AU537559B2 - Production of ammonia and the corresponding synthesis gas - Google Patents

Production of ammonia and the corresponding synthesis gas

Info

Publication number
AU537559B2
AU537559B2 AU65488/80A AU6548880A AU537559B2 AU 537559 B2 AU537559 B2 AU 537559B2 AU 65488/80 A AU65488/80 A AU 65488/80A AU 6548880 A AU6548880 A AU 6548880A AU 537559 B2 AU537559 B2 AU 537559B2
Authority
AU
Australia
Prior art keywords
gas
ammonia
subjecting
feedstock
reforming
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
AU65488/80A
Other languages
English (en)
Other versions
AU6548880A (en
Inventor
David Leon Banquy
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Foster Wheeler Energy Corp
Original Assignee
Foster Wheeler Energy Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Foster Wheeler Energy Corp filed Critical Foster Wheeler Energy Corp
Publication of AU6548880A publication Critical patent/AU6548880A/en
Application granted granted Critical
Publication of AU537559B2 publication Critical patent/AU537559B2/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0219—Refinery gas, cracking gas, coke oven gas, gaseous mixtures containing aliphatic unsaturated CnHm or gaseous mixtures of undefined nature
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/025—Preparation or purification of gas mixtures for ammonia synthesis
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0276—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of H2/N2 mixtures, i.e. of ammonia synthesis gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/02—Processes or apparatus using separation by rectification in a single pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/74—Refluxing the column with at least a part of the partially condensed overhead gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/80—Processes or apparatus using separation by rectification using integrated mass and heat exchange, i.e. non-adiabatic rectification in a reflux exchanger or dephlegmator
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00—Processes characterised by the type or other details of the feed stream
    • F25J2210/20—H2/N2 mixture, i.e. synthesis gas for or purge gas from ammonia synthesis
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/151—Reduction of greenhouse gas [GHG] emissions, e.g. CO2

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Industrial Gases (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
AU65488/80A 1980-01-07 1980-12-17 Production of ammonia and the corresponding synthesis gas Ceased AU537559B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR8000196A FR2473032A1 (fr) 1980-01-07 1980-01-07 Procede de production d'ammoniac et du gaz de synthese correspondant
FR8000196 1980-01-07

Publications (2)

Publication Number Publication Date
AU6548880A AU6548880A (en) 1981-07-16
AU537559B2 true AU537559B2 (en) 1984-06-28

Family

ID=9237259

Family Applications (1)

Application Number Title Priority Date Filing Date
AU65488/80A Ceased AU537559B2 (en) 1980-01-07 1980-12-17 Production of ammonia and the corresponding synthesis gas

Country Status (8)

Country Link
US (1) US4296085A (show.php)
EP (1) EP0032096B1 (show.php)
JP (1) JPS6041004B2 (show.php)
AT (1) ATE8866T1 (show.php)
AU (1) AU537559B2 (show.php)
CA (1) CA1152727A (show.php)
DE (1) DE3068921D1 (show.php)
FR (1) FR2473032A1 (show.php)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU572163B2 (en) * 1983-07-05 1988-05-05 Foster Wheeler Energy Corporation Process for the production of ammonia

Families Citing this family (56)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0093502B2 (en) * 1982-04-14 1988-11-17 Imperial Chemical Industries Plc Ammonia production process
US4613492A (en) * 1982-09-01 1986-09-23 Humphreys & Glasgow, Ltd. Production of synthesis gas
US4479925A (en) * 1982-09-13 1984-10-30 The M. W. Kellogg Company Preparation of ammonia synthesis gas
JPS59199501A (ja) * 1983-04-27 1984-11-12 Res Assoc Residual Oil Process<Rarop> 水素の製造法
US4822521A (en) * 1983-06-09 1989-04-18 Uop Integrated process and apparatus for the primary and secondary catalytic steam reforming of hydrocarbons
US4545976A (en) * 1983-11-10 1985-10-08 Exxon Research & Engineering Co. Hydrocarbon steam reforming using series steam superheaters
CA1229485A (en) * 1984-01-23 1987-11-24 Toyo Engineering Corporation Process for refining an ammonia synthesis gas
US4592860A (en) * 1984-02-07 1986-06-03 Union Carbide Corporation Process and apparatus for ammonia synthesis gas production
US4755361A (en) * 1984-02-07 1988-07-05 Union Carbide Corporation Apparatus for ammonia synthesis gas production
EP0157480B1 (en) * 1984-03-02 1989-07-26 Imperial Chemical Industries Plc Process for producing ammonia synthesis gas
EP0214991A1 (en) * 1984-06-30 1987-03-25 Stamicarbon B.V. Process for preparing ammonia
GB8420644D0 (en) * 1984-08-14 1984-09-19 Petrocarbon Dev Ltd Ammonia synthesis gas
US4572829A (en) * 1984-11-09 1986-02-25 Union Carbide Corporation Ammonia synthesis gas purification
GB2186870A (en) * 1986-02-26 1987-08-26 Foster Wheeler Energy Ltd Ammonia synthesis
GB8609099D0 (en) * 1986-04-15 1986-05-21 British Petroleum Co Plc Production of synthesis gas
US4728506A (en) * 1986-05-16 1988-03-01 Catalyst Services, Inc. Start-up method for ammonia plants
DK167864B1 (da) * 1990-02-02 1993-12-27 Topsoe Haldor As Fremgangsmaade og reaktorsystem til reforming af carbonhydrider under varmeveksling
US5736116A (en) * 1995-10-25 1998-04-07 The M. W. Kellogg Company Ammonia production with enriched air reforming and nitrogen injection into the synthesis loop
US5935544A (en) * 1996-06-06 1999-08-10 Brown & Root, Inc. Moderate excess nitrogen Braun Purifier™ process and method for retrofitting non-Braun Purifier™ ammonia plants
EP0849245A1 (en) * 1996-12-20 1998-06-24 Kvaerner Process Technology Limited Process and plant for the production of methanol
AU7524598A (en) * 1997-04-10 1998-10-30 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Oxygen and nitrogen injection for increasing ammonia production
US6214258B1 (en) * 1998-08-13 2001-04-10 Air Products And Chemicals, Inc. Feed gas pretreatment in synthesis gas production
ATE279374T1 (de) * 2000-02-10 2004-10-15 Haldor Topsoe As Verfahren und vorrichtung zur herstellung von ammoniak
US6620399B1 (en) 2000-04-10 2003-09-16 Robert Rudolf Josef Jungerhans Purification of gases, in synthesis gas production process
EP1348919A4 (en) * 2000-08-29 2008-04-23 Kawajureinetsukougyo K K ABSORPTION CHILLER
US20060076275A1 (en) * 2002-07-12 2006-04-13 Smith Anthon L Process for the recovery of hydrocarbon fractions from hydrocarbonaceous solids
US6709573B2 (en) * 2002-07-12 2004-03-23 Anthon L. Smith Process for the recovery of hydrocarbon fractions from hydrocarbonaceous solids
US7090816B2 (en) * 2003-07-17 2006-08-15 Kellogg Brown & Root Llc Low-delta P purifier for nitrogen, methane, and argon removal from syngas
WO2006091987A1 (en) * 2005-02-28 2006-08-31 The Petroleum Oil And Gas Corporation Of South Africa (Pty) Ltd. Method for removing salt deposits in reformer waste heat boilers
US7377951B2 (en) * 2005-04-15 2008-05-27 Air Products And Chemicals, Inc. Process to utilize low-temperature waste heat for the preparation of synthesis gas
EP2022754A1 (en) * 2007-08-08 2009-02-11 Ammonia Casale S.A. Process for producing ammonia synthesis gas
EP2065337A1 (en) * 2007-11-27 2009-06-03 Ammonia Casale S.A. Process for producing ammonia synthesis gas
JP5424566B2 (ja) * 2008-03-14 2014-02-26 独立行政法人石油天然ガス・金属鉱物資源機構 天然ガスからの液状炭化水素製造プロセスにおける合成ガスの製造方法
EP2159192A1 (en) * 2008-08-28 2010-03-03 Ammonia Casale S.A. Process for the production of ammonia synthesis gas with improved cryogenic purification
EP2172417A1 (en) * 2008-10-02 2010-04-07 Ammonia Casale S.A. Process for the production of ammonia synthesis gas
DE102008056538A1 (de) * 2008-11-10 2010-05-12 Uhde Gmbh Prozessgaserzeugung mittels Wärmerückgewinnung aus Niedertemperaturabwärme
JP5766397B2 (ja) * 2009-09-16 2015-08-19 三菱重工業株式会社 アンモニア製造方法及び装置
CN103025649A (zh) * 2010-05-26 2013-04-03 Gtl汽油有限公司 使用超纯高压氢气制备氨
EP2404869A1 (en) * 2010-07-06 2012-01-11 Ammonia Casale S.A. Process for producing ammonia synthesis gas
US8889093B2 (en) * 2010-09-16 2014-11-18 Kellogg Brown & Root Llc High pressure cyrogenic process and system for producing ammonia products
EP2801550A1 (en) 2013-05-10 2014-11-12 Ammonia Casale S.A. A process for producing ammonia synthesis gas with high temperature shift and low steam-to-carbon ratio
EP2818447A1 (en) * 2013-06-26 2014-12-31 Ammonia Casale S.A. A process for purification of a synthesis gas containing hydrogen and impurities
US9561968B2 (en) * 2013-08-07 2017-02-07 Kellogg Brown & Root Llc Methods and systems for producing and processing syngas in a pressure swing adsorption unit and making ammonia therefrom
EP2886513A1 (en) 2013-12-20 2015-06-24 Casale Sa Process for producing ammonia synthesis gas
EP3037386A1 (en) * 2014-12-23 2016-06-29 Casale SA A plant and a process for ammonia production with cryogenic purification, and a related method of revamping
EP3124433B1 (de) * 2015-07-27 2021-09-01 L'Air Liquide Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Verfahren zur kühlung von synthesegas
DE102016123661A1 (de) 2016-12-07 2018-06-07 Ask Chemicals Gmbh Alkalische Resolbinder mit verbesserter Fließfähigkeit
DE102017201681A1 (de) * 2017-02-02 2018-08-02 Thyssenkrupp Ag Verfahren zur Behandlung eines Synthesegasstroms
CN106679243B (zh) * 2017-02-17 2022-05-20 查都(海南)科技有限公司 一种降低液氨消耗的制冷系统
DE102017011601A1 (de) * 2017-12-14 2019-06-19 Linde Aktiengesellschaft Ammoniaksynthese mit internem Kühlkreislauf
EP3623343A1 (en) * 2018-09-11 2020-03-18 Casale Sa Process for the synthesis of ammonia
WO2020150247A1 (en) * 2019-01-15 2020-07-23 Sabic Global Technologies, B.V. Use of renewable energy in methanol synthesis
CN112499646B (zh) * 2020-11-19 2024-04-05 宁夏坤辉气化有限公司 一种串联式氨合成工艺
IT202200004073A1 (it) * 2022-03-04 2023-09-04 Nuovo Pignone Tecnologie Srl Unità di multi-compressione per la produzione di ammoniaca
CN121311444A (zh) * 2023-08-23 2026-01-09 诺瓦泰克公共股份公司 通过天然气生产低碳氨的方法
KR20250172851A (ko) * 2023-08-30 2025-12-09 퍼블리크노에 악치오네르노에 옵스체스트보 “노바텍” 천연가스로부터 저탄소 암모니아를 생산하기 위한 방법

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US2829113A (en) * 1953-10-14 1958-04-01 Kellogg M W Co Production of nitrogen and hydrogen for ammonia synthesis
US3278452A (en) * 1959-12-24 1966-10-11 Pullman Inc Production of hydrogen-containing gases
US3264066A (en) * 1962-05-01 1966-08-02 Pullman Inc Production of hydrogen
FR1409027A (fr) * 1963-09-09 1965-08-20 Chemical Construction Corproat Procédé de préparation simultanée de l'ammoniac et de l'urée
US3388074A (en) * 1963-12-26 1968-06-11 Catalysts & Chem Inc Two-stage steam reforming with rapid warm-up in first stage by means of a promoted catalyst
US3442613A (en) * 1965-10-22 1969-05-06 Braun & Co C F Hydrocarbon reforming for production of a synthesis gas from which ammonia can be prepared
GB1156003A (en) * 1965-10-22 1969-06-25 Braun & Co C F Ammonia Synthesis Gas Purification Process and Apparatus.
US3441393A (en) * 1966-01-19 1969-04-29 Pullman Inc Process for the production of hydrogen-rich gas
US3556751A (en) * 1968-04-05 1971-01-19 Texaco Inc Production of synthesis gas
FR1604197A (en) * 1968-12-30 1971-07-26 Reforming of hydrocarbons to obtain - ammonia synthesis gas
FR2044617A2 (en) * 1969-11-28 1971-02-26 Cem Comp Electro Mec Reforming of hydrocarbons to obtain - ammonia synthesis gas
DE1920001A1 (de) * 1969-04-19 1970-12-17 Metallgesellschaft Ag Verfahren zur Erzeugung eines Synthesegases fuer die Herstellung von Ammoniak
DE2732587A1 (de) * 1976-09-22 1978-03-23 Bach Jean Francois Polypeptid mit thymischer wirksamkeit
US4148866A (en) * 1976-10-04 1979-04-10 Pullman Incorporated Low energy ammonia synthesis process
US4079017A (en) * 1976-11-19 1978-03-14 Pullman Incorporated Parallel steam reformers to provide low energy process

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU572163B2 (en) * 1983-07-05 1988-05-05 Foster Wheeler Energy Corporation Process for the production of ammonia

Also Published As

Publication number Publication date
JPS5734021A (en) 1982-02-24
EP0032096B1 (fr) 1984-08-08
DE3068921D1 (en) 1984-09-13
JPS6041004B2 (ja) 1985-09-13
EP0032096A2 (fr) 1981-07-15
FR2473032B1 (show.php) 1985-03-08
FR2473032A1 (fr) 1981-07-10
CA1152727A (en) 1983-08-30
ATE8866T1 (de) 1984-08-15
EP0032096A3 (en) 1981-07-22
AU6548880A (en) 1981-07-16
US4296085A (en) 1981-10-20

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