AU2004288994B2 - Polar silanes for binding to substrates and use of the bound substrates in chromatography - Google Patents

Polar silanes for binding to substrates and use of the bound substrates in chromatography Download PDF

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Publication number
AU2004288994B2
AU2004288994B2 AU2004288994A AU2004288994A AU2004288994B2 AU 2004288994 B2 AU2004288994 B2 AU 2004288994B2 AU 2004288994 A AU2004288994 A AU 2004288994A AU 2004288994 A AU2004288994 A AU 2004288994A AU 2004288994 B2 AU2004288994 B2 AU 2004288994B2
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AU
Australia
Prior art keywords
alkyl
group
reverse phase
phase chromatography
separation medium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
AU2004288994A
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English (en)
Other versions
AU2004288994A1 (en
Inventor
Andrei V. Bordunov
Christopher A. Pohl
Liu Xiaodong
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dionex Corp
Original Assignee
Dionex Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dionex Corp filed Critical Dionex Corp
Publication of AU2004288994A1 publication Critical patent/AU2004288994A1/en
Application granted granted Critical
Publication of AU2004288994B2 publication Critical patent/AU2004288994B2/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3242—Layers with a functional group, e.g. an affinity material, a ligand, a reactant or a complexing group
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286—Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286—Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • B01J20/287—Non-polar phases; Reversed phases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C07F7/1804—Compounds having Si-O-C linkages
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/54—Sorbents specially adapted for analytical or investigative chromatography
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31652—Of asbestos
    • Y10T428/31663—As siloxane, silicone or silane

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
AU2004288994A 2003-11-04 2004-10-04 Polar silanes for binding to substrates and use of the bound substrates in chromatography Ceased AU2004288994B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/702,109 2003-11-04
US10/702,109 US7074491B2 (en) 2003-11-04 2003-11-04 Polar silanes for binding to substrates and use of the bound substrates
PCT/US2004/032655 WO2005047886A1 (en) 2003-11-04 2004-10-04 Polar silanes for binding to substrates and use of the bound substrates in chromatography

Publications (2)

Publication Number Publication Date
AU2004288994A1 AU2004288994A1 (en) 2005-05-26
AU2004288994B2 true AU2004288994B2 (en) 2011-07-14

Family

ID=34551590

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2004288994A Ceased AU2004288994B2 (en) 2003-11-04 2004-10-04 Polar silanes for binding to substrates and use of the bound substrates in chromatography

Country Status (8)

Country Link
US (1) US7074491B2 (enExample)
EP (1) EP1680432B1 (enExample)
JP (1) JP4904161B2 (enExample)
KR (1) KR20060125788A (enExample)
CN (1) CN1901990B (enExample)
AU (1) AU2004288994B2 (enExample)
CA (1) CA2544636A1 (enExample)
WO (1) WO2005047886A1 (enExample)

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US7402243B2 (en) 2004-09-10 2008-07-22 Dionex Corporation Organosilanes and substrate bonded with same
US7468130B2 (en) * 2005-02-15 2008-12-23 Dionex Corporation Organosilanes and substrates covalently bonded with same and methods for synthesis and use same
US7557232B2 (en) * 2007-05-25 2009-07-07 Dionex Corporation Compositions useful as chromatography stationary phases
US9314712B2 (en) 2008-05-09 2016-04-19 Dionex Corporation Functionalized substrates with ion-exchange properties
CN102939140B (zh) 2010-05-19 2015-05-20 迪奥内克斯公司 具有芳香族堆积特性的官能化的基质
EP2675560B1 (en) 2011-02-14 2019-08-28 Dionex Corporation Liquid chromatographic column including a ligand comprising a polyhedral oligomeric silsequioxane moiety, and liquid chromatografic method using the column
CN104428045B (zh) 2012-05-15 2017-12-01 沃特世科技公司 色谱材料
CN111644164B (zh) * 2012-05-15 2024-03-08 沃特世科技公司 用于分离不饱和分子的色谱材料
SG11201404681VA (en) 2012-09-17 2014-09-26 Grace W R & Co Chromatography media and devices
US9610576B2 (en) 2012-09-27 2017-04-04 Agilent Technologies, Inc. Hydrolytically stable ion-exchange stationary phases and uses thereof
CN103357390A (zh) * 2012-11-12 2013-10-23 北京迪马欧泰科技发展中心 多层结构键合硅胶液相色谱填料及其合成方法
US9169331B2 (en) 2012-12-21 2015-10-27 Dionex Corporation Separation of glycans by mixed-mode liquid chromatography
EP2745904B1 (en) 2012-12-21 2015-12-16 Dionex Corporation HILIC/Anion-Exchange/Cation-Exchange Multimodal Media
US9310344B2 (en) 2013-06-14 2016-04-12 Dionex Corporation HILIC/anion-exchange/cation-exchange multimodal media
CN103170311A (zh) * 2013-03-20 2013-06-26 华东理工大学 新型氨基系列色谱固定相及制备方法
EP3936226A3 (en) 2013-06-11 2022-03-16 Waters Technologies Corporation Chromatographic columns and separation devices comprising a superficially porous material; and use thereof for supercritical fluid chromatography and other chromatography
CN107847907A (zh) 2014-05-02 2018-03-27 格雷斯公司 官能化载体材料以及制备和使用官能化载体材料的方法
WO2016115101A1 (en) 2015-01-15 2016-07-21 Dionex Corporation Chromatographic material having improved ph stability, method for preparation thereof and uses thereof
US10695744B2 (en) 2015-06-05 2020-06-30 W. R. Grace & Co.-Conn. Adsorbent biprocessing clarification agents and methods of making and using the same
US10618920B2 (en) 2016-06-03 2020-04-14 Agilent Technologies, Inc. Functionalized particles having modified phases
US20190126167A1 (en) 2017-11-01 2019-05-02 Dionex Corporation Sulfonamide based anion exchange resins
CN111135808B (zh) * 2019-12-30 2023-03-31 纳谱分析技术（苏州）有限公司 硅化合物、固定相及其应用

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4623740A (en) * 1984-07-04 1986-11-18 Ulrich Deschler N,N'- and N,N',N'-substituted silylureas and process for their production
US5019637A (en) * 1988-11-04 1991-05-28 Peter Panster Organopolysiloxane urea derivatives and organopolysiloxane thiourea derivatives, methods of their preparation and use
WO1994000408A1 (en) * 1992-06-23 1994-01-06 Research Corporation Technologies, Inc. High performance chiral selector
WO1994009013A1 (en) * 1992-10-13 1994-04-28 Caschem, Inc. Dual curing conformal coatings

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BE623601A (enExample) * 1961-10-16 1900-01-01
DE2250921A1 (de) 1972-10-18 1974-04-25 Dynamit Nobel Ag Neue silane von sulfon- und phosphorsaeureamiden
DE2357184A1 (de) * 1973-11-16 1975-05-22 Merck Patent Gmbh Verfahren zur herstellung von organisch modifizierten siliciumdioxiden
DE2641201A1 (de) * 1976-09-14 1978-03-16 Consortium Elektrochem Ind Diorganopolysiloxane enthaltende gemische und verfahren zu ihrer herstellung
US4584138A (en) * 1983-09-30 1986-04-22 Union Carbide Corporation Novel fatty ethenoid acylaminoorganosilicon compounds and their use as a coupling agent
US4705725A (en) * 1986-11-28 1987-11-10 E. I. Du Pont De Nemours And Company Substrates with sterically-protected, stable, covalently-bonded organo-silane films
DE3706521A1 (de) * 1987-02-28 1988-09-08 Degussa Benzoylthioharnstoffgruppen-haltige organosilane, verfahren zu ihrer herstellung
DE3821465A1 (de) * 1988-06-25 1989-12-28 Degussa Verfahren zur herstellung ein- oder mehrfach substituierter organyloxysilylfunktioneller thioharnstoffe und diese verbindungen
JPH0219387A (ja) * 1988-07-08 1990-01-23 Toshiba Silicone Co Ltd 有機ケイ素化合物およびその製造方法
US4990641A (en) * 1988-07-08 1991-02-05 Toshiba Silicone Co., Ltd. Organosilicon compound and its preparing method
JPH02107650A (ja) * 1988-10-17 1990-04-19 Toshiba Silicone Co Ltd 無機ケイ素質充填剤用処理剤
US5374755A (en) * 1992-07-17 1994-12-20 Millipore Corporation Liquid chromatography stationary phases with reduced silanol interactions
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CA2222137A1 (en) * 1995-06-05 1996-12-12 Basil V. Gregorovich Coating composition containing silane functionality
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US6800777B2 (en) * 2001-05-03 2004-10-05 Gelest, Inc. Trialkylsilanes for use in chromatographic applications, substrates including such compounds and methods of producing the same
US6645378B1 (en) * 2002-03-05 2003-11-11 Dionex Corporation Polar silanes and their use on silica supports
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Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4623740A (en) * 1984-07-04 1986-11-18 Ulrich Deschler N,N'- and N,N',N'-substituted silylureas and process for their production
US5019637A (en) * 1988-11-04 1991-05-28 Peter Panster Organopolysiloxane urea derivatives and organopolysiloxane thiourea derivatives, methods of their preparation and use
WO1994000408A1 (en) * 1992-06-23 1994-01-06 Research Corporation Technologies, Inc. High performance chiral selector
WO1994009013A1 (en) * 1992-10-13 1994-04-28 Caschem, Inc. Dual curing conformal coatings

Also Published As

Publication number Publication date
CA2544636A1 (en) 2005-05-26
WO2005047886A1 (en) 2005-05-26
KR20060125788A (ko) 2006-12-06
JP2007510644A (ja) 2007-04-26
EP1680432B1 (en) 2014-08-20
EP1680432A1 (en) 2006-07-19
AU2004288994A1 (en) 2005-05-26
CN1901990B (zh) 2013-04-03
JP4904161B2 (ja) 2012-03-28
US7074491B2 (en) 2006-07-11
US20050095440A1 (en) 2005-05-05
CN1901990A (zh) 2007-01-24

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FGA Letters patent sealed or granted (standard patent)
MK14 Patent ceased section 143(a) (annual fees not paid) or expired