AR082838A1 - Proceso de refinacion de sustancias quimicas a partir de aguas residuales de molinos de pasta y de papel - Google Patents

Proceso de refinacion de sustancias quimicas a partir de aguas residuales de molinos de pasta y de papel

Info

Publication number
AR082838A1
AR082838A1 ARP110101173A ARP110101173A AR082838A1 AR 082838 A1 AR082838 A1 AR 082838A1 AR P110101173 A ARP110101173 A AR P110101173A AR P110101173 A ARP110101173 A AR P110101173A AR 082838 A1 AR082838 A1 AR 082838A1
Authority
AR
Argentina
Prior art keywords
condensate
interest
compound
insoluble material
extract containing
Prior art date
Application number
ARP110101173A
Other languages
English (en)
Inventor
Craig Brennan Milestone
Deborah L Maclatchy
Mark Hewitt
Original Assignee
Ca Minister Environment
Craig Brennan Milestone
Deborah L Maclatchy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ca Minister Environment, Craig Brennan Milestone, Deborah L Maclatchy filed Critical Ca Minister Environment
Publication of AR082838A1 publication Critical patent/AR082838A1/es

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00—Purification; Separation; Stabilisation; Use of additives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/26—Multiple-effect evaporating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0492—Applications, solvents used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/42—Selective adsorption, e.g. chromatography characterised by the development mode, e.g. by displacement or by elution
    • B01D15/424—Elution mode
    • B01D15/426—Specific type of solvent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/025—Reverse osmosis; Hyperfiltration
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/048—Purification of waste water by evaporation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/36—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/38—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/79—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/005—Processes comprising at least two steps in series
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/10—Purification; Separation; Use of additives by extraction, i.e. purification or separation of liquid hydrocarbons with the aid of liquids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/08—Specific process operations in the concentrate stream
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/18—Details relating to membrane separation process operations and control pH control
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/26—Further operations combined with membrane separation processes
    • B01D2311/2626—Absorption or adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/26—Further operations combined with membrane separation processes
    • B01D2311/2649—Filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/26—Further operations combined with membrane separation processes
    • B01D2311/2676—Centrifugal separation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/26—Nature of the water, waste water, sewage or sludge to be treated from the processing of plants or parts thereof
    • C02F2103/28—Nature of the water, waste water, sewage or sludge to be treated from the processing of plants or parts thereof from the paper or cellulose industry
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
    • C07C2602/14—All rings being cycloaliphatic
    • C07C2602/26—All rings being cycloaliphatic the ring system containing ten carbon atoms
    • C07C2602/28—Hydrogenated naphthalenes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Analytical Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Nanotechnology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Paper (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Compounds Of Unknown Constitution (AREA)

Abstract

Proceso para aislar al menos un compuesto de interés, tal como manool, geranil linalool, etil guayacol, eugenol, veratraldehído, escualeno, terpina, colesterol, b-sitosterol, campesterol, estigmasterol, estigmastenol y ácido deshidroabiético, a partir de una biomasa, donde dicho proceso incluye los pasos de: obtener un condensado proveniente de un evaporador de recuperación, un retentato de ósmosis inversa de un condensado de un molino de pasta y papel, o ambos; donde el condensado, el retentato o ambos están sustancialmente libres de materiales de celulosa y/o lignina y/o derivados de lignina de mayor peso molecular (aproximadamente > 1000 Da); opcionalmente ajustar el pH y filtrar el condensado para recolectar el material insoluble; extraer el condensado, el material insoluble recolectado, o ambos, mediante una extracción en fase sólida (SPE), extracción líquido-líquido o extracción sólido-líquido para producir un extracto que contiene dicho al menos un compuesto de interés; y opcionalmente purificar el extracto que contiene dicho al menos un compuesto de interés por fraccionamiento térmico, separación cromatográfica, recristalización por intercambio iónico, quelación, adsorción/desorción, liofilización y sublimación o combinaciones de los mismos. El método es de particular utilidad para aislar los compuestos de interés a partir de las aguas residuales producidas en un molino de pasta y papel kraft, especialmente a partir de los condensados de los evaporadores de recuperación producidos durante el tratamiento del licor negro.
ARP110101173A 2010-04-07 2011-04-07 Proceso de refinacion de sustancias quimicas a partir de aguas residuales de molinos de pasta y de papel AR082838A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US32158210P 2010-04-07 2010-04-07

Publications (1)

Publication Number Publication Date
AR082838A1 true AR082838A1 (es) 2013-01-16

Family

ID=44676632

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP110101173A AR082838A1 (es) 2010-04-07 2011-04-07 Proceso de refinacion de sustancias quimicas a partir de aguas residuales de molinos de pasta y de papel

Country Status (13)

Country Link
US (3) US8993809B2 (es)
EP (1) EP2556041B1 (es)
AR (1) AR082838A1 (es)
AU (1) AU2011238386B2 (es)
BR (1) BR112012025704B1 (es)
CA (1) CA2795642C (es)
CL (1) CL2012002807A1 (es)
ES (1) ES2701027T3 (es)
NZ (2) NZ603328A (es)
PT (1) PT2556041T (es)
RU (1) RU2599639C2 (es)
UY (1) UY33321A (es)
WO (1) WO2011123948A1 (es)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR112014026267A2 (pt) * 2012-04-26 2017-06-27 Archer Daniels Midland Co método para processar biomassa lignocelulósica; composição; e composição obtida pelo método
CN105019291A (zh) * 2015-08-11 2015-11-04 怀宁县天元纸业有限公司 一种造纸黑液处理方法
CN109134184B (zh) * 2017-06-16 2021-03-19 中国科学院上海药物研究所 二萜类化合物、其制备方法及用途
CN107389410A (zh) * 2017-08-24 2017-11-24 山东省城市供排水水质监测中心 一种水中痕量有机污染物的分类提取检测方法
CN107478496A (zh) * 2017-08-24 2017-12-15 山东省城市供排水水质监测中心 一种水中有机磷的提取检测方法
CN107478795A (zh) * 2017-08-24 2017-12-15 山东省城市供排水水质监测中心 一种城市饮用水水体遗传毒性的检测方法
EP3722501A1 (de) * 2019-04-12 2020-10-14 Lenzing Aktiengesellschaft Verfahren zur rückgewinnung von alkalischer lösung, sowie verfahren zur herstellung regenerierter cellulosischer formkörper umfassend ein solches verfahren
AR122640A1 (es) * 2020-06-17 2022-09-28 Suzano Sa Método para tratar un condensado en un proceso de fabricación de pulpa
CN111751477B (zh) * 2020-07-01 2022-06-28 中国林业科学研究院亚热带林业研究所 一种测定植物油中角鲨烯和β-谷甾醇含量的方法
SE545943C2 (en) * 2021-07-02 2024-03-19 Soedra Skogsaegarna Ekonomisk Foerening Method for processing bark press water from sawmills and/or pulp mills
CN114460192A (zh) * 2022-01-21 2022-05-10 中科检测技术服务(广州)股份有限公司 一种固体废物中半挥发性有机污染物的快速筛查方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6110376A (en) 1998-02-09 2000-08-29 J. D. Irving, Limited Use of reverse osmosis membranes to treat evaporator clean condensate

Also Published As

Publication number Publication date
US20160326695A1 (en) 2016-11-10
RU2599639C2 (ru) 2016-10-10
EP2556041B1 (en) 2018-09-19
EP2556041A4 (en) 2015-08-05
NZ603328A (en) 2015-01-30
US9394211B2 (en) 2016-07-19
CA2795642C (en) 2018-12-04
UY33321A (es) 2011-09-30
BR112012025704B1 (pt) 2020-09-24
US8993809B2 (en) 2015-03-31
WO2011123948A8 (en) 2012-01-05
RU2012147024A (ru) 2014-05-20
AU2011238386A1 (en) 2012-11-22
BR112012025704A2 (pt) 2016-07-05
WO2011123948A1 (en) 2011-10-13
NZ702100A (en) 2016-07-29
CA2795642A1 (en) 2011-10-13
AU2011238386B2 (en) 2016-07-07
EP2556041A1 (en) 2013-02-13
CL2012002807A1 (es) 2013-03-22
US20150322627A1 (en) 2015-11-12
ES2701027T3 (es) 2019-02-20
PT2556041T (pt) 2018-12-14
US20130072724A1 (en) 2013-03-21

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