AU2008260452A1 - Silica particles and methods of making and using the same - Google Patents

Silica particles and methods of making and using the same Download PDF

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Publication number
AU2008260452A1
AU2008260452A1 AU2008260452A AU2008260452A AU2008260452A1 AU 2008260452 A1 AU2008260452 A1 AU 2008260452A1 AU 2008260452 A AU2008260452 A AU 2008260452A AU 2008260452 A AU2008260452 A AU 2008260452A AU 2008260452 A1 AU2008260452 A1 AU 2008260452A1
Authority
AU
Australia
Prior art keywords
particle
silica particles
particles
porous
porous silica
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2008260452A
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English (en)
Inventor
Lawrence Kindt
James Neil Pryor
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Alltech Associates Inc
Original Assignee
Alltech Associates Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Alltech Associates Inc filed Critical Alltech Associates Inc
Publication of AU2008260452A1 publication Critical patent/AU2008260452A1/en
Abandoned legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/124Preparation of adsorbing porous silica not in gel form and not finely divided, i.e. silicon skeletons, by acidic treatment of siliceous materials
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016Particle form
    • B01J20/28019Spherical, ellipsoidal or cylindrical
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057Surface area, e.g. B.E.T specific surface area
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28069Pore volume, e.g. total pore volume, mesopore volume, micropore volume
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28078Pore diameter
    • B01J20/28083Pore diameter being in the range 2-50 nm, i.e. mesopores
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/282Porous sorbents
    • B01J20/283Porous sorbents based on silica
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3291Characterised by the shape of the carrier, the coating or the obtained coated product
    • B01J20/3293Coatings on a core, the core being particle or fiber shaped, e.g. encapsulated particles, coated fibers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/145Preparation of hydroorganosols, organosols or dispersions in an organic medium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/146After-treatment of sols
    • C01B33/148Concentration; Drying; Dehydration; Stabilisation; Purification
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/16Preparation of silica xerogels
    • C01B33/163Preparation of silica xerogels by hydrolysis of organosilicon compounds, e.g. ethyl orthosilicate
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982Particulate matter [e.g., sphere, flake, etc.]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Nanotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Silicon Compounds (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Cosmetics (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
AU2008260452A 2007-06-04 2008-06-04 Silica particles and methods of making and using the same Abandoned AU2008260452A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US93306907P 2007-06-04 2007-06-04
US60/933,069 2007-06-04
PCT/US2008/007034 WO2008150537A2 (en) 2007-06-04 2008-06-04 Silica particles and methods of making and using the same

Publications (1)

Publication Number Publication Date
AU2008260452A1 true AU2008260452A1 (en) 2008-12-11

Family

ID=40056210

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2008260452A Abandoned AU2008260452A1 (en) 2007-06-04 2008-06-04 Silica particles and methods of making and using the same

Country Status (12)

Country Link
US (1) US20100116743A1 (cg-RX-API-DMAC7.html)
EP (1) EP2167425A2 (cg-RX-API-DMAC7.html)
JP (1) JP5498377B2 (cg-RX-API-DMAC7.html)
KR (1) KR20100022499A (cg-RX-API-DMAC7.html)
CN (1) CN101918312A (cg-RX-API-DMAC7.html)
AR (1) AR066853A1 (cg-RX-API-DMAC7.html)
AU (1) AU2008260452A1 (cg-RX-API-DMAC7.html)
CA (1) CA2690537A1 (cg-RX-API-DMAC7.html)
IN (1) IN2009DN08217A (cg-RX-API-DMAC7.html)
MX (1) MX2009013170A (cg-RX-API-DMAC7.html)
TW (1) TW200914372A (cg-RX-API-DMAC7.html)
WO (1) WO2008150537A2 (cg-RX-API-DMAC7.html)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101411007B1 (ko) * 2010-12-31 2014-06-23 제일모직주식회사 방현 필름용 조성물 및 이를 포함하는 방현 필름
CN102380345B (zh) * 2011-08-03 2013-01-16 济南大学 孔呈梯度分布的中空二氧化硅微球及其制备方法和应用
GB2497105B (en) * 2011-12-01 2014-07-23 Thermo Electron Mfg Ltd Process for the preparation of porous silica particles
IN2015DN02055A (cg-RX-API-DMAC7.html) 2012-09-17 2015-08-14 Grace W R & Co
PL3137209T3 (pl) 2014-05-02 2023-01-02 W.R. Grace & Co. - Conn. Funkcjonalizowany materiał nośnikowy i sposoby wytwarzania oraz stosowania funkcjonalizowanego materiału nośnikowego
PL3302784T3 (pl) 2015-06-05 2022-01-17 W.R. Grace & Co.-Conn. Adsorbentowe środki klarujące do bioprzetwarzania oraz sposoby ich wytwarzania i stosowania
WO2017033914A1 (ja) * 2015-08-25 2017-03-02 昭和電工株式会社 液体クロマトグラフィー用カラム及びそれを備えた液体クロマトグラフ装置
AU2018262708B2 (en) 2017-05-04 2021-06-03 Nanologica Ab A process for manufacturing porous silica particles loaded with at least one bioactive compound adapted for lung, nasal, sublingual and/or pharyngeal delivery
US10661250B2 (en) * 2018-04-13 2020-05-26 Agilent Technologies, Inc. Synthetic silica as packing material in supported liquid extraction
KR102427987B1 (ko) * 2018-11-27 2022-08-02 주식회사 엘지화학 전가수분해된 폴리실리케이트의 합성방법
GB201916122D0 (en) 2019-11-06 2019-12-18 Nanologica Ab New compositions
CN118833827A (zh) * 2020-01-28 2024-10-25 三菱化学株式会社 二氧化硅粒子、硅溶胶、研磨组合物、研磨方法、半导体晶片的制造方法和半导体装置的制造方法
JP2025508226A (ja) * 2022-03-16 2025-03-21 ダブリュー・アール・グレース・アンド・カンパニー-コーン 多孔質の球状シリカゲル粒子を生産する方法
US20240018006A1 (en) * 2022-07-13 2024-01-18 Uchicago Argonne, Llc Method For Producing Porous Nanocrystalline Silicon

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1473239A (cg-RX-API-DMAC7.html) * 1966-01-31 1967-05-29
US3591518A (en) * 1968-12-31 1971-07-06 Du Pont Silica aquasols and powders
SE417431B (sv) * 1975-12-12 1981-03-16 Pharmacia Fine Chemicals Ab Dextranderivatgel for elektroforetisk separation
US4160728A (en) * 1976-12-08 1979-07-10 E. I. Du Pont De Nemours And Company Bimodal chromatographic resolving zone
US4301034A (en) * 1980-05-21 1981-11-17 Phillips Petroleum Company Silica from single phase controlled hydrolysis of silicate ester
DE3616133A1 (de) * 1985-09-25 1987-11-19 Merck Patent Gmbh Kugelfoermige sio(pfeil abwaerts)2(pfeil abwaerts)-partikel
US4943425A (en) * 1988-04-01 1990-07-24 Gte Laboratories Incorporated Method of making high purity dense silica of large particle size
US5023208A (en) * 1989-12-19 1991-06-11 Orion Laboratories, Inc. Sol-gel process for glass and ceramic articles
IT1240673B (it) * 1990-04-24 1993-12-17 Tenav Microsfere di aerogels di ossidi inorganici a stretta distribuzione dei diametri dei pori e metodo per la loro preparazione
US5409683A (en) * 1990-08-23 1995-04-25 Regents Of The University Of California Method for producing metal oxide aerogels
DE69128073T2 (de) * 1990-08-23 1998-02-26 Univ California As Represented Verfahren zur herstellung von metalloxidaerogelen mit dichte weniger als 0,02 g/cm3
US5425930A (en) * 1993-09-17 1995-06-20 Alliedsignal Inc. Process for forming large silica spheres by low temperature nucleation
IT1266660B1 (it) * 1993-11-04 1997-01-09 Eniricerche Spa Procedimento per la preparazione di xerogels di silice porosi in forma sferica
JP2580537B2 (ja) * 1994-06-27 1997-02-12 工業技術院長 シリカ球状粒子からなる三次元網状構造体
US5728457A (en) * 1994-09-30 1998-03-17 Cornell Research Foundation, Inc. Porous polymeric material with gradients
US6290735B1 (en) * 1997-10-31 2001-09-18 Nanogram Corporation Abrasive particles for surface polishing
GB2355711B (en) * 1999-10-27 2003-12-24 Agilent Technologies Inc Porous silica microsphere scavengers
US6569908B2 (en) * 2000-01-19 2003-05-27 Oji Paper Co., Ltd. Dispersion of silica particle agglomerates and process for producing the same
JP4216716B2 (ja) * 2001-08-09 2009-01-28 ウォーターズ・インヴェストメンツ・リミテッド クロマトグラフィー分離用多孔質有機・無機ハイブリッドモノリス状物質、およびその製造方法
CA2729228C (fr) * 2001-08-13 2014-11-18 Rhodia Chimie Silices a distribution granulometrique et/ou repartition poreuse particulieres et leurs utilisations, notamment pour le renforcement de polymeres
US7101523B2 (en) * 2001-09-25 2006-09-05 Mitsubishi Chemical Corporation Silica
US20040091411A1 (en) * 2002-11-08 2004-05-13 Bijan Modrek-Najafabadi High surface area, high porosity silica packing with narrow particle and pore diameter distribution and methods of making same
JP2005154195A (ja) * 2003-11-25 2005-06-16 Matsushita Electric Works Ltd エアロゲル材、及びこのエアロゲル材にて形成される物品
US20060169640A1 (en) * 2005-02-01 2006-08-03 Hubert Quinn High throughput screening, purification and recovery system for large and small molecules
US7468130B2 (en) * 2005-02-15 2008-12-23 Dionex Corporation Organosilanes and substrates covalently bonded with same and methods for synthesis and use same
PT103257B (pt) * 2005-04-05 2007-05-31 Inst Superior Tecnico Método de produção subcrítica de xerogéis e aerogéis monolíticos híbridos de sílica e látex modificado com grupos alcoxissilano
SG131016A1 (en) * 2005-09-19 2007-04-26 Millipore Corp Asymmetric porous adsorptive bead
US20070189944A1 (en) * 2006-02-13 2007-08-16 Advanced Materials Technology, Inc. Porous microparticles with solid cores
CN100396612C (zh) * 2006-09-15 2008-06-25 南开大学 纳米球形介孔二氧化硅材料和制备方法

Also Published As

Publication number Publication date
MX2009013170A (es) 2010-03-01
WO2008150537A3 (en) 2010-08-12
CA2690537A1 (en) 2008-12-11
CN101918312A (zh) 2010-12-15
JP2010531798A (ja) 2010-09-30
AR066853A1 (es) 2009-09-16
US20100116743A1 (en) 2010-05-13
JP5498377B2 (ja) 2014-05-21
WO2008150537A2 (en) 2008-12-11
EP2167425A2 (en) 2010-03-31
IN2009DN08217A (cg-RX-API-DMAC7.html) 2015-07-24
KR20100022499A (ko) 2010-03-02
TW200914372A (en) 2009-04-01

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