WO2022080682A1 - Procédé pour l'aromatisation et la maturation de matière à fumer, et article pour fumeur fabriqué à l'aide de celui-ci - Google Patents

Procédé pour l'aromatisation et la maturation de matière à fumer, et article pour fumeur fabriqué à l'aide de celui-ci Download PDF

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Publication number
WO2022080682A1
WO2022080682A1 PCT/KR2021/012546 KR2021012546W WO2022080682A1 WO 2022080682 A1 WO2022080682 A1 WO 2022080682A1 KR 2021012546 W KR2021012546 W KR 2021012546W WO 2022080682 A1 WO2022080682 A1 WO 2022080682A1
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Prior art keywords
smoking material
weight
smoking
flavored
aging
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PCT/KR2021/012546
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English (en)
Korean (ko)
Inventor
이철희
차광호
김한진
정내오
이장미
임창근
Original Assignee
주식회사 케이티앤지
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Application filed by 주식회사 케이티앤지 filed Critical 주식회사 케이티앤지
Priority to CN202180006568.2A priority Critical patent/CN114727644A/zh
Priority to EP21880330.2A priority patent/EP4042883A4/fr
Priority to US17/791,042 priority patent/US20230043392A1/en
Priority to JP2022524688A priority patent/JP2023503231A/ja
Publication of WO2022080682A1 publication Critical patent/WO2022080682A1/fr

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    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B13/00—Tobacco for pipes, for cigars, e.g. cigar inserts, or for cigarettes; Chewing tobacco; Snuff
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/165—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes comprising as heat source a carbon fuel or an oxidized or thermally degraded carbonaceous fuel, e.g. carbohydrates, cellulosic material
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00—Preparing tobacco in the factory
    • A24B3/12—Steaming, curing, or flavouring tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B7/00—Cutting tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B9/00—Control of the moisture content of tobacco products, e.g. cigars, cigarettes, pipe tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
    • A24D1/045—Cigars; Cigarettes with mouthpieces or filter-tips with smoke filter means
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/002—Cigars; Cigarettes with additives, e.g. for flavouring

Definitions

  • the present invention relates to a method for flavored aging of a smoking material and a smoking article manufactured using the same, and more particularly, to a method for flavored aging of a smoking material capable of improving positive sensory quality and differentiated flavor expression characteristics compared to existing smoking articles; , to a flavored aged leaf tobacco manufactured using the same, and to a smoking article comprising the flavored aged leaf tobacco.
  • the taste of tobacco felt during smoking is determined by various factors such as the composition of the smoking material part, the filter part, and the cigarette paper, but fundamentally, leaf tobacco, leaf tobacco, etc.
  • the taste is determined or affected by the type of composition, additives such as fragrance components, and their aging method.
  • the present invention has been devised to solve the above problems, and an object of the present invention is to provide a method for flavored aging of a smoking material capable of enhancing the taste and flavor of tobacco, and a smoking article manufactured using the same.
  • the method comprising: diluting a flavoring agent in a base solution and adding it to the smoking material;
  • a method for flavored aging of a smoking material for constituting at least a portion of a smoking material portion of a smoking article, comprising the step of aging the smoking material to which the flavoring agent has been added under constant temperature and humidity conditions.
  • the combined weight of the flavoring agent and the base solution may be 1% to 20% based on the total weight of the smoking material.
  • each of the weight of the flavoring agent and the weight of the base solution may be 1% to 10% based on the total weight of the smoking material.
  • the method for flavored aging of the smoking material may further include, between the step of adding the flavoring and the aging step, adjusting the moisture of the smoking material so that the moisture of the smoking material is 15% to 35% by weight.
  • the aging step is preferably performed for 7 to 25 days under conditions of an internal temperature of 60°C to 80°C and an internal relative humidity of 20% to 40%.
  • the smoking material may be leaf tobacco having a total sugar content of 20% to 40% by weight.
  • the flavoring agent is at least one of vanilla concentrate, chocolate concentrate, maple syrup, prune concentrate, cocoa concentrate, pine flavoring solution, cinnamon flavoring solution, and red wine flavoring solution.
  • the flavoring agent may be the vanilla concentrate, and the base solution may be alcohol.
  • the flavoring agent may be the chocolate concentrate, and the base solution may be water.
  • the method for flavored aging of the smoking material includes the steps of: moistening the aging-treated smoking material after adding the flavoring; first moisturizing the smoking material that has been wetted by adding at least one of propylene glycol and glycerin; cutting the first moistened smoking material; drying the cut smoking material; and secondarily moisturizing the dried smoking material by adding at least one of the propylene glycol and the glycerin.
  • the wet point treatment step is performed under a temperature of 90 ° C. to 110 ° C.
  • the drying step is performed under a temperature of 100 ° C. to 120 ° C.
  • the weight of the propylene glycol added in the first moisturizing step is the first Doedoe less than the weight of the glycerin added in the moisturizing step
  • the weight of the propylene glycol added in the second moisturizing step may be greater than the weight of the glycerin added in the second moisturizing step.
  • a flavored aged leaf tobacco flavored by the above-described flavored aging method for constituting at least a portion of the smoking material portion of a smoking article.
  • At least a portion of the smoking material part filled with the flavored aged leaf tobacco at least a portion of the smoking material part filled with the flavored aged leaf tobacco; and a filter unit located downstream of the smoking material unit.
  • the smoking material part includes 15% to 35% by weight of the flavored aged leaf tobacco, 5% to 25% by weight of the non-flavored aged leaf tobacco, 15% to 35% by weight of toast leaves, 1 weight% of the leaf tobacco % to 20% by weight and 15% to 35% by weight of swollen stems may be blended and filled.
  • the smoking material flavor aging method it is possible to provide a smoking material with a differentiated flavor character, and it is possible to provide a smoking article having excellent flavor persistence and improved overall tobacco taste.
  • FIG. 1 is a flowchart exemplarily illustrating a method for flavored aging of a smoking material according to some embodiments of the present invention.
  • FIG. 2 is a diagram illustrating an exemplary configuration of a smoking article including flavored-aged leaf tobacco according to some embodiments of the present invention.
  • FIG. 3 is a view showing a comparison of smoking sensory evaluation results of smoking articles manufactured according to Examples and Comparative Examples, respectively.
  • smoking article means any product capable of smoking or a smoking experience, whether based on tobacco, tobacco derivatives, expanded tobacco, reconstituted tobacco or tobacco substitutes. It may mean any product that can provide
  • smoking articles may include smokeable products such as cigarettes, cigars, and cigarillos.
  • smoking material may mean any kind of material that can be used in a smoking article.
  • upstream or “upstream direction” means a direction away from the smoker's bend
  • downstream or “downstream direction” may mean a direction approaching from the smoker's bend.
  • longitudinal direction may mean a direction corresponding to the longitudinal axis of the smoking article.
  • 'smoking articles' may refer to articles that can generate aerosols, such as cigarettes (cigarettes) and cigars.
  • Smoking articles may include an aerosol-generating material or an aerosol-forming substrate.
  • the smoking article may contain solid materials based on tobacco raw materials, such as leaf tobacco, cut filler, reconstituted tobacco, and the like.
  • Smoking materials may contain volatile compounds.
  • FIG. 1 is a flowchart exemplarily illustrating a method for flavored aging of a smoking material according to some embodiments of the present invention.
  • the method for flavor aging of a smoking material includes the steps of diluting a flavoring agent in a base solution and adding it to the smoking material (S10), adjusting the moisture of the flavored smoking material (S20), and moisture-adjusted smoking material aging under constant temperature and humidity conditions (S30), wet-point treatment of the aged smoking material (S40), primary moisturizing treatment of the wet-pointed smoking material (S50), It may include a step of cutting (S60), a step of drying the cut smoking material (S70), and a step of secondary moisturizing the dried smoking material (S80).
  • the smoking material flavored and matured by the above method may be blended with non-flavored aged leaf tobacco, plate leaf, toast leaf and expanded stem, etc., and then filled with the smoking material portion of the smoking article.
  • the flavoring agent added to the smoking material may include at least one of various flavoring ingredients, and the base solution may be alcohol or water. .
  • the flavoring agent includes at least one of vanilla concentrate, chocolate concentrate, maple syrup, prune concentrate, cocoa concentrate, pine flavor, cinnamon flavor, and red wine flavor.
  • the base solution may be selected from any one of alcohol and water according to the flavoring agent.
  • the flavoring agent may be a vanilla concentrate or a chocolate concentrate.
  • the flavoring agent may be a vanilla concentrate, and in this case, the base solution may be alcohol.
  • the flavoring agent may be chocolate concentrate, and in this case, the base solution may be water.
  • the combined weight of the flavoring agent and the base solution may be about 1% to 20% based on the total weight of the smoking material, preferably about 5% to 15% based on the total weight of the smoking material. .
  • each of the weight of the flavoring agent and the weight of the base solution may be about 1% to 10%, preferably about 2% to 6%, based on the total weight of the smoking material.
  • the flavoring agent and the base solution may be diluted in a ratio of 1:2 to 2:1 (eg, about 1:1).
  • about 4% of the flavoring agent and about 4% of the base solution based on the total weight of the smoking material may be added to the smoking material.
  • the smoking material is preferably leaf tobacco having a total sugar content of about 20% to 40% by weight. More preferably, the smoking material may be true xanth species having a total sugar content of about 25% to 35% by weight.
  • the flavored smoking material has a moisture content of about 10% to 35% by weight, preferably about 15% to 25% by weight, more preferably about 17% by weight. Moisture may be adjusted so as to be from weight % to 23 weight %.
  • the step of aging the moisture-adjusted smoking material under constant temperature and humidity conditions (S30) is to be carried out for about 7 to 25 days under the condition that the internal temperature is about 60°C to 80°C and the internal relative humidity is about 20% to 40%.
  • the aging step (S30) may be performed for about 10 to 18 days under the condition that the internal temperature is about 65 °C to 75 °C and the internal relative humidity is about 25% to 35%.
  • the wet-point treatment of the aged smoking material (S40) is performed under a temperature of 90°C to 110°C, preferably 95°C to 105°C, and the drying of the cut smoking material (S70) is the wet-point treatment step ( S40) higher than the temperature, for example, 100 °C to 120 °C, it may be carried out under a temperature of preferably 105 °C to 115 °C.
  • the smoking material may be subjected to at least one moisturizing treatment step.
  • at least one of propylene glycol and glycerin may be added to the smoking material.
  • the at least one moisturizing treatment step includes the first moisturizing treatment step (S50) performed between the aging step (S30) and the cutting step (S60), and the second moisturizing treatment step performed after the drying step (S70). (S80) may be included.
  • the added weight of propylene glycol is smaller than the added weight of glycerin, and in the second moisturizing step (S80), the added weight of propylene glycol is greater than the added weight of glycerin. there is.
  • the first moisturizing treatment step (S50) about 0.8% to 1.2% of propylene glycol and about 1.3% to 1.7% of glycerin are added relative to the total weight of the smoking material, and in the second moisturizing treatment step (S80), smoking About 0.1% to 0.5% propylene glycol and about 0.01% to 0.05% glycerin may be added relative to the total weight of the material.
  • the smoking material such as leaf tobacco may be cut into tobacco strands having a width of approximately 0.5 mm to 1.5 mm, preferably 0.7 mm to 1.1 mm.
  • the composition of flavor components in the smoking material can be more preferably modified. And it is possible to manufacture a smoking article with improved overall tobacco taste by reducing irritation and taste.
  • the flavor-aged smoking material as described above may be blended with non-flavored aged leaf tobacco, plate leaf, toast leaf and expanded stem, etc., and then filled with the smoking material portion of the smoking article.
  • the non-flavoured leaf tobacco may mean leaf tobacco that has not been subjected to the flavor aging treatment described with reference to FIG. 1 . That is, the non-flavored aged leaf tobacco may include, for example, raw leaf tobacco that is not subjected to flavoring and aging, leaf tobacco treated only in the flavoring process, or leaf tobacco treated only in the aging process.
  • the smoking material filled in the smoking material unit 110 to be described with reference to FIG. 2 is about 15% to 35% by weight of the flavored aged leaf tobacco, about 5% to 25% by weight of the non-flavoured leaf tobacco, toast About 15% to 35% by weight of the leaf, about 1% to 20% by weight of the plate leaf, and about 15% to 35% by weight of the swelling stem may be blended.
  • FIG. 2 is a diagram illustrating an exemplary configuration of a smoking article 100 including flavored-aged leaf tobacco according to some embodiments of the present invention.
  • the smoking article 100 is a combustion cigarette
  • the present invention is not limited thereto, and the smoking article 100 may be a heated cigarette used together with an aerosol generating device (not shown) such as an electronic cigarette device. of course there is
  • a smoking article 100 includes a smoking material part 110 in which a smoking material wrapper 110a is wrapped, a filter part 120 in which the filter wrapper 120a is wrapped, and the smoking material part 110 and It may include a tip paper 130 for coupling the filter unit 120 .
  • the smoking material unit 110 may have an elongated rod shape and may have various lengths, circumferences, and diameters.
  • the smoking material unit 110 may be filled with a mixture of flavored-aged leaf tobacco, non-flavored-aged leaf tobacco, plate leaf, toast leaf, and expanded stems in the manner described above with reference to FIG. 1 .
  • an aerosol generating material of at least one of glycerin, propylene glycol, ethylene glycol, dipropylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol, and oleyl alcohol may be additionally added to the smoking material unit 110 .
  • the smoking material portion 110 may contain other additives such as flavoring agents, wetting agents and/or acetate compounds.
  • flavoring agents include licorice, sucrose, fructose syrup, double sweetener, cocoa, lavender, cinnamon, cardamom, celery, fenugreek, cascarilla, sandalwood, bergamot, geranium, honey essence, rose oil, vanilla, lemon. oil, orange oil, mint oil, cinnamon, caraway, cognac, jasmine, chamomile, menthol, cinnamon, ylang-ylang, sage, spearmint, ginger, coriander or coffee and the like.
  • the wetting agent may include glycerin or propylene glycol, and the like.
  • the smoking material unit 110 pulverizes the flavored aged leaf tobacco, plate leaves, toast leaves, swollen stems, etc., and then mixes a solvent and various additives to form a slurry, and then dried to form a sheet. These sheets may then be processed to include reconstituted tobacco material formed into pieces such as rods.
  • smoking material portion 110 comprises a plurality of strands of reconstituted tobacco material, one strand approximately 10 to 14 mm long (eg, 12 mm) and approximately 0.8 mm to 1.2 mm wide (eg, For example, 1 mm) and the thickness may be approximately 0.08 mm to 0.12 mm (eg, 0.1 mm), but is not limited thereto.
  • the smoking material unit 110 may be wrapped by the smoking material wrapper 110a.
  • glycerin and a supporting agent such as K-citrate and/or NA-citrate for promoting complete combustion of the smoking material by catalysis, etc.
  • a supporting agent such as K-citrate and/or NA-citrate for promoting complete combustion of the smoking material by catalysis, etc.
  • calcium carbonate, titanium dioxide, oxidized A filler such as magnesium may be included.
  • the smoking material wrapper 110a may have a double wrapper structure. Specifically, the smoking material wrapper 110a is in contact with the smoking material unit 110 and covers an inner wrapper surrounding the smoking material unit 110 , and an outer wrapper which contacts the inner wrapper and wraps the outside of the inner wrapper. ) may be included.
  • the smoking material wrapper 110a may be a cigarette paper having one or more low ignition resistance (LIP) bands (not shown) formed thereon.
  • LIP low ignition resistance
  • the filter unit 120 may be disposed downstream of the smoking material unit 110 , and may be an area through which the aerosol material generated in the smoking material unit 110 passes just before inhalation by the user.
  • the filter unit 120 may be formed of various materials, for example, the filter unit 120 may be a cellulose acetate filter.
  • the filter unit 120 may be a cellulose acetate filter in which the fragrance material is not flavored, but is not limited thereto, and the filter unit 120 may be a transfer jet nozzle system (TJNS) filter in which the fragrance material is processed.
  • TJNS transfer jet nozzle system
  • the filter unit 120 may be a tube-shaped structure including a hollow therein.
  • the filter unit 120 may be manufactured by inserting a structure such as a film or a tube made of the same or different material inside (eg, hollow).
  • the filter unit 120 of the present embodiment is illustrated as a mono filter including a single filter, it is not limited thereto.
  • the filter unit 120 may be provided as a dual filter or a triple filter having two acetate filters in order to increase filter efficiency.
  • a capsule (not shown) may be included in the filter unit 120 .
  • the capsule may have a structure in which the liquid containing the fragrance is wrapped with a film, for example, the capsule may have a spherical or cylindrical shape.
  • the material forming the capsule film may be a natural material, starch and/or a gelling agent.
  • MCTG medium chain fatty acid triglyceride
  • the internal solution may contain other additives such as a colorant, an emulsifier, and a thickener.
  • the content of the capsule may include flavorings such as menthol and essential oils of plants, but is not limited thereto.
  • the filter unit 120 may be wrapped by a filter wrapper 120a.
  • the filter wrapper 120a may be made of a wrapper having oil resistance.
  • the filter wrapper 120a may be made of oil-resistant paper in order to prevent the capsule content that is released to the outside of the capsule from passing through the filter wrapper 120a as the capsule that may be included in the filter unit 120 is crushed by the smoker.
  • an aluminum foil may be further included on the inner surface of the filter wrapper 120a.
  • the filter unit 120 packaged by the filter wrapper 120a and the smoking material unit 110 packaged by the smoking material wrapper 110a may be combined and packaged by the tip paper 130 . That is, the tip paper 130 may be surrounded by at least a portion (eg, a downstream partial region) of the smoking material wrapper 110a and the outside of the filter wrapper 120a. Meanwhile, the tip paper 130 may contain a non-combustible material to prevent the filter unit 120 from being combusted according to the combustion of the smoking material unit 110 .
  • the smoking material portion of the cigarette prepared for testing was removed, and about 20% by weight of flavored aged leaf tobacco, about 20% by weight of non-flavored aged leaf tobacco, about 25% by weight of toast leaf, about 10% by weight of platelet leaf and swollen stem About 25% by weight was formulated to fill the smoking material part.
  • the flavored-aged leaf tobacco used in the formulation was prepared by flavor-aging the domestic xanthium leaves with a total sugar content of about 30% by weight. After moisture adjustment so that the moisture content of the leaf tobacco is about 20%, it was aged for about 14 days at an internal temperature of about 70°C and an internal relative humidity of about 30%. Aged leaf tobacco is subjected to wet point treatment at a temperature of about 100°C, then about 1000g of PG and about 1500g of glycerin are added for primary moisturizing, cut to a width of about 0.9mm, dried at a temperature of about 110°C, and then about 300g of PG and glycerin About 30 g was added to perform secondary moisturizing treatment.
  • a smoking article was prepared in the same manner as in Example 1, except that chocolate concentrate was used as a flavoring agent and water was used as a base solution in the flavor aging process.
  • a smoking article was prepared in the same manner as in Example 2, except that dried cucumber concentrate was used as a flavoring agent in the flavor aging process.
  • a smoking article was prepared in the same manner as in Example 2, except that maple syrup was used as a flavoring agent in the flavor aging process.
  • a smoking article was prepared in the same manner as in Example 2, except that cocoa concentrate was used as a flavoring agent in the flavor aging process.
  • the smoking material part of the cigarette prepared for testing is removed, and about 20% by weight of aged leaf tobacco, about 20% by weight of non-flavored aged leaf tobacco, about 25% by weight of toast leaves, about 10% by weight of platelets and about swollen stems 25% by weight was blended to fill the smoking material part.
  • the aged leaf tobacco used in the formulation was prepared by aging the same leaf tobacco as in Example 1 in the same manner as in Example 1 in a state where no flavoring was added.
  • the smoking material part of the cigarette prepared for testing was removed, and about 20% by weight of flavored leaf tobacco, about 20% by weight of non-flavored leaf tobacco, about 25% by weight of toast leaf, about 10% by weight of platelet leaf, and swelling About 25% by weight of the stem was blended to fill the smoking material part.
  • Example 1 For the flavored leaf tobacco, about 4 kg of vanilla concentrate was diluted with about 4 kg of alcohol and added to about 100 kg of the same leaf tobacco as in Example 1, then the aging process was omitted and the wet point treatment, moisturizing treatment, cutting and drying processes were performed with Example 1 It was prepared in the same way.
  • a smoking article was prepared in the same manner as in Comparative Example 2, except that chocolate concentrate was used as a flavoring agent and leaf tobacco was flavored using water as a base solution.
  • the flavor components in the leaves of the flavored aged leaf tobacco, aged leaf tobacco, and flavored leaf tobacco used in each of Examples and Comparative Examples were analyzed by SPME-GC/MS (Solid Phase Micro Extraction-Gas Chromatography/Mass Spectrometry) measurement method 1 is shown.
  • Table 2 shows the flavor component analysis results for evaluating the degree of loss of flavor components before and after the aging process in Examples 1 and 2, respectively (wet point, moisturizing, cutting, drying, etc.). Numerical values for each component in Tables 1 and 2 indicate peak area ratios (relative values) analyzed according to SPME-GC/MS measurement.
  • Glycolysis products with roasted flavor properties were particularly increased, and in the flavored-aged leaf tobacco of Example 2, semi-volatile compounds with sweet flavor properties such as 'p-Anisaldehyde' and 'Anisyl acetate' were particularly increased.
  • the flavor component modification effect according to the aging did not appear in the flavored-aged leaf tobacco aged for about 1 week, and the flavored-aged leaf tobacco aged for about 4 weeks and the total sugar content were about Flavor-aged leaf tobacco using leaf tobacco of 15 wt% showed deterioration in physical properties and yield of leaf tobacco, and flavored-aged leaf tobacco using leaf tobacco having a total sugar content of about 40 wt% was detected in the amount of nicotine less than the reference value, and Comparative Examples.
  • Example 1 (Vanilla ripening)
  • Example 2 (chocolate ripening) characteristic ingredient before the fair after process before the fair after process
  • Roasted 3,6-Dimethyl-4H-furo[3,2-c] pyran-4-one 86 79 22 23 2(3H)-Furanone, dihydro-5-propyl- 3,259 2,358 232 292 3-Furaldehyde 248 145 238 151 5-Methylfurfural 141 99 138 104
  • Furfuryl alcohol 44 40 39 32 gamma-Nonalactone 5,319 4,518 319 479 2,3'-Dipyridyl 79 100 92 96
  • Sweet Piperonal 1,602 1,367 114 186 Piperonyl alcohol 132 103 111 109 Anisyl acetate 1,538 1,111 7,110 6,753
  • Anise alcohol 45 55 705 706 p-Anisaldehyde 29 37 313 275 To
  • the sensory evaluation was performed on the taste intensity, aroma intensity, flavor satisfaction, irritation, off-taste, clean aftertaste, and overall tobacco taste of each smoking article in Examples and Comparative Examples.
  • the sensory characteristic evaluation was conducted for 27 evaluation panel members using each of the smoking articles manufactured according to the Examples, and a total score of 7 was used as the standard.
  • FIG. 3 is a view showing a comparison of smoking sensory evaluation results of smoking articles manufactured according to Examples and Comparative Examples, respectively.
  • Example 1 flavored with vanilla concentrate and Example 2 flavored with chocolate concentrate
  • higher flavor strength, flavor satisfaction, clean aftertaste, and overall tobacco taste characteristics were shown compared to Comparative Examples and other Examples, It was confirmed that the effect of reducing taste and irritation was also superior to that of the other examples.
  • smoking articles containing flavored aged leaf tobacco have less artificial taste and flavor than smoking products containing unaged leaf tobacco or unscented leaf tobacco, and It was also found that the perceived negative attributes decreased.

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  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
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  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Molecular Biology (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

Un mode de réalisation de la présente invention concerne un procédé pour l'aromatisation et la maturation d'une matière à fumer, comprenant les étapes consistant à : diluer un agent d'aromatisation avec une solution de base et ajouter ceux-ci à une matière à fumer ; et faire maturer, dans des conditions de température et d'humidité constantes, la matière à fumer à laquelle l'agent d'aromatisation est ajouté.
PCT/KR2021/012546 2020-10-14 2021-09-15 Procédé pour l'aromatisation et la maturation de matière à fumer, et article pour fumeur fabriqué à l'aide de celui-ci WO2022080682A1 (fr)

Priority Applications (4)

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CN202180006568.2A CN114727644A (zh) 2020-10-14 2021-09-15 吸烟材料的加香熟成方法及使用该方法制备的吸烟制品
EP21880330.2A EP4042883A4 (fr) 2020-10-14 2021-09-15 Procédé pour l'aromatisation et la maturation de matière à fumer, et article pour fumeur fabriqué à l'aide de celui-ci
US17/791,042 US20230043392A1 (en) 2020-10-14 2021-09-15 Method of flavoring and aging smoking material and smoking article manufactured using the same
JP2022524688A JP2023503231A (ja) 2020-10-14 2021-09-15 喫煙材料の加香熟成方法およびこれを用いて製造された喫煙物品

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KR1020200132495A KR102571394B1 (ko) 2020-10-14 2020-10-14 흡연재료의 가향숙성방법 및 이를 이용하여 제조된 흡연물품
KR10-2020-0132495 2020-10-14

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WO2022080682A1 true WO2022080682A1 (fr) 2022-04-21

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US (1) US20230043392A1 (fr)
EP (1) EP4042883A4 (fr)
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CN (1) CN114727644A (fr)
WO (1) WO2022080682A1 (fr)

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EP4042883A1 (fr) 2022-08-17
KR20220049188A (ko) 2022-04-21
EP4042883A4 (fr) 2023-01-11
CN114727644A (zh) 2022-07-08
KR102571394B1 (ko) 2023-08-25
US20230043392A1 (en) 2023-02-09
JP2023503231A (ja) 2023-01-27

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