AR108817A1 - Métodos para fabricar ciertas sulfiliminas sustituidas - Google Patents

Métodos para fabricar ciertas sulfiliminas sustituidas

Info

Publication number
AR108817A1
AR108817A1 ARP170101685A ARP170101685A AR108817A1 AR 108817 A1 AR108817 A1 AR 108817A1 AR P170101685 A ARP170101685 A AR P170101685A AR P170101685 A ARP170101685 A AR P170101685A AR 108817 A1 AR108817 A1 AR 108817A1
Authority
AR
Argentina
Prior art keywords
methods
continuous loop
better
sulfilimine
formula
Prior art date
Application number
ARP170101685A
Other languages
English (en)
Inventor
Aaron A Shinkle
Kurt D Olson
Original Assignee
Dow Agrosciences Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Agrosciences Llc filed Critical Dow Agrosciences Llc
Publication of AR108817A1 publication Critical patent/AR108817A1/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/28—Radicals substituted by singly-bound oxygen or sulphur atoms
    • C07D213/32—Sulfur atoms
    • C07D213/34—Sulfur atoms to which a second hetero atom is attached
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/242—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/2435—Loop-type reactors
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/54—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/57—Nitriles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00085—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00177—Controlling or regulating processes controlling the pH
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

Se proporcionan métodos y/o sistemas para convertir intermedios de sulfuro en sulfiliminas usando una serie de reactores de bucle continuo en vez de un reactor de lote. Las ventajas de los métodos y sistemas proporcionados incluyen mejor rendimiento total, mejor gestión del calor, mejor mezcla de fases y/o mejor gestión de volumen. Un método para preparar una sulfilimina de fórmula (1), donde X representa halógeno, alquilo C₁₋₄ o haloalquilo C₁₋₄; que comprende (a) mezclar una solución de cianamida, una solución de hipoclorito y un solvente en un primer reactor de bucle continuo; (b) transferir la mezcla del Paso (a) a un segundo reactor de bucle continuo; (c) agregar un sulfuro de fórmula (2) al segundo reactor de bucle continuo que reacciona con la mezcla del Paso (a) para formar la sulfilimina, donde X es como se define anteriormente y (d) decantar la fase acuosa dando una fase orgánica que contiene una sulfilimina de fórmula (1).
ARP170101685A 2016-06-21 2017-06-19 Métodos para fabricar ciertas sulfiliminas sustituidas AR108817A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US201662352699P 2016-06-21 2016-06-21

Publications (1)

Publication Number Publication Date
AR108817A1 true AR108817A1 (es) 2018-09-26

Family

ID=60661163

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP170101685A AR108817A1 (es) 2016-06-21 2017-06-19 Métodos para fabricar ciertas sulfiliminas sustituidas

Country Status (12)

Country Link
US (1) US10214488B2 (es)
EP (1) EP3475259B1 (es)
CN (1) CN109311814B (es)
AR (1) AR108817A1 (es)
AU (1) AU2017280953B2 (es)
BR (1) BR112018074523B8 (es)
CA (1) CA3025879C (es)
ES (1) ES2836450T3 (es)
HU (1) HUE051823T2 (es)
IL (1) IL263300B (es)
TW (1) TWI735573B (es)
WO (1) WO2017222924A1 (es)

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI395736B (zh) * 2006-11-08 2013-05-11 Dow Agrosciences Llc 作為殺蟲劑之雜芳基（取代的）烷基ｎ-取代的磺醯亞胺（二）
DK2114886T3 (da) * 2007-02-26 2014-06-30 Dow Agrosciences Llc Fremgangsmåde til fremstilling af visse substituerede sulfiliminer
ES2625106T3 (es) * 2012-02-16 2017-07-18 Dow Agrosciences Llc Métodos de producción de compuestos de sulfilimina
JP2016504304A (ja) * 2012-12-11 2016-02-12 ダウ アグロサイエンシィズ エルエルシー ｜ｎ−シアノ−ｓ−［１−（ピリジン−３−イル）エチル］−ｓ−メチルスルフィルイミンの改良された製造方法

Also Published As

Publication number Publication date
EP3475259A1 (en) 2019-05-01
CN109311814B (zh) 2022-10-11
CA3025879A1 (en) 2017-12-28
TW201800394A (zh) 2018-01-01
ES2836450T3 (es) 2021-06-25
IL263300A (en) 2018-12-31
US10214488B2 (en) 2019-02-26
BR112018074523A2 (pt) 2019-03-06
BR112018074523B8 (pt) 2023-05-16
WO2017222924A1 (en) 2017-12-28
AU2017280953A1 (en) 2018-11-22
CA3025879C (en) 2023-10-03
IL263300B (en) 2019-11-28
AU2017280953B2 (en) 2019-08-22
BR112018074523B1 (pt) 2022-08-23
US20170362177A1 (en) 2017-12-21
CN109311814A (zh) 2019-02-05
HUE051823T2 (hu) 2021-03-29
EP3475259A4 (en) 2020-03-11
TWI735573B (zh) 2021-08-11
EP3475259B1 (en) 2020-09-23

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