ZA200505981B - Method for recovery of zinc by countercurrent leaching - Google Patents
Method for recovery of zinc by countercurrent leaching Download PDFInfo
- Publication number
- ZA200505981B ZA200505981B ZA200505981A ZA200505981A ZA200505981B ZA 200505981 B ZA200505981 B ZA 200505981B ZA 200505981 A ZA200505981 A ZA 200505981A ZA 200505981 A ZA200505981 A ZA 200505981A ZA 200505981 B ZA200505981 B ZA 200505981B
- Authority
- ZA
- South Africa
- Prior art keywords
- stage
- leaching
- zinc
- concentrate
- iron
- Prior art date
Links
- 238000002386 leaching Methods 0.000 title claims description 123
- 238000000034 method Methods 0.000 title claims description 58
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 title claims description 55
- 239000011701 zinc Substances 0.000 title claims description 55
- 229910052725 zinc Inorganic materials 0.000 title claims description 55
- 238000011084 recovery Methods 0.000 title claims description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 162
- 229910052742 iron Inorganic materials 0.000 claims description 80
- 239000012141 concentrate Substances 0.000 claims description 70
- 229910052935 jarosite Inorganic materials 0.000 claims description 50
- 239000002253 acid Substances 0.000 claims description 47
- 230000007935 neutral effect Effects 0.000 claims description 43
- 238000001556 precipitation Methods 0.000 claims description 39
- 238000006243 chemical reaction Methods 0.000 claims description 32
- 239000007787 solid Substances 0.000 claims description 27
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims description 27
- 235000009529 zinc sulphate Nutrition 0.000 claims description 27
- 239000011686 zinc sulphate Substances 0.000 claims description 25
- 229910000859 α-Fe Inorganic materials 0.000 claims description 23
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 15
- 239000001301 oxygen Substances 0.000 claims description 15
- 229910052760 oxygen Inorganic materials 0.000 claims description 15
- 238000005868 electrolysis reaction Methods 0.000 claims description 12
- 239000002244 precipitate Substances 0.000 claims description 11
- 238000000746 purification Methods 0.000 claims description 9
- 239000005083 Zinc sulfide Substances 0.000 claims description 8
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 claims description 8
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 5
- 239000005864 Sulphur Substances 0.000 claims description 5
- 230000002378 acidificating effect Effects 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 4
- 238000005188 flotation Methods 0.000 claims description 4
- 229910021653 sulphate ion Inorganic materials 0.000 claims description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 3
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 claims description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 3
- 229910052787 antimony Inorganic materials 0.000 claims description 3
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 3
- 229910052732 germanium Inorganic materials 0.000 claims description 3
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 claims description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 3
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical class [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 3
- 235000010755 mineral Nutrition 0.000 claims description 3
- 239000011707 mineral Substances 0.000 claims description 3
- -1 ammonium ions Chemical class 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 1
- 239000002994 raw material Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 description 76
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical group [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 14
- 229910052598 goethite Inorganic materials 0.000 description 10
- AEIXRCIKZIZYPM-UHFFFAOYSA-M hydroxy(oxo)iron Chemical compound [O][Fe]O AEIXRCIKZIZYPM-UHFFFAOYSA-M 0.000 description 10
- 230000003647 oxidation Effects 0.000 description 10
- 238000007254 oxidation reaction Methods 0.000 description 10
- 238000006386 neutralization reaction Methods 0.000 description 8
- 239000011787 zinc oxide Substances 0.000 description 7
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 235000011149 sulphuric acid Nutrition 0.000 description 6
- 239000001117 sulphuric acid Substances 0.000 description 6
- 229910052595 hematite Inorganic materials 0.000 description 5
- 239000011019 hematite Substances 0.000 description 5
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 4
- 230000003472 neutralizing effect Effects 0.000 description 4
- 239000002562 thickening agent Substances 0.000 description 4
- 229910001308 Zinc ferrite Inorganic materials 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- WGEATSXPYVGFCC-UHFFFAOYSA-N zinc ferrite Chemical compound O=[Zn].O=[Fe]O[Fe]=O WGEATSXPYVGFCC-UHFFFAOYSA-N 0.000 description 3
- 239000003929 acidic solution Substances 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 229960004887 ferric hydroxide Drugs 0.000 description 2
- IEECXTSVVFWGSE-UHFFFAOYSA-M iron(3+);oxygen(2-);hydroxide Chemical compound [OH-].[O-2].[Fe+3] IEECXTSVVFWGSE-UHFFFAOYSA-M 0.000 description 2
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical group [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 description 2
- 229910052683 pyrite Inorganic materials 0.000 description 2
- 239000011028 pyrite Substances 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 150000004763 sulfides Chemical class 0.000 description 2
- CKPWHLGHHXSVJI-UHFFFAOYSA-N 3-fluoroethamphetamine Chemical compound CCNC(C)CC1=CC=CC(F)=C1 CKPWHLGHHXSVJI-UHFFFAOYSA-N 0.000 description 1
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000005569 Iron sulphate Substances 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 150000003868 ammonium compounds Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000011790 ferrous sulphate Substances 0.000 description 1
- 235000003891 ferrous sulphate Nutrition 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000014413 iron hydroxide Nutrition 0.000 description 1
- KFZAUHNPPZCSCR-UHFFFAOYSA-N iron zinc Chemical compound [Fe].[Zn] KFZAUHNPPZCSCR-UHFFFAOYSA-N 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 235000002020 sage Nutrition 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 150000003752 zinc compounds Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
- C22B3/08—Sulfuric acid, other sulfurated acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/04—Obtaining zinc by distilling
- C22B19/08—Obtaining zinc by distilling in blast furnaces
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/20—Obtaining zinc otherwise than by distilling
- C22B19/22—Obtaining zinc otherwise than by distilling with leaching with acids
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/20—Obtaining zinc otherwise than by distilling
- C22B19/26—Refining solutions containing zinc values, e.g. obtained by leaching zinc ores
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Environmental & Geological Engineering (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Electrolytic Production Of Metals (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FI20030285A FI116071B (sv) | 2003-02-26 | 2003-02-26 | Förfarande för tillvaratagande av zink med motströmsupplösning |
Publications (1)
Publication Number | Publication Date |
---|---|
ZA200505981B true ZA200505981B (en) | 2006-05-31 |
Family
ID=8565718
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ZA200505981A ZA200505981B (en) | 2003-02-26 | 2005-07-26 | Method for recovery of zinc by countercurrent leaching |
Country Status (18)
Country | Link |
---|---|
US (1) | US7517383B2 (sv) |
EP (1) | EP1597403B1 (sv) |
JP (1) | JP4511519B2 (sv) |
KR (1) | KR101084522B1 (sv) |
CN (1) | CN100572569C (sv) |
AT (1) | ATE389038T1 (sv) |
AU (1) | AU2004215197B2 (sv) |
BR (1) | BRPI0407700B1 (sv) |
CA (1) | CA2516411C (sv) |
DE (1) | DE602004012394T2 (sv) |
EA (1) | EA008362B1 (sv) |
ES (1) | ES2301973T3 (sv) |
FI (1) | FI116071B (sv) |
MX (1) | MXPA05008897A (sv) |
NO (1) | NO20054254L (sv) |
PE (1) | PE20041037A1 (sv) |
WO (1) | WO2004076698A1 (sv) |
ZA (1) | ZA200505981B (sv) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100361750C (zh) * | 2005-12-07 | 2008-01-16 | 冯国臣 | 硫精矿除杂提纯浮选工艺 |
FI118226B (sv) * | 2005-12-29 | 2007-08-31 | Outokumpu Technology Oyj | Förfarande för tillvaratagning av sällsynta metaller i en upplösningsprocess för zink |
FI122676B (sv) | 2010-10-12 | 2012-05-15 | Outotec Oyj | Förfarande för behandling av en zinksulfathaltig lösning |
KR101047986B1 (ko) * | 2010-11-26 | 2011-07-13 | 한국지질자원연구원 | Ccd 공정을 이용한 리튬 이온의 흡착/탈착 장치 및 그 방법 |
CN103210099A (zh) * | 2011-04-15 | 2013-07-17 | 泰姆5有限公司 | 从硫化锌精矿开始回收含硫介质中的锌的湿法冶金方法 |
CN102191371B (zh) * | 2011-04-18 | 2013-02-06 | 中南大学 | 一种传统锌湿法冶炼过程中铁锌分离的方法 |
FI123884B (sv) | 2011-11-08 | 2013-11-29 | Outotec Oyj | Förfarande för lakning av sulfidiskt metallkoncentrat |
MX2016003686A (es) * | 2013-09-20 | 2016-06-22 | Metaleach Ltd | Metodo para la lixiviacion de cinc a partir de menas incrustadas en carbonato. |
EP2902510A1 (en) * | 2014-01-29 | 2015-08-05 | Canbekte, Hüsnü Sinan | A new method for leaching of electric arc furnace dust (EAFD) with sulphuric acid |
CN105734290A (zh) * | 2016-03-29 | 2016-07-06 | 湖北大江环保科技股份有限公司 | 一种锌湿法冶金的除砷工艺 |
CN106048217B (zh) * | 2016-07-29 | 2018-06-29 | 四环锌锗科技股份有限公司 | 氧化锌粉的综合回收利用方法 |
RU2767385C1 (ru) * | 2021-02-18 | 2022-03-17 | Федеральное государственное автономное образовательное учреждение высшего образования "Балтийский федеральный университет имени Иммануила Канта" (БФУ им. И. Канта) | Способ переработки окисленной цинковой руды |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FI50097C (fi) * | 1973-02-12 | 1980-10-24 | Outokumpu Oy | Hydrometallurgiskt foerfarande foer aotervinning av zink koppar och kadmium fraon deras ferriter |
CA1090143A (en) * | 1976-01-26 | 1980-11-25 | Hans Reinhardt | Method of recovering zinc from a material containing zinc and iron |
CA1104837A (en) * | 1977-08-19 | 1981-07-14 | Donald R. Weir | Process for recovery of copper and zinc from complex sulfides |
LU78802A1 (fr) * | 1977-12-30 | 1979-07-20 | Prayon | Procede de traitement de residus de minerais de zinc ferriferes |
LU85385A1 (fr) * | 1984-05-28 | 1986-01-29 | Mines Fond Zinc Vieille | Procede de lixiviation de sulfures contenant du zinc et du fer |
FI88516C (sv) * | 1990-02-16 | 1993-05-25 | Outokumpu Oy | Hydrometallurgiskt förfarande för behandling av zinksulfidhaltiga råäm nen |
JP3713579B2 (ja) * | 1993-08-27 | 2005-11-09 | ユミコア ソシエテ アノニム | 硫化物濃縮物からの亜鉛の抽出方法 |
FI100806B (sv) * | 1996-08-12 | 1998-02-27 | Outokumpu Base Metals Oy | Förfarande för upplösning av zinkslig under atmosfäriska för hållanden |
JP2001021224A (ja) * | 1999-07-06 | 2001-01-26 | Tadao Nakano | 浴槽の対流改善装置 |
JP3911536B2 (ja) * | 2000-01-31 | 2007-05-09 | Dowaメタルマイン株式会社 | 亜鉛精鉱の浸出法 |
FI20002699A0 (sv) * | 2000-12-08 | 2000-12-08 | Outokumpu Oy | Förfarande för hydrolytisk utfällning av järn |
-
2003
- 2003-02-26 FI FI20030285A patent/FI116071B/sv not_active IP Right Cessation
-
2004
- 2004-02-24 WO PCT/FI2004/000085 patent/WO2004076698A1/en active IP Right Grant
- 2004-02-24 JP JP2006502070A patent/JP4511519B2/ja not_active Expired - Fee Related
- 2004-02-24 EA EA200500980A patent/EA008362B1/ru not_active IP Right Cessation
- 2004-02-24 AU AU2004215197A patent/AU2004215197B2/en not_active Ceased
- 2004-02-24 EP EP04713920A patent/EP1597403B1/en not_active Expired - Lifetime
- 2004-02-24 MX MXPA05008897A patent/MXPA05008897A/es active IP Right Grant
- 2004-02-24 AT AT04713920T patent/ATE389038T1/de not_active IP Right Cessation
- 2004-02-24 BR BRPI0407700A patent/BRPI0407700B1/pt not_active IP Right Cessation
- 2004-02-24 ES ES04713920T patent/ES2301973T3/es not_active Expired - Lifetime
- 2004-02-24 KR KR1020057016072A patent/KR101084522B1/ko not_active IP Right Cessation
- 2004-02-24 CN CNB2004800027969A patent/CN100572569C/zh not_active Expired - Fee Related
- 2004-02-24 US US10/544,272 patent/US7517383B2/en not_active Expired - Fee Related
- 2004-02-24 CA CA2516411A patent/CA2516411C/en not_active Expired - Fee Related
- 2004-02-24 DE DE602004012394T patent/DE602004012394T2/de not_active Expired - Lifetime
- 2004-02-25 PE PE2004000192A patent/PE20041037A1/es not_active Application Discontinuation
-
2005
- 2005-07-26 ZA ZA200505981A patent/ZA200505981B/en unknown
- 2005-09-14 NO NO20054254A patent/NO20054254L/no not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
PE20041037A1 (es) | 2005-01-18 |
US20060213332A1 (en) | 2006-09-28 |
FI116071B (sv) | 2005-09-15 |
FI20030285A0 (sv) | 2003-02-26 |
EA200500980A1 (ru) | 2006-04-28 |
CN1742104A (zh) | 2006-03-01 |
ES2301973T3 (es) | 2008-07-01 |
NO20054254L (no) | 2005-09-14 |
ATE389038T1 (de) | 2008-03-15 |
AU2004215197B2 (en) | 2009-08-27 |
JP4511519B2 (ja) | 2010-07-28 |
MXPA05008897A (es) | 2006-02-17 |
JP2006519309A (ja) | 2006-08-24 |
FI20030285A (sv) | 2004-08-27 |
DE602004012394T2 (de) | 2009-04-02 |
CA2516411A1 (en) | 2004-09-10 |
EP1597403B1 (en) | 2008-03-12 |
CN100572569C (zh) | 2009-12-23 |
US7517383B2 (en) | 2009-04-14 |
KR20050103512A (ko) | 2005-10-31 |
AU2004215197A1 (en) | 2004-09-10 |
KR101084522B1 (ko) | 2011-11-18 |
BRPI0407700B1 (pt) | 2015-12-22 |
BRPI0407700A (pt) | 2006-04-11 |
EP1597403A1 (en) | 2005-11-23 |
EA008362B1 (ru) | 2007-04-27 |
DE602004012394D1 (de) | 2008-04-24 |
CA2516411C (en) | 2013-07-02 |
WO2004076698A1 (en) | 2004-09-10 |
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