AU2012347153B2 - Method and device for separating hydrogen sulfide and hydrogen production system using the same - Google Patents

Method and device for separating hydrogen sulfide and hydrogen production system using the same Download PDF

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Publication number
AU2012347153B2
AU2012347153B2 AU2012347153A AU2012347153A AU2012347153B2 AU 2012347153 B2 AU2012347153 B2 AU 2012347153B2 AU 2012347153 A AU2012347153 A AU 2012347153A AU 2012347153 A AU2012347153 A AU 2012347153A AU 2012347153 B2 AU2012347153 B2 AU 2012347153B2
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AU
Australia
Prior art keywords
hydrogen sulfide
carbon dioxide
adsorbent
gas
hydrogen
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
AU2012347153A
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English (en)
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AU2012347153A1 (en
Inventor
Masatoshi Hirokawa
Norihiko Kumada
Toshinori Muraoka
Takashi Nakamoto
Shigenobu OKAJIMA
Takatoshi Shoji
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kawasaki Motors Ltd
Original Assignee
Kawasaki Heavy Industries Ltd
Kawasaki Jukogyo KK
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Publication of AU2012347153A1 publication Critical patent/AU2012347153A1/en
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Ceased legal-status Critical Current
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification
    • C01B3/508—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification by using hydrogen storage media
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0462—Temperature swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/46—Removing components of defined structure
    • B01D53/48—Sulfur compounds
    • B01D53/52—Hydrogen sulfide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/81—Solid phase processes
    • B01D53/82—Solid phase processes with stationary reactants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/16—Hydrogen sulfides
    • C01B17/167—Separation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification
    • C01B3/56—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/50—Carbon dioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/20—Organic absorbents
    • B01D2252/204—Amines
    • B01D2252/20431—Tertiary amines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/20—Organic adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/25—Coated, impregnated or composite adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/16—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/30—Sulfur compounds
    • B01D2257/304—Hydrogen sulfide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/504—Carbon dioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042—Purification by adsorption on solids
    • C01B2203/043—Regenerative adsorption process in two or more beds, one for adsorption, the other for regeneration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0475—Composition of the impurity the impurity being carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0485—Composition of the impurity the impurity being a sulfur compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/146—At least two purification steps in series
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/146—At least two purification steps in series
    • C01B2203/147—Three or more purification steps in series
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00—Capture or disposal of greenhouse gases
    • Y02C20/40—Capture or disposal of greenhouse gases of CO2

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Combustion & Propulsion (AREA)
  • Gas Separation By Absorption (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Treating Waste Gases (AREA)
  • Hydrogen, Water And Hydrids (AREA)
AU2012347153A 2011-12-08 2012-10-29 Method and device for separating hydrogen sulfide and hydrogen production system using the same Ceased AU2012347153B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2011-268825 2011-12-08
JP2011268825A JP5906074B2 (ja) 2011-12-08 2011-12-08 水素製造システム
PCT/JP2012/006928 WO2013084402A1 (ja) 2011-12-08 2012-10-29 硫化水素分離方法および装置並びにこれを用いた水素製造システム

Publications (2)

Publication Number Publication Date
AU2012347153A1 AU2012347153A1 (en) 2014-07-10
AU2012347153B2 true AU2012347153B2 (en) 2015-09-24

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
AU2012347153A Ceased AU2012347153B2 (en) 2011-12-08 2012-10-29 Method and device for separating hydrogen sulfide and hydrogen production system using the same

Country Status (5)

Country Link
US (1) US9365423B2 (https=)
JP (1) JP5906074B2 (https=)
CN (1) CN103958029B (https=)
AU (1) AU2012347153B2 (https=)
WO (1) WO2013084402A1 (https=)

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KR102472112B1 (ko) * 2014-10-24 2022-11-28 리써치 트라이앵글 인스티튜트 가스 스트림으로부터 산 가스를 제거하기 위한 통합 시스템 및 방법
CA2977765A1 (en) * 2015-02-27 2016-09-01 Dow Global Technologies Llc Method to selectively remove hydrogen sulfide from a gas stream using a functionalized cross-linked macroporous polymer
CN108537475A (zh) * 2017-03-03 2018-09-14 顺丰科技有限公司 快件揽收订单匹配方法及装置
CN107628619A (zh) * 2017-09-15 2018-01-26 深圳市水务(集团)有限公司 一种掺杂食物下脚料的富氮污泥活性炭的制备方法
JP7121049B2 (ja) * 2017-12-25 2022-08-17 住友化学株式会社 硫化水素の製造方法及び硫黄の回収方法
US12325004B2 (en) 2020-07-07 2025-06-10 Exxonmobil Technology & Engineering Company Acid gas scrubbing methods featuring amine phase separation for hydrogen sulfide capture
RS64117B1 (sr) * 2020-10-29 2023-04-28 Rwe Generation Nl B V Konvertovanje čvrstog otpada u sintetički gas i vodonik
CN113231037A (zh) * 2021-05-21 2021-08-10 南京工业大学 一种用于脱除微量硫化氢的固体胺吸附剂及其制备方法
CN113231036A (zh) * 2021-05-21 2021-08-10 南京工业大学 一种用于脱除超低浓度硫化氢的负载型吸附剂及其制备方法
CN114777421B (zh) * 2022-03-31 2024-08-02 中科瑞奥能源科技股份有限公司 从氯乙酸或氯乙酰氯合成尾气中提纯氯化氢的系统和方法
US11959637B2 (en) * 2022-04-06 2024-04-16 Next Carbon Solutions, Llc Devices, systems, facilities and processes for CO2 post combustion capture incorporated at a data center
CN115254022A (zh) * 2022-08-11 2022-11-01 湖南宇洁活性炭环保科技有限公司 一种高效净化硫化氢气体的改性活性炭及其制备方法
CN117268879B (zh) * 2023-11-22 2024-02-02 天津朔程科技有限公司 一种采气井口的气体采集分析方法及装置

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JPS6456114A (en) * 1987-08-26 1989-03-03 Sumitomo Heavy Industries Adsorption reactor for gaseous carbon dioxide
JPH07258664A (ja) * 1994-03-18 1995-10-09 Kansai Electric Power Co Inc:The ガス中の硫化水素を選択的に除去する方法
JPH07256096A (ja) * 1994-01-06 1995-10-09 Akzo Nobel Nv ガス混合物からガス状不純物を除去するための物質
WO2001028916A1 (en) * 1999-10-21 2001-04-26 Ebara Corporation Method of producing hydrogen by gasification of combustibles and electric power generation using fuel cell
WO2011108212A1 (ja) * 2010-03-02 2011-09-09 独立行政法人石油天然ガス・金属鉱物資源機構 合成ガスの製造方法

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JPS6456114A (en) * 1987-08-26 1989-03-03 Sumitomo Heavy Industries Adsorption reactor for gaseous carbon dioxide
JPH07256096A (ja) * 1994-01-06 1995-10-09 Akzo Nobel Nv ガス混合物からガス状不純物を除去するための物質
JPH07258664A (ja) * 1994-03-18 1995-10-09 Kansai Electric Power Co Inc:The ガス中の硫化水素を選択的に除去する方法
WO2001028916A1 (en) * 1999-10-21 2001-04-26 Ebara Corporation Method of producing hydrogen by gasification of combustibles and electric power generation using fuel cell
WO2011108212A1 (ja) * 2010-03-02 2011-09-09 独立行政法人石油天然ガス・金属鉱物資源機構 合成ガスの製造方法

Also Published As

Publication number Publication date
AU2012347153A1 (en) 2014-07-10
US20140360368A1 (en) 2014-12-11
JP5906074B2 (ja) 2016-04-20
WO2013084402A1 (ja) 2013-06-13
US9365423B2 (en) 2016-06-14
CN103958029A (zh) 2014-07-30
JP2013119503A (ja) 2013-06-17
CN103958029B (zh) 2016-01-20

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