ATE212330T1 - Batch-gross-verfahren zur herstellung von diazomethan - Google Patents

Batch-gross-verfahren zur herstellung von diazomethan

Info

Publication number
ATE212330T1
ATE212330T1 AT98203801T AT98203801T ATE212330T1 AT E212330 T1 ATE212330 T1 AT E212330T1 AT 98203801 T AT98203801 T AT 98203801T AT 98203801 T AT98203801 T AT 98203801T AT E212330 T1 ATE212330 T1 AT E212330T1
Authority
AT
Austria
Prior art keywords
diazomethane
reaction vessel
phase
maintained
less
Prior art date
Application number
AT98203801T
Other languages
English (en)
Inventor
Thomas G Archibald
Der-Shing Huang
Mark H Pratton
James C Barnard
Original Assignee
Aerojet Fine Chemicals Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aerojet Fine Chemicals Llc filed Critical Aerojet Fine Chemicals Llc
Application granted granted Critical
Publication of ATE212330T1 publication Critical patent/ATE212330T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C245/00—Compounds containing chains of at least two nitrogen atoms with at least one nitrogen-to-nitrogen multiple bond
    • C07C245/12—Diazo compounds, i.e. compounds having the free valencies of >N2 groups attached to the same carbon atom
    • C07C245/14—Diazo compounds, i.e. compounds having the free valencies of >N2 groups attached to the same carbon atom having diazo groups bound to acyclic carbon atoms of a carbon skeleton
    • C07C245/16—Diazomethane

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Saccharide Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
AT98203801T 1997-11-13 1998-11-11 Batch-gross-verfahren zur herstellung von diazomethan ATE212330T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/970,035 US5817778A (en) 1997-11-13 1997-11-13 Large scale batch process for diazomethane

Publications (1)

Publication Number Publication Date
ATE212330T1 true ATE212330T1 (de) 2002-02-15

Family

ID=25516336

Family Applications (1)

Application Number Title Priority Date Filing Date
AT98203801T ATE212330T1 (de) 1997-11-13 1998-11-11 Batch-gross-verfahren zur herstellung von diazomethan

Country Status (6)

Country Link
US (1) US5817778A (de)
EP (1) EP0916649B1 (de)
JP (1) JP3017982B2 (de)
AT (1) ATE212330T1 (de)
BR (1) BR9804639A (de)
DE (1) DE69803538T2 (de)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6605732B1 (en) * 1999-05-03 2003-08-12 Aerojet Fine Chemicals Llc Clean, high-yield preparation of S,S and R,S amino acid isosteres
GB2357501B (en) * 1999-12-23 2001-11-28 Phoenix Chemicals Ltd Generation of diazomethane
DE102004030371A1 (de) * 2004-06-23 2006-01-19 Dynamit Nobel Gmbh Verfahren zur Herstellung von gasförmigen Diazoalkanen
GB0619395D0 (en) * 2006-10-02 2006-11-08 Almac Sciences Ltd Soluble diazoalkane precursors
CN101844063B (zh) * 2010-06-24 2013-09-25 凯莱英医药集团（天津）股份有限公司 一种大批量连续安全生产重氮甲烷反应器及其工作方法
GB201201066D0 (en) 2012-01-23 2012-03-07 Bakhu Ltd A method for the preparation of diazoalkanes
CN104557606B (zh) * 2013-10-18 2017-06-30 中国石油化工股份有限公司 一种利用重氮甲烷甲基化的方法
US9233924B2 (en) 2014-03-11 2016-01-12 Ampac Fine Chemicals Llc Methods for preparing D-threo methylphenidate using diazomethane, and compositions thereof
KR20210124350A (ko) 2019-05-21 2021-10-14 아심켐 래보러토리즈 (톈진) 컴퍼니, 리미티드 디아조메탄의 제조 공정

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6351366A (ja) * 1986-08-21 1988-03-04 Kurita Water Ind Ltd ジアゾメタンのエ−テル溶液の製造方法
US5459243A (en) * 1994-03-10 1995-10-17 Isis Pharmaceuticals, Inc. Apparatus and processes for the large scale generation and transfer of diazomethane

Also Published As

Publication number Publication date
EP0916649A1 (de) 1999-05-19
EP0916649B1 (de) 2002-01-23
DE69803538D1 (de) 2002-03-14
DE69803538T2 (de) 2002-08-08
JP3017982B2 (ja) 2000-03-13
JPH11228516A (ja) 1999-08-24
US5817778A (en) 1998-10-06
BR9804639A (pt) 2001-03-20

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