184T1 (hr) Postupci za tretiranje vodenih sastava koji sadrže litij sulfat i sumpornu kiselinu
BR112014008497A2 (pt) método e dispositivo para a separação de gases acídicos a partir de uma mistura de gás
BR112013026186A2 (pt) processo operável continuamente para a preparação de compostos de carbonila por meio de um catalisador contendo um radical nitroxila
RU2013142931A (ru) Селективное извлечение солей из смешанного солевого рассола
BR112012031442A2 (pt) método e aparelho para produção em linha de leite de cal em um processo de produção em linha de pcc disposto com relação a uma máquina de trama fibrosa
BR112018009327A8 (pt) ?processo para purificar ácidos alcanossulfônicos, ácido alcanossulfônico, e, hidrato do ácido alcanossulfônico?
BR112015020774B1 (pt) método de refino de 1,5-diaminopentano
BR112013024121A2 (pt) processo para a cristalização de um composto solúvel em água
MX2015011381A (es) Metodo para purificar acido ferulico y/o sales del mismo.
CL2016000627A1 (es) Proceso para producir carbonato de litio, a partir de una salmuera con relación ca/li 35 a 50 p/p, y mg/li 8 a 11 p/p, con etapas de extracción con solvente, primera purificacion a traves de un separador y cristalizador, segunda y tercera purificacion, contactar salmuera con carbonato de sodio, lavar y secar.
BR112019002432A2 (pt) cristalização de glicosídeos de esteviol
BR112014009858A2 (pt) processo para rápida identificação e preparação de formas cristalinas
AR102532A1 (es) Proceso de obtención de fertilizantes que contienen amonio a partir de humos de coquería
RU2012158069A (ru) Способ получения кристаллической ангидридной глюкозы
MX2015008901A (es) Método para extraer ácido ferúlico y/o sales del mismo.
WO2016105107A3 (ko) 무수당 알코올의 효과적인 생산 및 정제 방법
CN104163812A (zh) 一种无定型的伊马替尼甲磺酸盐及其制备方法
MX2015007168A (es) Proceso para preparar particulas de una composicion detergente.
UA84992U (ru) Способ получения соли тройной кристаллической из сточных вод мышьяково-содовой сероочистки
BR112022001487A2 (pt) Processo contínuo para preparar a forma cristalina ii de sotagliflozina
TH83584B (th) วิธีการสำหรับการตกผลึกแบบทำให้เย็นเชิงแอเดียแบติกของสารประกอบอินทรีย์ และเครื่องสำหรับวิธีการดังกล่าว
CN105541960A (zh) 17α-羟基-3-氧代-γ-内酯-孕甾-4-烯-（7α，9α）-二羧酸内酯的制备方法

Legal Events

Date Code Title Description
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 19/03/2012, OBSERVADAS AS CONDICOES LEGAIS. (CO) 20 (VINTE) ANOS CONTADOS A PARTIR DE 19/03/2012, OBSERVADAS AS CONDICOES LEGAIS

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 10A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2662 DE 11-01-2022 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.