WO2024055341A1 - 一种纤维织物整理用涂料及其使用方法 - Google Patents

一种纤维织物整理用涂料及其使用方法 Download PDF

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WO2024055341A1
WO2024055341A1 PCT/CN2022/119833 CN2022119833W WO2024055341A1 WO 2024055341 A1 WO2024055341 A1 WO 2024055341A1 CN 2022119833 W CN2022119833 W CN 2022119833W WO 2024055341 A1 WO2024055341 A1 WO 2024055341A1
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fiber fabric
parts
waterproofing agent
stir
titanate coupling
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PCT/CN2022/119833
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English (en)
French (fr)
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谢佐鹏
朱克俭
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浙江泰斯德电气有限公司
温岭市电力绝缘器材有限公司
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Publication of WO2024055341A1 publication Critical patent/WO2024055341A1/zh

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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/10—Repellency against liquids
    • D06M2200/12—Hydrophobic properties
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments

Definitions

  • the invention belongs to the field of fabric coatings, and is specifically a coating for fiber fabric finishing and a method of using the coating.
  • the coating has functions such as waterproofing, breathability, UV protection, and anti-static.
  • CN1478949A discloses a coating used for finishing electrical insulation cloth, including in parts by weight: water: 100 parts, fluorocarbon surfactant: 3 to 7 parts, adhesive: 2 to 7 parts, catalyst: 0.5 ⁇ 1.2 servings.
  • the fluorocarbon surfactant is TG521 fluorocarbon surfactant;
  • the binder is melamine and KH560 silane coupling agent;
  • the catalyst uses triethylenetetramine; it also contains penetrant: isopropyl alcohol; it also contains dialkyl dimethyl Ammonium salt softener.
  • the fabric treated with this impregnation agent has good waterproof, oil-proof, and anti-fouling properties, it provides extremely convenient and reliable conditions for field operations, humid and rainy seasons.
  • the finishing cloth has poor air permeability and does not have anti-static function. In the context of increasing demands for improving work safety, there are still potential safety hazards.
  • the purpose of the present invention is to provide a waterproof, breathable, ultraviolet-proof, and anti-static coating for fiber fabric finishing. Its specific technical solutions are as follows:
  • a coating for fiber fabric finishing including the following components in parts by mass:
  • Nano titanium dioxide 4-6 parts.
  • waterproof agent is selected from one or more of waterproof agent AG-710, waterproof agent AG-7500, waterproof agent AG-7600, waterproof agent AG415, waterproof agent AG-950, and waterproof agent AG-E061.
  • the titanate coupling agent is preferably a chelating titanate coupling agent.
  • the particle size of the nano titanium dioxide is 10-12 nanometers.
  • a waterproofing agent to the silicone rubber emulsion, mix and stir, and gradually add nano-titanium dioxide in a mixer with a speed of not less than 300 rpm, disperse and stir for 30 minutes, then add titanate coupling agent, disperse and stir for not less than 60min, finally add water and stir for 30 minutes.
  • a method of using the coating for fiber fabric finishing includes the following steps:
  • Step 1 Fully wash the fiber fabric to be treated, and dry the washed fiber to remove moisture
  • Step 2 Dip the fiber fabric into the fiber fabric finishing coating described in one of claims 1-5, and continuously turn it over to allow it to be fully impregnated;
  • Step 3 Shake off the excess paint on the fully impregnated fiber fabric in a low-speed centrifuge, so that 70-75% of the liquid content of the fabric is retained;
  • Step 4 Put the dehydrated fiber fabric into the drying box and gradually heat it up, and turn on the fan to make the temperature of the drying box uniform, and then cool it with the furnace;
  • Step 5 Iron and shape the dried fiber fabric according to different materials and shapes.
  • step 1 the drying temperature is greater than 100°C and not less than 2 hours.
  • step 4 the drying temperature and time are as follows:
  • the present invention is a coating and a method of use that simultaneously endow fiber fabrics, especially clothing fabrics, with functions such as rainproof, breathable, UV-proof, and anti-static. It is a technological innovation in the multi-functional textile finishing industry. It includes complete usage methods such as textile purification treatment, coating formula and auxiliary materials, and temperature rise curve.
  • the coating for fiber fabric finishing in this implementation includes the following components in parts by mass:
  • the titanate coupling agent is preferably a chelating titanate coupling agent, and the nanometer titanium dioxide particle size is 10-12 nanometers.
  • Configuration method Add waterproof agent AG-710 to the silicone rubber emulsion, mix and stir, and gradually add nano-titanium dioxide into the mixer with a speed of not less than 300 rpm, disperse and stir for 30 minutes, then add titanate coupling agent, disperse and stir continuously. Less than 60 minutes, finally add water to disperse and stir for 30 minutes.
  • the coating for fiber fabric finishing in this implementation includes the following components in parts by mass:
  • the titanate coupling agent is preferably a chelating titanate coupling agent, and the nanometer titanium dioxide particle size is 10-12 nanometers.
  • Configuration method Add waterproofing agent AG-7500 to the silicone rubber emulsion, mix and stir, and gradually add nano-titanium dioxide into the mixer with a speed of not less than 300 rpm, disperse and stir for 30 minutes, then add titanate coupling agent, disperse and stir continuously. Less than 60 minutes, finally add water to disperse and stir for 30 minutes.
  • the coating for fiber fabric finishing in this implementation includes the following components in parts by mass:
  • the titanate coupling agent is preferably a chelating titanate coupling agent, and the nanometer titanium dioxide particle size is 10-12 nanometers.
  • Configuration method Add waterproofing agent AG-7600 to the silicone rubber emulsion, mix and stir, and gradually add nano-titanium dioxide into the mixer with a speed of not less than 300 rpm, disperse and stir for 30 minutes, then add titanate coupling agent, disperse and stir continuously. Less than 60 minutes, finally add water to disperse and stir for 30 minutes.
  • the coating for fiber fabric finishing in this implementation includes the following components in parts by mass:
  • the titanate coupling agent is preferably a chelating titanate coupling agent, and the nanometer titanium dioxide particle size is 10-12 nanometers.
  • Configuration method Add waterproofing agent AG415 to the silicone rubber emulsion, mix and stir, and gradually add nano titanium dioxide into the mixer with a speed of not less than 300 rpm, disperse and stir for 30 minutes, then add titanate coupling agent, disperse and stir for not less than 60min, finally add water and stir for 30 minutes.
  • the coating for fiber fabric finishing in this implementation includes the following components in parts by mass:
  • the titanate coupling agent is preferably a chelating titanate coupling agent, and the nanometer titanium dioxide particle size is 10-12 nanometers.
  • Configuration method Add waterproof agent AG-950 to the silicone rubber emulsion, mix and stir, and gradually add nano-titanium dioxide into the mixer with a speed of not less than 300 rpm, disperse and stir for 30 minutes, then add titanate coupling agent, disperse and stir continuously. Less than 60 minutes, finally add water to disperse and stir for 30 minutes.
  • the coating for fiber fabric finishing in this implementation includes the following components in parts by mass:
  • the titanate coupling agent is preferably a chelating titanate coupling agent, and the nanometer titanium dioxide particle size is 10-12 nanometers.
  • Configuration method Add waterproof agent AG-E061 to the silicone rubber emulsion, mix and stir, and gradually add nano-titanium dioxide into the mixer with a speed of not less than 300 rpm, disperse and stir for 30 minutes, then add titanate coupling agent, disperse and stir continuously. Less than 60 minutes, finally add water to disperse and stir for 30 minutes.
  • the invention also provides a method of using a coating for fiber fabric finishing, which is used for fiber fabric finishing, so that the fiber fabric has functions such as waterproof, breathable, ultraviolet protection, and anti-static. Includes the following steps:
  • Step 1 Fully wash the fiber fabric to be processed to remove the remaining materials in the fiber and fabric production process, such as release agent, dye, softener and other residues, to ensure the purity of the fiber fabric; at the same time, it is also necessary to Moisture content of fibers after drying and washing; drying temperature is greater than 100°C and not less than 2 hours;
  • Step 2 Dip the fiber fabric into the above-mentioned fiber fabric finishing coating, and keep turning it over to allow it to be fully impregnated;
  • Step 3 Shake off the excess paint on the fully impregnated fiber fabric in a low-speed centrifuge, so that 70-75% of the liquid content of the fabric is retained;
  • Step 4 Put the dehydrated fiber fabric into the drying box and gradually heat it up, and turn on the fan to make the temperature of the drying box uniform. Drying temperature and time are as follows:
  • Step 5 Iron and shape the dried fiber fabric according to different materials and shapes.
  • the treated fiber fabric is evaluated according to national standards and has good waterproof, breathable, anti-ultraviolet, and anti-static properties, and is very environmentally friendly.

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Paints Or Removers (AREA)

Abstract

一种纤维织物整理用涂料，包括以下质量份数的成分：水80-120份；防水剂7-11份；硅橡胶乳液8-15份；钛酸酯偶联剂1-3份；纳米二氧化钛4-6份。其使用方法包括如下步骤：步骤1：将待处理的纤维织物进行充分水洗，烘干；步骤2：将纤维织物浸入所述的纤维织物整理用涂料中，不断翻转，让其充分浸渍；步骤3：将充分浸渍的纤维织物在低转速的离心机上甩脱多余的涂料；步骤4：将脱液的纤维织物放入烘干箱中逐步升温，并打开风机，使烘干箱温度均匀，然后随炉冷却；步骤5：对烘干的纤维织物，根据材料、形状不同进行熨烫定型处理。

Description

一种纤维织物整理用涂料及其使用方法 技术领域
本发明属于织物涂料领域，具体是一种纤维织物整理用涂料及其使用方法，该涂料兼具防水透气、防紫外线、防静电等功能。
背景技术
在带电作业特别是高压带电作业时，作业人员的工作服质量、性能好坏，直接关系到线路畅通和人身安全。特别在潮湿或雨季的野外作业更需用具有多功能的工作服。现有作业人员的工作服一般使用纤维织物并在其上涂上涂层。
CN1478949A公开了一种用于电绝缘布整理的涂料，以重量份数比计包括：水：100份、氟碳表面活性剂：3～7份、粘合剂：2～7份、触媒：0.5～1.2份。氟碳表面活性剂是TG521型氟碳表面活性剂；粘合剂是三聚氰胺和KH560硅烷偶联剂；触媒使用三乙烯四胺；还含有浸透剂：异丙醇；还含有二烷基二甲基铵盐柔软剂。布料经该涂料整理后，电绝缘性能指标好，使整理过的布料适宜制作多种带电作业穿着的行业服装，为带电作业操作人员提供了安全保障。由于该浸剂整理过的布料尚有良好的防水、防油、防污性能，为野外作业，潮湿和雨季作业提供了极为方便可靠的条件。但是该整理布透气性较差，且不具有防静电的功能，在现在日益要求提高作业安全的背景下，还是存在安全隐患。
发明内容
为了解决现有技术中存在的上述技术问题，本发明的目的是提供一种具有防水透气、防紫外线、防静电的涂料，用于纤维织物整理。其具体技术方案如下：
一种纤维织物整理用涂料，包括以下质量份数的成分：
水80-120份；
防水剂7-11份；
硅橡胶乳液8-15份；
钛酸酯偶联剂1-3份；
纳米二氧化钛4-6份。
进一步的，所述防水剂选自防水剂AG-710、防水剂AG-7500、防水剂AG-7600、防水剂AG415、防水剂AG-950、防水剂AG-E061中的一种或几种。
进一步的，所述钛酸酯偶联剂优选为螯合型钛酸酯偶联剂。
进一步的，所述纳米二氧化钛粒径为10-12纳米。
进一步的，先在硅橡胶乳液加入防水剂混合搅拌，并用转速不少于300转/分钟的搅拌机中逐步加入纳米二氧化钛，分散搅拌30分钟，再加入钛酸酯偶联剂，分散搅拌不少于60min，最后加入水分散搅拌30分钟。
一种所述的纤维织物整理用涂料的使用方法，包括如下步骤：
步骤1：将待处理的纤维织物进行充分水洗，烘干水洗后纤维水分；
步骤2：将纤维织物浸入权利要求1-5之一所述的纤维织物整理用涂料中，不断翻转，让其充分浸渍；
步骤3：将充分浸渍的纤维织物在低转速的离心机上甩脱多余的涂料，使织物带液量保留70-75％；
步骤4：将脱液的纤维织物放入烘干箱中逐步升温，并打开风机，使烘干箱温度均匀，然后随炉冷却；
步骤5：对烘干的纤维织物，根据材料、形状不同进行熨烫定型处理。
进一步的，步骤1中，烘干温度大于100℃和不少于2个小时。
进一步的，步骤4中，烘干温度和时间如下：
1.常温→60℃，50min；
2. 60℃→110℃80min；
3. 110℃→160℃20min。
本发明是同时赋予纤维织物尤其是服装面料，同时具有防雨透气、防紫外线、防静电等功能的涂料及使用方法。属于纺织品多功能整理行业的科技创新。它包括纺织品纯净处理，涂料的配方和辅料的配合及温升曲线等完整的使用方法。
具体实施方式
以下对本发明的具体实施方式进行详细说明。应当理解的是，此处所描述的具体实施方式仅用于说明和解释本发明，并不用于限制本发明。
实施例1
本实施的纤维织物整理用涂料，包括以下质量份数的成分：
水80份；
防水剂AG-710 10份；
硅橡胶乳液12份；
钛酸酯偶联剂1份；
纳米二氧化钛5份；
其中钛酸酯偶联剂优选为螯合型钛酸酯偶联剂，纳米二氧化钛粒径为10-12纳米。
配置方法：在硅橡胶乳液加入防水剂AG-710混合搅拌，并用转速不少于300转/分钟的搅拌机中逐步加入纳米二氧化钛，分散搅拌30分钟，再加入钛酸酯偶联剂，分散搅拌不少于60min，最后加入水分散搅拌30分钟。
实施例2
本实施的纤维织物整理用涂料，包括以下质量份数的成分：
水100份；
防水剂AG-7500 11份；
硅橡胶乳液8份；
钛酸酯偶联剂13份；
纳米二氧化钛6份；
其中钛酸酯偶联剂优选为螯合型钛酸酯偶联剂，纳米二氧化钛粒径为10-12纳米。
配置方法：在硅橡胶乳液加入防水剂AG-7500混合搅拌，并用转速不少于300转/分钟的搅拌机中逐步加入纳米二氧化钛，分散搅拌30分钟，再加入钛酸酯偶联剂，分散搅拌不少于60min，最后加入水分散搅拌30分钟。
实施例3
本实施的纤维织物整理用涂料，包括以下质量份数的成分：
水120份；
防水剂AG-7600 7份；
硅橡胶乳液15份；
钛酸酯偶联剂2份；
纳米二氧化钛4份；
其中钛酸酯偶联剂优选为螯合型钛酸酯偶联剂，纳米二氧化钛粒径为10-12纳米。
配置方法：在硅橡胶乳液加入防水剂AG-7600混合搅拌，并用转速不少于300转/分钟的搅拌机中逐步加入纳米二氧化钛，分散搅拌30分钟，再加入钛酸酯偶联剂，分散搅拌不少于60min，最后加入水分散搅拌30分钟。
实施例4
本实施的纤维织物整理用涂料，包括以下质量份数的成分：
水110份；
防水剂AG415 9份；
硅橡胶乳液14份；
钛酸酯偶联剂3份；
纳米二氧化钛6份；
其中钛酸酯偶联剂优选为螯合型钛酸酯偶联剂，纳米二氧化钛粒径为10-12纳米。
配置方法：在硅橡胶乳液加入防水剂AG415混合搅拌，并用转速不少于300转/分钟的搅拌机中逐步加入纳米二氧化钛，分散搅拌30分钟，再加入钛酸酯偶联剂，分散搅拌不少于60min，最后加入水分散搅拌30分钟。
实施例5
本实施的纤维织物整理用涂料，包括以下质量份数的成分：
水85份；
防水剂AG-950 9份；
硅橡胶乳液10份；
钛酸酯偶联剂1份；
纳米二氧化钛6份；
其中钛酸酯偶联剂优选为螯合型钛酸酯偶联剂，纳米二氧化钛粒径为10-12纳米。
配置方法：在硅橡胶乳液加入防水剂AG-950混合搅拌，并用转速不少于300转/分钟的搅拌机中逐步加入纳米二氧化钛，分散搅拌30分钟，再加入钛酸酯偶联剂，分散搅拌不少于60min，最后加入水分散搅拌30分钟。
实施例6
本实施的纤维织物整理用涂料，包括以下质量份数的成分：
水110份；
防水剂AG-E061 11份；
硅橡胶乳液15份；
钛酸酯偶联剂3份；
纳米二氧化钛6份；
其中钛酸酯偶联剂优选为螯合型钛酸酯偶联剂，纳米二氧化钛粒径为10-12纳米。
配置方法：在硅橡胶乳液加入防水剂AG-E061混合搅拌，并用转速不少于300转/分钟的搅拌机中逐步加入纳米二氧化钛，分散搅拌30分钟，再加入钛酸酯偶联剂，分散搅拌不少于60min，最后加入水分散搅拌30分钟。
实施例7
本发明还提供了一种纤维织物整理用涂料的使用方法，用于纤维织物整理，使得纤维织物具防水透气、防紫外线、防静电等功能。包括如下步骤：
步骤1：将待处理的纤维织物进行充分水洗，以除去纤维及织物在生产过程中残留的材料，如脱模剂、染色剂、柔软剂等残留物，确保纤维织物的纯净；同时，也需要烘干水洗后纤维水分；烘干温度大于100℃和不少于2个小时；
步骤2：将纤维织物浸入上述纤维织物整理用涂料中，不断翻转，让其充分浸渍；
步骤3：将充分浸渍的纤维织物在低转速的离心机上甩脱多余的涂料，使织物带液量保留70-75％；
步骤4：将脱液的纤维织物放入烘干箱中逐步升温，并打开风机，使烘干箱温度均匀。烘干温度和时间如下：
1.常温→60℃，50min；
2. 60℃→110℃80min；
3. 110℃→160℃20min；
然后随炉冷却；
步骤5：对烘干的纤维织物，根据材料、形状不同进行熨烫定型处理。
经处理后的纤维织物，按国标测评，具有良好的防水透气、防紫外线、防静电性能，且非常环保。
以上实施例仅用以说明本发明的技术方案，而非对其限制；尽管参照前述实施例对本发明进行了详细的说明，本领域的普通技术人员应当理解：其依然可以对前述实施例所记载的技术方案进行修改，或者对其中部分或者全部技术特征进行等同替换；而这些修改或者替换，并不使相应技术方案的本质脱离本发明实施例技术方案的范围。

Claims (8)

  1. 一种纤维织物整理用涂料，包括以下质量份数的成分：
    水80-120份；
    防水剂7-11份；
    硅橡胶乳液8-15份；
    钛酸酯偶联剂1-3份；
    纳米二氧化钛4-6份。
  2. 根据权利要求1所述的纤维织物整理用涂料，其特征在于：
    所述防水剂选自防水剂AG-710、防水剂AG-7500、防水剂AG-7600、防水剂AG415、防水剂AG-950、防水剂AG-E061中的一种或几种。
  3. 根据权利要求1所述的纤维织物整理用涂料，其特征在于：
    所述钛酸酯偶联剂优选为螯合型钛酸酯偶联剂。
  4. 根据权利要求1所述的纤维织物整理用涂料，其特征在于：
    所述纳米二氧化钛粒径为10-12纳米。
  5. 根据权利要求1所述的纤维织物整理用涂料，其特征在于：
    先在硅橡胶乳液加入防水剂混合搅拌，并用转速不少于300转/分钟的搅拌机中逐步加入纳米二氧化钛，分散搅拌30分钟，再加入钛酸酯偶联剂，分散搅拌不少于60min，最后加入水分散搅拌30分钟。
  6. 一种根据权利要求1-5之一所述的纤维织物整理用涂料的使用方法，包括如下步骤：
    步骤1：将待处理的纤维织物进行充分水洗，烘干水洗后纤维水分；
    步骤2：将纤维织物浸入权利要求1-5之一所述的纤维织物整理用涂料中，不断翻转，让其充分浸渍；
    步骤3：将充分浸渍的纤维织物在低转速的离心机上甩脱多余的涂料，使织物带液量保留70-75％；
    步骤4：将脱液的纤维织物放入烘干箱中逐步升温，并打开风机，使烘干箱温度均匀，然后随炉冷却；
    步骤5：对烘干的纤维织物，根据材料、形状不同进行熨烫定型处理。
  7. 根据权利要求6的使用方法，其特征在于：步骤1中，烘干温度大于100℃和不少于2个小时。
  8. 根据权利要求6的使用方法，其特征在于：步骤4中，烘干温度和时间如下：
    1.常温→60℃，50min；
    2. 60℃→110℃80min；
    3. 110℃→160℃20min。
PCT/CN2022/119833 2022-09-14 2022-09-20 一种纤维织物整理用涂料及其使用方法 WO2024055341A1 (zh)

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