ATE212329T1 - Kontinuierliches verfahren zur herstellung von diazomethan - Google Patents

Kontinuierliches verfahren zur herstellung von diazomethan

Info

Publication number
ATE212329T1
ATE212329T1 AT98203800T AT98203800T ATE212329T1 AT E212329 T1 ATE212329 T1 AT E212329T1 AT 98203800 T AT98203800 T AT 98203800T AT 98203800 T AT98203800 T AT 98203800T AT E212329 T1 ATE212329 T1 AT E212329T1
Authority
AT
Austria
Prior art keywords
organic
phase
continuously
product mixture
aqueous
Prior art date
Application number
AT98203800T
Other languages
English (en)
Inventor
Thomas G Archibald
James C Barnard
Harlan F Reese
Original Assignee
Aerojet Fine Chemicals Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aerojet Fine Chemicals Llc filed Critical Aerojet Fine Chemicals Llc
Application granted granted Critical
Publication of ATE212329T1 publication Critical patent/ATE212329T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C245/00—Compounds containing chains of at least two nitrogen atoms with at least one nitrogen-to-nitrogen multiple bond
    • C07C245/12—Diazo compounds, i.e. compounds having the free valencies of >N2 groups attached to the same carbon atom
    • C07C245/14—Diazo compounds, i.e. compounds having the free valencies of >N2 groups attached to the same carbon atom having diazo groups bound to acyclic carbon atoms of a carbon skeleton
    • C07C245/16—Diazomethane

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
AT98203800T 1997-11-13 1998-11-11 Kontinuierliches verfahren zur herstellung von diazomethan ATE212329T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/969,993 US5854405A (en) 1997-11-13 1997-11-13 Continuous process for diazomethane from an n-methyl-n-nitrosoamine and from methylurea through n-methyl-n-nitrosourea

Publications (1)

Publication Number Publication Date
ATE212329T1 true ATE212329T1 (de) 2002-02-15

Family

ID=25516271

Family Applications (1)

Application Number Title Priority Date Filing Date
AT98203800T ATE212329T1 (de) 1997-11-13 1998-11-11 Kontinuierliches verfahren zur herstellung von diazomethan

Country Status (6)

Country Link
US (1) US5854405A (de)
EP (1) EP0916648B1 (de)
JP (1) JP3294560B2 (de)
AT (1) ATE212329T1 (de)
BR (1) BR9804629A (de)
DE (1) DE69803537T2 (de)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6605732B1 (en) * 1999-05-03 2003-08-12 Aerojet Fine Chemicals Llc Clean, high-yield preparation of S,S and R,S amino acid isosteres
GB2357501B (en) * 1999-12-23 2001-11-28 Phoenix Chemicals Ltd Generation of diazomethane
DE102004030371A1 (de) * 2004-06-23 2006-01-19 Dynamit Nobel Gmbh Verfahren zur Herstellung von gasförmigen Diazoalkanen
CN101844063B (zh) * 2010-06-24 2013-09-25 凯莱英医药集团（天津）股份有限公司 一种大批量连续安全生产重氮甲烷反应器及其工作方法
CN103189346B (zh) * 2010-11-01 2015-11-25 帝斯曼知识产权资产管理有限公司 重氮化合物的连续生产和反应
GB201318886D0 (en) * 2013-10-25 2013-12-11 Givaudan Sa Improvements i or relating to organic compounds
GB201318894D0 (en) 2013-10-25 2013-12-11 Givaudan Sa Improvements in or relating to organic compounds
US9233924B2 (en) 2014-03-11 2016-01-12 Ampac Fine Chemicals Llc Methods for preparing D-threo methylphenidate using diazomethane, and compositions thereof
GB201516396D0 (en) 2015-09-16 2015-10-28 Givaudan Sa Improvements in or relating to organic compounds
GB201810514D0 (en) 2018-06-27 2018-08-15 Givaudan Sa Improvements in or relating to organic compounds
KR20210124350A (ko) 2019-05-21 2021-10-14 아심켐 래보러토리즈 (톈진) 컴퍼니, 리미티드 디아조메탄의 제조 공정
CN110078637B (zh) * 2019-05-21 2022-08-30 凯莱英医药集团（天津）股份有限公司 重氮甲烷的制备工艺
JP7441863B2 (ja) * 2019-07-02 2024-03-01 アシムケム ラボラトリーズ （ティエンジン） カンパニー リミテッド シクロプロパン系化合物の連続合成方法及び装置
WO2022044038A1 (en) * 2020-08-24 2022-03-03 Council Of Scientific And Industrial Research Automated diazomethane generator, reactor and solid phase quencher

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1033671B (de) * 1957-04-02 1958-07-10 Phrix Werke Ag Verfahren zur Herstellung von Diazomethan
JPS54103803A (en) * 1978-02-02 1979-08-15 Minoru Sekiya Nn**nnnitrosoalkylamino*methyl*carbamic acid ester*its manufacture and diazoalkane formation using said compound
JPS6178758A (ja) * 1984-09-27 1986-04-22 Taoka Chem Co Ltd ジアゾメタン誘導体の製造方法
JPS6351366A (ja) * 1986-08-21 1988-03-04 Kurita Water Ind Ltd ジアゾメタンのエ−テル溶液の製造方法
US5459243A (en) * 1994-03-10 1995-10-17 Isis Pharmaceuticals, Inc. Apparatus and processes for the large scale generation and transfer of diazomethane

Also Published As

Publication number Publication date
DE69803537D1 (de) 2002-03-14
EP0916648A1 (de) 1999-05-19
US5854405A (en) 1998-12-29
EP0916648B1 (de) 2002-01-23
JPH11209330A (ja) 1999-08-03
DE69803537T2 (de) 2002-08-08
BR9804629A (pt) 2001-03-20
JP3294560B2 (ja) 2002-06-24

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