JP4904161B2 - 基材結合用の極性シラン及び結合された基材のクロマトグラフィーにおける使用 - Google Patents

基材結合用の極性シラン及び結合された基材のクロマトグラフィーにおける使用 Download PDF

Info

Publication number
JP4904161B2
JP4904161B2 JP2006538010A JP2006538010A JP4904161B2 JP 4904161 B2 JP4904161 B2 JP 4904161B2 JP 2006538010 A JP2006538010 A JP 2006538010A JP 2006538010 A JP2006538010 A JP 2006538010A JP 4904161 B2 JP4904161 B2 JP 4904161B2
Authority
JP
Japan
Prior art keywords
group
substrate
silicon compound
silica
use according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP2006538010A
Other languages
English (en)
Japanese (ja)
Other versions
JP2007510644A (ja
JP2007510644A5 (enExample
Inventor
リウ シァオドン
アンドレイ ヴィー ボーデュノフ
クリストファー エイ ポール
Original Assignee
ダイオネックス コーポレイション
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ダイオネックス コーポレイション filed Critical ダイオネックス コーポレイション
Publication of JP2007510644A publication Critical patent/JP2007510644A/ja
Publication of JP2007510644A5 publication Critical patent/JP2007510644A5/ja
Application granted granted Critical
Publication of JP4904161B2 publication Critical patent/JP4904161B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/18Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3242Layers with a functional group, e.g. an affinity material, a ligand, a reactant or a complexing group
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • B01J20/287Non-polar phases; Reversed phases
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/18Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C07F7/1804Compounds having Si-O-C linkages
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00Aspects relating to sorbent materials
    • B01J2220/50Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/54Sorbents specially adapted for analytical or investigative chromatography
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/31504Composite [nonstructural laminate]
    • Y10T428/31652Of asbestos
    • Y10T428/31663As siloxane, silicone or silane

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
JP2006538010A 2003-11-04 2004-10-04 基材結合用の極性シラン及び結合された基材のクロマトグラフィーにおける使用 Expired - Lifetime JP4904161B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/702,109 2003-11-04
US10/702,109 US7074491B2 (en) 2003-11-04 2003-11-04 Polar silanes for binding to substrates and use of the bound substrates
PCT/US2004/032655 WO2005047886A1 (en) 2003-11-04 2004-10-04 Polar silanes for binding to substrates and use of the bound substrates in chromatography

Publications (3)

Publication Number Publication Date
JP2007510644A JP2007510644A (ja) 2007-04-26
JP2007510644A5 JP2007510644A5 (enExample) 2007-06-14
JP4904161B2 true JP4904161B2 (ja) 2012-03-28

Family

ID=34551590

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2006538010A Expired - Lifetime JP4904161B2 (ja) 2003-11-04 2004-10-04 基材結合用の極性シラン及び結合された基材のクロマトグラフィーにおける使用

Country Status (8)

Country Link
US (1) US7074491B2 (enExample)
EP (1) EP1680432B1 (enExample)
JP (1) JP4904161B2 (enExample)
KR (1) KR20060125788A (enExample)
CN (1) CN1901990B (enExample)
AU (1) AU2004288994B2 (enExample)
CA (1) CA2544636A1 (enExample)
WO (1) WO2005047886A1 (enExample)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7402243B2 (en) 2004-09-10 2008-07-22 Dionex Corporation Organosilanes and substrate bonded with same
US7468130B2 (en) * 2005-02-15 2008-12-23 Dionex Corporation Organosilanes and substrates covalently bonded with same and methods for synthesis and use same
US7557232B2 (en) * 2007-05-25 2009-07-07 Dionex Corporation Compositions useful as chromatography stationary phases
US9314712B2 (en) 2008-05-09 2016-04-19 Dionex Corporation Functionalized substrates with ion-exchange properties
CN102939140B (zh) 2010-05-19 2015-05-20 迪奥内克斯公司 具有芳香族堆积特性的官能化的基质
EP2675560B1 (en) 2011-02-14 2019-08-28 Dionex Corporation Liquid chromatographic column including a ligand comprising a polyhedral oligomeric silsequioxane moiety, and liquid chromatografic method using the column
CN104428045B (zh) 2012-05-15 2017-12-01 沃特世科技公司 色谱材料
CN111644164B (zh) * 2012-05-15 2024-03-08 沃特世科技公司 用于分离不饱和分子的色谱材料
SG11201404681VA (en) 2012-09-17 2014-09-26 Grace W R & Co Chromatography media and devices
US9610576B2 (en) 2012-09-27 2017-04-04 Agilent Technologies, Inc. Hydrolytically stable ion-exchange stationary phases and uses thereof
CN103357390A (zh) * 2012-11-12 2013-10-23 北京迪马欧泰科技发展中心 多层结构键合硅胶液相色谱填料及其合成方法
US9169331B2 (en) 2012-12-21 2015-10-27 Dionex Corporation Separation of glycans by mixed-mode liquid chromatography
EP2745904B1 (en) 2012-12-21 2015-12-16 Dionex Corporation HILIC/Anion-Exchange/Cation-Exchange Multimodal Media
US9310344B2 (en) 2013-06-14 2016-04-12 Dionex Corporation HILIC/anion-exchange/cation-exchange multimodal media
CN103170311A (zh) * 2013-03-20 2013-06-26 华东理工大学 新型氨基系列色谱固定相及制备方法
EP3936226A3 (en) 2013-06-11 2022-03-16 Waters Technologies Corporation Chromatographic columns and separation devices comprising a superficially porous material; and use thereof for supercritical fluid chromatography and other chromatography
CN107847907A (zh) 2014-05-02 2018-03-27 格雷斯公司 官能化载体材料以及制备和使用官能化载体材料的方法
WO2016115101A1 (en) 2015-01-15 2016-07-21 Dionex Corporation Chromatographic material having improved ph stability, method for preparation thereof and uses thereof
US10695744B2 (en) 2015-06-05 2020-06-30 W. R. Grace & Co.-Conn. Adsorbent biprocessing clarification agents and methods of making and using the same
US10618920B2 (en) 2016-06-03 2020-04-14 Agilent Technologies, Inc. Functionalized particles having modified phases
US20190126167A1 (en) 2017-11-01 2019-05-02 Dionex Corporation Sulfonamide based anion exchange resins
CN111135808B (zh) * 2019-12-30 2023-03-31 纳谱分析技术(苏州)有限公司 硅化合物、固定相及其应用

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE623601A (enExample) * 1961-10-16 1900-01-01
DE2250921A1 (de) 1972-10-18 1974-04-25 Dynamit Nobel Ag Neue silane von sulfon- und phosphorsaeureamiden
DE2357184A1 (de) * 1973-11-16 1975-05-22 Merck Patent Gmbh Verfahren zur herstellung von organisch modifizierten siliciumdioxiden
DE2641201A1 (de) * 1976-09-14 1978-03-16 Consortium Elektrochem Ind Diorganopolysiloxane enthaltende gemische und verfahren zu ihrer herstellung
US4584138A (en) * 1983-09-30 1986-04-22 Union Carbide Corporation Novel fatty ethenoid acylaminoorganosilicon compounds and their use as a coupling agent
DE3424534A1 (de) * 1984-07-04 1986-01-09 Degussa Ag, 6000 Frankfurt N,n'- und n,n',n'-substituierte silylharnstoffe und verfahren zu deren herstellung
US4705725A (en) * 1986-11-28 1987-11-10 E. I. Du Pont De Nemours And Company Substrates with sterically-protected, stable, covalently-bonded organo-silane films
DE3706521A1 (de) * 1987-02-28 1988-09-08 Degussa Benzoylthioharnstoffgruppen-haltige organosilane, verfahren zu ihrer herstellung
DE3821465A1 (de) * 1988-06-25 1989-12-28 Degussa Verfahren zur herstellung ein- oder mehrfach substituierter organyloxysilylfunktioneller thioharnstoffe und diese verbindungen
JPH0219387A (ja) * 1988-07-08 1990-01-23 Toshiba Silicone Co Ltd 有機ケイ素化合物およびその製造方法
US4990641A (en) * 1988-07-08 1991-02-05 Toshiba Silicone Co., Ltd. Organosilicon compound and its preparing method
JPH02107650A (ja) * 1988-10-17 1990-04-19 Toshiba Silicone Co Ltd 無機ケイ素質充填剤用処理剤
DE3837415A1 (de) * 1988-11-04 1990-05-10 Degussa Organopolysiloxan-harnstoff- und organopolysiloxan-thioharnstoff-derivate, verfahren zu ihrer herstellung und verwendung
US5290440A (en) 1992-06-23 1994-03-01 Research Corporation Technologies, Inc. High performance chiral selector
US5374755A (en) * 1992-07-17 1994-12-20 Millipore Corporation Liquid chromatography stationary phases with reduced silanol interactions
US5523443A (en) 1992-10-13 1996-06-04 Caschem, Inc. Dual curing conformal coatings
US5888491A (en) 1993-12-06 1999-03-30 Minnesota Mining And Manufacturing Company Optionally crosslinkable coatings, compositions and methods of use
CA2222137A1 (en) * 1995-06-05 1996-12-12 Basil V. Gregorovich Coating composition containing silane functionality
DE69721748T2 (de) * 1996-12-30 2004-03-11 Hydro-Québec, Montréal Oberflächenmodifizierte kohlenstoffmaterialien
DE19756831A1 (de) * 1997-12-19 1999-07-01 Wacker Chemie Gmbh Siliciumdioxid, das an seiner Oberfläche teil- oder vollständig silylierte Polykieselsäureketten trägt
JPH11335380A (ja) 1998-05-22 1999-12-07 Nitto Boseki Co Ltd 耐水性向上シランカップリング剤
US6262216B1 (en) * 1998-10-13 2001-07-17 Affymetrix, Inc. Functionalized silicon compounds and methods for their synthesis and use
EP1163050B1 (en) 1999-02-05 2007-01-03 Waters Investments Limited Preparation of porous inorganic/organic hybrid particles for chromatographic separations
JP4387518B2 (ja) 1999-10-18 2009-12-16 日東電工株式会社 接着剤組成物
US6528167B2 (en) * 2001-01-31 2003-03-04 Waters Investments Limited Porous hybrid particles with organic groups removed from the surface
US6800777B2 (en) * 2001-05-03 2004-10-05 Gelest, Inc. Trialkylsilanes for use in chromatographic applications, substrates including such compounds and methods of producing the same
US6645378B1 (en) * 2002-03-05 2003-11-11 Dionex Corporation Polar silanes and their use on silica supports
DE10393599T5 (de) * 2002-10-30 2005-10-27 Waters Investments Ltd., New Castle Poröse anorganische/organische Homogene copolymerische Hybridmaterialien für chromatographische Auftrennungen und Verfahren für deren Herstellung

Also Published As

Publication number Publication date
CA2544636A1 (en) 2005-05-26
WO2005047886A1 (en) 2005-05-26
KR20060125788A (ko) 2006-12-06
JP2007510644A (ja) 2007-04-26
EP1680432B1 (en) 2014-08-20
EP1680432A1 (en) 2006-07-19
AU2004288994A1 (en) 2005-05-26
CN1901990B (zh) 2013-04-03
US7074491B2 (en) 2006-07-11
US20050095440A1 (en) 2005-05-05
CN1901990A (zh) 2007-01-24
AU2004288994B2 (en) 2011-07-14

Similar Documents

Publication Publication Date Title
JP4904161B2 (ja) 基材結合用の極性シラン及び結合された基材のクロマトグラフィーにおける使用
JP4282324B2 (ja) 表面から有機基を取り除いた多孔質混成物粒子
CN1917953B (zh) 用于色谱分离的极性改性的键合相材料
US4705725A (en) Substrates with sterically-protected, stable, covalently-bonded organo-silane films
EP0437912B1 (en) Method for producing dual zone materials by use of an organosilane mixture
JPH0626666B2 (ja) ビデンテート シラン変性構造表面
JP6869181B2 (ja) 改善されたpH安定性を有するクロマトグラフィー材料、その調製法、及びその使用
CA2477782C (en) Polar silanes and their use on silica supports
WO2003078159A1 (en) Silica-based materials and methods
US7534352B2 (en) Reversed endcapping and bonding of chromatographic stationary phases using hydrosilanes
KR100638478B1 (ko) 이치환 쿠커비투릴이 결합된 실리카겔
Kricheldorf Chemical modification of polymers and surfaces

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20070228

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20070228

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20100405

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20100705

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20100712

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20101005

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20101122

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20110222

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20110224

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20110301

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20111212

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20120106

R150 Certificate of patent or registration of utility model

Ref document number: 4904161

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20150113

Year of fee payment: 3

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term