WO2021008016A1 - 速干型无熔滴面料 - Google Patents

速干型无熔滴面料 Download PDF

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Publication number
WO2021008016A1
WO2021008016A1 PCT/CN2019/116461 CN2019116461W WO2021008016A1 WO 2021008016 A1 WO2021008016 A1 WO 2021008016A1 CN 2019116461 W CN2019116461 W CN 2019116461W WO 2021008016 A1 WO2021008016 A1 WO 2021008016A1
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Prior art keywords
fabric
quick
spinning
drying
drying non
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PCT/CN2019/116461
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English (en)
French (fr)
Inventor
陈明青
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浙江蓝天海纺织服饰科技有限公司
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Publication of WO2021008016A1 publication Critical patent/WO2021008016A1/zh

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Classifications

    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
    • D02G3/04—Blended or other yarns or threads containing components made from different materials
    • D—TEXTILES; PAPER
    • D03—WEAVING
    • D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04B—KNITTING
    • D04B1/00—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
    • D04B1/14—Other fabrics or articles characterised primarily by the use of particular thread materials
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04B—KNITTING
    • D04B21/00—Warp knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/01—Natural vegetable fibres
    • D10B2201/02—Cotton
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/02—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyamides
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]

Definitions

  • the present invention relates to a quick-drying non-melt dripping fabric that can be used as tooling or uniform and tooling or uniform containing the fabric.
  • a method for preparing a quick-drying non-drip fabric includes the following steps in sequence:
  • step S2 the drawing process uses the polyamide ester fiber, cotton fiber and polyester fiber to prepare the yarn for blending, and the yarn manufacturing process can adopt ring spinning, Siro spinning, The spinning equipment and technology of compact spinning, open-end spinning or vortex spinning, through the rapier loom or air-jet loom, single yarn warp and weft interweaving or different warp and weft yarn interweaving to make a blended woven fabric, also can use knitted warp knitting Way to make a blended knitted fabric.
  • step S3 the post-finishing operations include desizing, singeing, bleaching, mercerizing, dyeing, post-finishing and winding;
  • the yarn can also be knitted and post-knitting operations, so
  • the finishing operations after knitting include pretreatment, mercerizing, dyeing, opening, shaping and rolling.
  • a further preferred technical solution is that according to the GB/T5455-2014 standard, the quick-drying non-melting fabric has no drips in the warp and weft directions.
  • a further preferred technical solution is that according to the GB/T5455-2014 standard, the quick-drying non-melt dripping fabric forms a carbonized layer after burning, and ordinary cotton/polyester fabrics will melt dripping.
  • step S1 by weight, the terephthalic acid is 100 parts, the ethylene glycol is 60-80 parts, the antimony triacetate is 0.05-0.07 parts, and the esterification reaction temperature is 220- 270°C, reaction pressure is 0.1-0.4Mpa, reaction time is 1-3h.
  • Fig. 1 is a graph of the drip-free combustion effect of the medium-speed-drying non-melt drip fabric of the present invention.
  • the left side of the figure is the existing fabric, and the right side is the fast-drying drip-free fabric of the present invention.
  • the fabric composition includes polyester fiber, cotton fiber and polyester fiber, the content of the polyester fiber is 20-50wt%, the cotton The content of the fiber is 50-75wt%, the content of the polyester fiber is 5-25wt%, and the polyamide ester fiber contains more than 3wt% of the total fiber.
  • a method for preparing a quick-drying non-drip fabric includes the following steps in sequence:
  • the yarn undergoes the steps of warping, sizing, reeding, machine weaving and dyeing, and blended to produce the C60/T40 32*32 130*70 2/1 quick-drying non-melting fabric.
  • step S2 the drawing process uses the polyester fiber, cotton fiber and polyester fiber to prepare the yarn for blending.
  • the yarn making process can adopt ring spinning, silo spinning, compact spinning, air spinning and vortex spinning.
  • the spinning equipment and process of spinning are used to obtain a blended woven fabric by interweaving a single warp and weft of a rapier loom or an air-jet loom or interlacing different warp and weft yarns.
  • step S3 the blended fabric is dyed after weaving Operation, the finishing operations include desizing, singeing, bleaching, mercerizing, dyeing, finishing and rolling.
  • the preparation method of the polyester fiber is as follows:
  • the point-to-point resistance of the quick-drying non-melt dripping fabric after washing 100 times is 5.3*106.
  • the evaporation rate of the quick-drying non-drip fabric before washing is 0.28g/h.
  • the evaporation rate of the quick-drying non-melting fabric after washing 5 times is 0.30 g/h.
  • the moisture permeability of the quick-drying non-melting fabric before washing is 10487 [g/(m2•24h)].
  • the moisture permeability of the quick-drying non-melt dripping fabric after washing 5 times is 10466 [g/(m2•24h)].
  • the quick-drying non-melt dripping fabric has no melting or dripping in the radial direction and the weft direction.
  • the quick-drying in this application refers to the evaporation rate and moisture permeability in the quick-drying according to GB/T21655.1-2008. No droplet means according to GB8965.1-2009 Melting, dripping items
  • the quick-drying non-melt dripping fabric contains polyamide ester fibers containing polyamide molecules, that is, if the weight content of the polyester fiber is less than 10wt%, according to the GBT21655.1-2008 standard, the quick-drying type non-melting The evaporation rate and moisture permeability of the dripping fabric decrease. If it exceeds 50wt%, the blending amount of other fibers becomes too small. According to the GB8965.1-2009 standard, the fabric will melt and drip. Therefore, the above 10-50 is determined The range of wt%.
  • the quick-drying non-melt dripping fabric is used for making clothing.
  • step S2 the drawing process uses the polyester fiber, cotton fiber and polyester fiber to prepare the yarn for blending.
  • the yarn making process can adopt ring spinning, silo spinning, compact spinning, air spinning and vortex spinning.
  • the spinning equipment and process of spinning are used to obtain a blended woven fabric by interweaving a single warp and weft of a rapier loom or an air-jet loom or interlacing different warp and weft yarns.
  • step S3 the blended fabric is dyed after weaving Operation, the finishing operations include desizing, singeing, bleaching, mercerizing, dyeing, finishing and rolling.
  • the preparation method of the polyester fiber is as follows:
  • the point-to-point resistance of the quick-drying non-melt dripping fabric after washing 100 times is 5.3*106.
  • the evaporation rate of the quick-drying non-melting fabric before washing is 0.31g/h.
  • the evaporation rate of the quick-drying non-melting fabric after washing 5 times is 0.34 g/h.
  • the moisture permeability of the quick-drying non-melting fabric before washing is 11450 [g/(m2•24h)].
  • the moisture permeability of the quick-drying non-melt dripping fabric after washing 5 times is 11482 [g/(m2•24h)].
  • the quick-drying non-melt dripping fabric has no melting or dripping in the radial direction and the weft direction.
  • the produced blended fabrics all have the advantages of good quick-drying and no droplets during combustion, and there is still no risk of dripping even in the case of burning through.
  • the fabric composition includes polyester fiber, cotton fiber and polyester fiber, the content of the polyester fiber is 10-50wt%, the cotton The content of the fiber is 30-85 wt%, the content of the polyester fiber is 5-20 wt%, and the polyamide ester fiber contains more than 3 wt% of the total fiber.
  • the quick-drying in this application refers to the evaporation rate and moisture permeability in the quick-drying according to GB/T21655.1-2008. No droplet means according to GB8965.1-2009 Melting and dripping items.
  • the quick-drying non-melt dripping fabric contains polyamide ester fibers containing polyamide molecules, that is, if the weight content of the polyester fiber is less than 10wt%, according to the GBT21655.1-2008 standard, the quick-drying type non-melting The evaporation rate and moisture permeability of the dripping fabric decrease. If it exceeds 50wt%, the blending amount of other fibers becomes too small. According to the GB8965.1-2009 standard, the fabric will melt and drip. Therefore, the above 10-50 is determined The range of wt%.
  • the quick-drying non-melt dripping fabric is used for making clothing.
  • the yarn is blended to obtain the quick-drying non-melt drip-free knitted jersey fabric through the warp drawing, machine weaving and dyeing steps.
  • step S2 the drawing process uses the polyester fiber, cotton fiber and polyester fiber to prepare the yarn for blending.
  • the yarn making process can adopt ring spinning, silo spinning, compact spinning, air spinning and vortex spinning. Spinning equipment and technology, by using knitted warp knitting and other methods to prepare blended knitted quick-drying non-melt drip knitted jersey fabric.
  • step S3 a dyeing operation is performed after the weaving of the blended fabric is completed, and the finishing operation includes pretreatment, mercerizing, dyeing, opening, shaping, and rolling.
  • the preparation method of the polyester fiber is as follows:
  • the point-to-point resistance of the quick-drying non-melt dripping fabric after washing 100 times is 5.3*106.
  • the evaporation rate of the quick-drying non-drip fabric before washing is 0.30g/h.
  • the evaporation rate of the quick-drying non-melting fabric after washing 5 times is 0.32 g/h.
  • the moisture permeability of the quick-drying non-melting fabric before washing is 11800 [g/(m2•24h)].
  • the moisture permeability of the quick-drying non-melt dripping fabric after washing 5 times is 12130 [g/(m2•24h)].
  • the quick-drying non-melting fabric has no melting or dripping in the radial and weft directions.
  • the produced blended quick-drying non-melt dripping knitted jersey fabric has the advantages of good quick-drying and no dripping when burning, and there is no risk of dripping even in the case of burning through.
  • the fabric composition includes polyester fiber, cotton fiber and polyester fiber, the content of the polyester fiber is 10-50wt%, so The content of the cotton fiber is 30-85 wt%, the content of the polyester fiber is 5-20 wt%, and the polyamide ester fiber contains polyamide accounting for more than 3 wt% of the total fiber.
  • the quick-drying non-melt dripping fabric contains polyamide ester fibers containing polyamide molecules, that is, if the weight content of the polyester fiber is less than 10wt%, according to the GBT21655.1-2008 standard, the quick-drying type non-melting The evaporation rate and moisture permeability of the dripping fabric decrease. If it exceeds 50wt%, the blending amount of other fibers becomes too small. According to the GB8965.1-2009 standard, the fabric will melt and drip. Therefore, the above 10-50 is determined The range of wt%.
  • the yarn is blended to obtain the quick-drying non-melt drip-free knitted pique mesh fabric through the steps of warp drawing, machine weaving and dyeing.
  • the point-to-point resistance of the quick-drying non-melt dripping fabric after washing 100 times is 5.3*106.
  • the evaporation rate of the quick-drying non-melting fabric before washing is 0.33g/h.
  • the evaporation rate of the quick-drying non-melting fabric after washing 5 times is 0.36 g/h.
  • the moisture permeability of the quick-drying non-melting fabric before washing is 13750[g/(m2•24h)].
  • the moisture permeability of the quick-drying non-melting fabric after washing 5 times is 13620 [g/(m2•24h)] according to the GB/T 5455-2014 standard, the quick-drying non-melting fabric The fabric has no melting or dripping in the radial direction and the weft direction.
  • the produced blended quick-drying non-melt dripping knitted beaded mesh fabric has the advantages of good quick-drying and no dripping when burned, and there is still no risk of dripping even in the case of burning through.
  • the fabric composition includes polyester fiber, cotton fiber and polyester fiber, the content of the polyester fiber is 10-50wt%, The content of the cotton fiber is 30-85 wt%, the content of the polyester fiber is 5-20 wt%, and the polyamide ester fiber contains more than 3 wt% of the total fiber.
  • the quick-drying in this application refers to the evaporation rate and moisture permeability in the quick-drying according to GB/T21655.1-2008. No droplet means according to GB8965.1-2009 Melting and dripping items.
  • the quick-drying non-melt dripping fabric contains polyamide ester fibers containing polyamide molecules, that is, if the weight content of the polyester fiber is less than 10wt%, according to the GBT21655.1-2008 standard, the quick-drying type non-melting The evaporation rate and moisture permeability of the dripping fabric decrease. If it exceeds 50wt%, the blending amount of other fibers becomes too small. According to the GB8965.1-2009 standard, the fabric will melt and drip. Therefore, the above 10-50 is determined The range of wt%.
  • the quick-drying non-melt dripping knitted beaded mesh elastic cloth fabric is used for making clothing.
  • the 32S yarn is made of three fiber blended yarns
  • the yarn is subjected to the steps of drawing, adding spandex elastic yarn, weaving and dyeing, and then blending the yarn to obtain the quick-drying non-melt dripping knitted pique mesh elastic fabric.
  • step S2 the drawing process uses the polyester fiber, cotton fiber and polyester fiber to prepare the yarn for blending.
  • the yarn making process can adopt ring spinning, silo spinning, compact spinning, air spinning and vortex spinning.
  • Spinning equipment and technology by using knitted warp knitting and adding spandex elastic yarn in the weaving process, the blended knitting quick-drying non-melt drip knitted pique mesh stretch fabric fabric is made.
  • step S3 the spandex stretch yarn is added during the weaving of the blended knitted piqué elastic fabric, and the dyeing operation is performed after the weaving is completed, and the finishing operations include pretreatment, mercerizing, dyeing, opening, shaping and rolling. .
  • the preparation method of the polyester fiber is as follows:
  • the point-to-point resistance of the quick-drying non-melt dripping fabric after washing 100 times is 5.3*106.
  • the evaporation rate of the quick-drying non-melting fabric before washing is 0.32g/h.
  • the evaporation rate of the quick-drying non-melting fabric after washing 5 times is 0.35 g/h.
  • the moisture permeability of the quick-drying non-melting fabric before washing is 13260 [g/(m2•24h)].
  • the moisture permeability of the quick-drying non-melting fabric after washing 5 times is 13540 [g/(m2•24h)] according to the GB/T 5455-2014 standard, the quick-drying non-melting fabric The fabric has no melting or dripping in the radial and weft directions.
  • the produced blended quick-drying non-melt dripping knitted beaded mesh fabric has the advantages of good quick-drying and no dripping when burned, and there is still no risk of dripping even in the case of burning through.
  • the final quick-drying non-melting fabric in the present invention is subjected to a combustion test in accordance with GB8965.1-2009 to see if there is any dripping phenomenon.
  • the final quick-drying non-melt dripping fabric in the present invention is tested for quick-drying according to the evaporation rate and moisture permeability in the quick-drying of GB/T21655.1-2008 to see if it has quick-drying performance.

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Woven Fabrics (AREA)
  • Knitting Of Fabric (AREA)
  • Artificial Filaments (AREA)

Abstract

一种能够作为工装或制服来使用的速干型无熔滴面料和含有该面料的服装。通过聚酰胺酯、棉纤维以及聚酯纤维三种纤维混纺，细纱工艺可以采用环锭纺、赛洛纺、紧密纺、气流纺或涡流纺等纺纱设备与工艺，通过剑杆织机或是喷气织机单一纱线经纬交织或是经纬不同纱线交织制得混纺机织面料，也可以使用针织经编等方式制得混纺针织面料。混纺面料制备工艺合理有效，混纺面料使用兼具速干性好以及燃烧无熔滴的优点，在彻底烧通后形成碳化层避免熔滴对人体皮肤的二次伤害，能够使面料在具有速干与无熔滴的同时，维持高性价比。

Description

速干型无熔滴面料 技术领域
本发明涉及能够作为工装或制服来使用的速干型无熔滴面料和含有该面料的工装或制服。
 背景技术
如涤纶、锦纶等合成纤维在燃烧过程中会产生熔滴现象，这些高温的滴落物很容易引燃其他聚合物材料，加速火焰传播及火灾规模的扩大；如果熔融的物质粘在皮肤上，会烫伤皮肤，甚至在去除熔融物质的时候容易把皮肤撕下来。
其中就有很大一部分原因是因为含合成纤维服装燃烧后所熔融滴落对皮肤造成二次伤害，轻则丧失工作能力，严重的会造成的死亡。
对于熔滴现象，在产业工人的一线工作现场经常会接触到火焰或是因为静电、粉尘、化工、机械等场合会出现燃烧火焰、金属飞溅等情况。按照现在的安全配备并不能所有的工人都配备阻燃的防护服，由于合成纤维具有耐磨、挺括等优点和速干等功能。目前常规工装或制服普遍采用合成纤维或合成纤维与纤维素纤维混纺的面料。然而合成纤维或合成纤维与纤维素纤维混纺的面料在燃烧后所产生熔滴会造成皮肤烫伤等二次伤害，熔滴甚至会引发助燃。所以市场上急需一款速干型无熔滴面料，来兼顾以上几个问题。
在工装及制服对面料功能多样性要求愈加增加的背景下，如何使功能性与无熔滴兼顾已成为行业的一大难题。
例如专利公告号为CN206553696U，公告日为2017.10.13的中国实用新型专利公开了一种包括防熔滴表层和驱蚊虫层的防熔滴装饰面料，所述驱蚊虫层采用包芯纱平纹交织而成；所述包芯纱包括芯纱和鞘纱，所述芯纱包括中空纤维，所述中空纤维的空腔内填充有驱虫剂超细粉末，所述鞘纱为棉纱线。
 技术问题
上述实用新型专利的装饰面料存在耐用性和舒适性的问题。
因此，行业需要一款同时能兼顾速干与无熔滴性的面料。
 技术解决方案
本发明的目的是提供速干型无熔滴面料和含有该面料的防护服装，其能通过聚酰胺酯纤维、棉纤维以及聚酯纤维三种纤维混纺的方式，有效制备速干型无熔滴面料。本发明中的混纺面料制备工艺合理有效，混纺面料使用兼具速干性好以及燃烧无熔滴的优点，即使在彻底烧通情况下也没有熔滴，能够使面料在具有速干与无熔滴同时，维持高性价比。
本发明涉及一种速干型无熔滴面料，面料组成包括聚酰胺酯纤维、棉纤维以及聚酯纤维，所述聚酰胺酯纤维的含量为10-50wt%，所述棉纤维的含量为30-85wt%，所述聚酯纤维的含量为5-20wt%，所述聚酰胺酯纤维内含有占纤维总量3wt%以上的聚酰胺。
进一步优选的技术方案在于：所述速干型无熔滴面料用于制作服装。
一种速干型无熔滴面料的制备方法，依次包括以下步骤：
S1、分别制备所述聚酰胺酯纤维、棉纤维以及聚酯纤维这三种纤维的棉条；
S2、经过并条、粗纱、细纱以及络筒工序制得纱线；
S3、所述纱线经过整经、浆纱、穿筘、上机织造以及染色步骤，也可混纺织造制得所述速干型无熔滴面料。
进一步优选的技术方案在于：步骤S1中，三种纤维制备时加入抗静电剂、平滑剂以及集束剂。
进一步优选的技术方案在于：步骤S2中，并条工艺将所述聚酰胺酯纤维、棉纤维以及聚酯纤维制得混纺用所述纱线，制纱工艺可以采用环锭纺、赛洛纺、紧密纺、气流纺或涡流纺的纺纱设备与工艺，通过剑杆织机或是喷气织机单一纱线经纬交织或是经纬不同纱线交织制得混纺机织面料，也可以使用针织经编方式制得混纺针织面料。
进一步优选的技术方案在于：步骤S3中，所述后整操作包括退浆、烧毛、漂白、丝光、染色、后整以及打卷；所述纱线也可以进行针织以及针织后整操作，所述针织后整操作包括前处理、丝光、染色、开副、定型以及打卷。
进一步优选的技术方案在于：按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗前的蒸发速率为≥0.18g/h。
进一步优选的技术方案在于：按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗5次后的蒸发速率为≥0.18g/h。
进一步优选的技术方案在于：按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗前的透湿量为≥10000[g/(㎡•24h)]。
进一步优选的技术方案在于：按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗5次后的透湿量为≥10000[g/(㎡•24h)]。
进一步优选的技术方案在于：按照GB/T5455-2014 标准，所述速干型无熔滴面料经向和纬向无熔滴。
进一步优选的技术方案在于：按照GB/T5455-2014 标准，所述速干型无熔滴面料在燃烧后形成碳化层，普通的棉涤面料会形成熔融滴落。
进一步优选的技术方案在于所述聚酰胺酯纤维的制备方法如下：
S1、在反应器中投入对苯二甲酸、乙二醇以及三醋酸锑，加热加压进行酯化反应；
S2、再在所述反应器中投入尼龙、抗氧化剂以及增白剂，加热搅拌并减压反应，最终得到所述聚酰胺酯纤维，
步骤S1中，按重量计，所述对苯二甲酸为100份，所述乙二醇为60-80份，所述三醋酸锑为0.05-0.07份，所述酯化反应的温度为220-270℃，反应压力为0.1-0.4Mpa，反应时间为1-3h。
进一步优选的技术方案在于：步骤S2中，所述尼龙的粘度为2.0-3.0，重量份为20-50份，所述抗氧化剂的重量份为0.01-0.5份，所述增白剂的重量份为0.01-0.2份，搅拌时间为10min，温度设定为200-300℃，压力控制在30-50min内逐步降至50Pa，反应时间为50-200min，所述尼龙包括PA6、PA11、PA12 以及PA56中的任意一种，所述抗氧化剂为L11、DH201-460、H161以及 ST-1385中的任意一种，所述增白剂为亚磷酸、亚磷酸三甲酯以及次磷酸钠中的任意一种。
进一步优选的技术方案在于所述聚酰胺酯纤维的制备方法如下：在1000t/a聚酯生产装置上，按重量计算，对苯二甲酸100份、乙二醇60份以及三醋酸锑0.06份投入酯化釜中，反应温度控制在240℃，在压力为0.25Mpa条件下酯化反应60min；再在250℃、0.15Mpa条件下反应50min，得对苯二甲酸乙二醇酯；然后反应物料进入缩聚反应釜，投入相对粘度为2.4的PA66尼龙40份、H10抗氧化剂0.1份、磷酸三甲酯0.1份、季戊四醇0.1份，在50min内将釜内真空逐渐建立并达到20000Pa，265℃反应80min；再在260℃、10000Pa下反应20min；再在260℃、2000Pa下反应100min，最终得到所述聚酰胺酯纤维。
 有益效果
本发明通过聚酰胺酯纤维、棉纤维以及聚酯纤维三种纤维混纺的方式，有效制备速干型无熔滴面料。本发明中的混纺面料制备工艺合理有效，混纺面料使用兼具速干性好以及燃烧无熔滴的优点，即使在彻底烧通情况下也没有熔滴，能够使面料在具有速干与无熔滴的同时，维持高性价比。
 附图说明
图1为本发明中速干型无熔滴面料的无熔滴燃烧效果图，图中左侧为现有面料，右侧为本发明中的速干型无熔滴面料。
 本发明的实施方式
实施例1
如附图1所示， C60/T40  32*32  130*70 2/1的速干型无熔滴面料，面料组成包括聚酰胺酯纤维、棉纤维以及聚酯纤维，所述聚酰胺酯纤维的含量为20-50wt%，所述棉纤维的含量为50-75wt%，所述聚酯纤维的含量为5-25wt%，所述聚酰胺酯纤维内含有占纤维总量3wt%以上的聚酰胺。
本申请中的速干是指根据GB/T21655.1-2008的速干性中的蒸发速率和透湿量。无熔滴是指根据GB8965.1-2009 熔融、滴落项
所述速干型无熔滴面料中含有聚酰胺分子的聚酰胺酯纤维，即所述聚酰胺酯纤维的重量含量若低于10wt%，则根据GBT21655.1-2008标准，速干型无熔滴面料的蒸发速率和透湿量下降，若超过50wt%，则由于其它纤维的配合量变的过少，根据GB8965.1-2009 标准该面料将有熔融，滴落，因此确定了上述10-50 wt%的范围。
所述速干型无熔滴面料用于制作服装。
一种速干型无熔滴面料的制备方法，依次包括以下步骤：
S1、分别制备所述聚酰胺酯纤维、棉纤维以及聚酯纤维这三种纤维的棉条；
S2、经过并条、粗纱、细纱以及络筒工序制得三种纤维混纺的32S纱线或是经纬不同纤维混纺的32S纱线；
S3、所述纱线经过整经、浆纱、穿筘、上机织造以及染色步骤，混纺织造制得所述C60/T40  32*32  130*70 2/1速干型无熔滴面料。
步骤S2中，并条工艺将所述聚酰胺酯纤维、棉纤维以及聚酯纤维制得混纺用所述纱线，制纱工艺可以采用环锭纺、赛洛纺、紧密纺、气流纺以及涡流纺的纺纱设备与工艺，通过剑杆织机或是喷气织机单一纱线经纬交织或是经纬不同纱线交织制得混纺机织面料，步骤S3中，所述混纺面料织造完成后进行染色操作，所述后整操作包括退浆、烧毛、漂白、丝光、染色、后整以及打卷。
所述聚酰胺酯纤维的制备方法如下：
不锈钢反应釜中投入按重量计的100份对苯二甲酸、60份乙二醇、三醋酸锑0.05份，反应温度控制235℃、反应压力0.25MPa，进行酯化反应2h；反应后投入相对粘度为2.0的PA6尼龙30份、L11抗氧化剂0.57份、亚磷酸三甲酯增白剂0.38份，搅拌10min，之后温度设定为260℃，压力在45min内逐步降至50Pa，继续反应105min，即得所述聚酰胺酯纤维。
按照GB 12014-2009标准，所述速干型无熔滴面料洗涤100次后的点对点电阻为5.3*106。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗前的蒸发速率为0.28g/h。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗5次后的蒸发速率为0.30g/h。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗前的透湿量为10487[g/(㎡•24h)]。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗5次后的透湿量为10466[g/(㎡•24h)]。
按照GB/T 5455-2014标准，所述速干型无熔滴面料在径向和纬向上均无熔融、滴落。
本发明中，生产出的所述混纺面料均具有速干性好以及燃烧无熔滴的优点，即使在烧通情况下仍然没有滴落风险。
以下所述仅为本发明的较佳实施例，非对本发明的范围进行限定。
实施例2
如附图1所示，C60/T40  32*32  130*70 2/1速干型无熔滴面料，面料组成包括聚酰胺酯纤维、棉纤维以及聚酯纤维，所述聚酰胺酯纤维的含量为25-45wt%，所述棉纤维的含量为55-70wt%，所述聚酯纤维的含量为5-20wt%，所述聚酰胺酯纤维内含有占纤维总量3wt%以上的聚酰胺。
本申请中的速干是指根据GB/T21655.1-2008的速干性中的蒸发速率和透湿量。无熔滴是指根据GB8965.1-2009 熔融、滴落项
所述速干型无熔滴面料中含有聚酰胺分子的聚酰胺酯纤维，即所述聚酰胺酯纤维的重量含量若低于10wt%，则根据GBT21655.1-2008标准，速干型无熔滴面料的蒸发速率和透湿量下降，若超过50wt%，则由于其它纤维的配合量变的过少，根据GB8965.1-2009 标准该面料将有熔融，滴落，因此确定了上述10-50 wt%的范围。
所述速干型无熔滴面料用于制作服装。
一种速干型无熔滴面料的制备方法，其特征在于依次包括以下步骤：
S1、分别制备所述聚酰胺酯纤维、棉纤维以及聚酯纤维这三种纤维的棉条；
S2、经过并条、粗纱、细纱以及络筒工序制得三种纤维混纺的32S纱线或是经纬不同纤维混纺的32S纱线；
S3、所述纱线经过整经、浆纱、穿筘、上机织造以及染色步骤，混纺织造制得所述C60/T40 32*32  130*70 2/1速干型无熔滴面料。
步骤S2中，并条工艺将所述聚酰胺酯纤维、棉纤维以及聚酯纤维制得混纺用所述纱线，制纱工艺可以采用环锭纺、赛洛纺、紧密纺、气流纺以及涡流纺的纺纱设备与工艺，通过剑杆织机或是喷气织机单一纱线经纬交织或是经纬不同纱线交织制得混纺机织面料，步骤S3中，所述混纺面料织造完成后进行染色操作，所述后整操作包括退浆、烧毛、漂白、丝光、染色、后整以及打卷。
所述聚酰胺酯纤维的制备方法如下：
不锈钢反应釜中投入按重量计的100份对苯二甲酸、60份乙二醇、三醋酸锑0.05份，反应温度控制235℃、反应压力0.25MPa，进行酯化反应2h；反应后投入相对粘度为2.0的PA6尼龙30份、L11抗氧化剂0.57份、亚磷酸三甲酯增白剂0.38份，搅拌10min，之后温度设定为260℃，压力在45min内逐步降至50Pa，继续反应105min，即得所述聚酰胺酯纤维。
按照GB 12014-2009标准，所述速干型无熔滴面料洗涤100次后的点对点电阻为5.3*106。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗前的蒸发速率为0.31g/h。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗5次后的蒸发速率为0.34g/h。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗前的透湿量为11450[g/(㎡•24h)]。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗5次后的透湿量为11482[g/(㎡•24h)]。
按照GB/T 5455-2014标准，所述速干型无熔滴面料在径向和纬向上均无熔融、滴落。
本发明中，生产出的所述混纺面料均具有速干性好以及燃烧无熔滴的优点，即使在烧通情况下仍然没有滴落风险。
实施例3
如附图1所示，速干型无熔滴针织汗布面料，面料组成包括聚酰胺酯纤维、棉纤维以及聚酯纤维，所述聚酰胺酯纤维的含量为10-50wt%，所述棉纤维的含量为30-85wt%，所述聚酯纤维的含量为5-20wt%，所述聚酰胺酯纤维内含有占纤维总量3wt%以上的聚酰胺。
本申请中的速干是指根据GB/T21655.1-2008的速干性中的蒸发速率和透湿量。无熔滴是指根据GB8965.1-2009 熔融、滴落项。
所述速干型无熔滴面料中含有聚酰胺分子的聚酰胺酯纤维，即所述聚酰胺酯纤维的重量含量若低于10wt%，则根据GBT21655.1-2008标准，速干型无熔滴面料的蒸发速率和透湿量下降，若超过50wt%，则由于其它纤维的配合量变的过少，根据GB8965.1-2009 标准该面料将有熔融，滴落，因此确定了上述10-50 wt%的范围。
所述速干型无熔滴面料用于制作服装。
一种速干型无熔滴面料的制备方法，其特征在于依次包括以下步骤：
S1、分别制备所述聚酰胺酯纤维、棉纤维以及聚酯纤维这三种纤维的棉条；
S2、经过并条、粗纱、细纱以及络筒工序制得三种纤维混纺的32S纱线；
S3、所述纱线经过牵经、上机织造以及染色步骤，混纺织造制得所述速干型无熔滴针织汗布面料。
步骤S2中，并条工艺将所述聚酰胺酯纤维、棉纤维以及聚酯纤维制得混纺用所述纱线，制纱工艺可以采用环锭纺、赛洛纺、紧密纺、气流纺以及涡流纺的纺纱设备与工艺，通过使用针织经编等方式制得混纺针织速干型无熔滴针织汗布面料。步骤S3中，所述混纺面料织造完成后进行染色操作，所述后整操作包括前处理、丝光、染色、开副、定型以及打卷。
所述聚酰胺酯纤维的制备方法如下：
不锈钢反应釜中投入按重量计的100份对苯二甲酸、60份乙二醇、三醋酸锑0.05份，反应温度控制235℃、反应压力0.25MPa，进行酯化反应2h；反应后投入相对粘度为2.0的PA6尼龙30份、L11抗氧化剂0.57份、亚磷酸三甲酯增白剂0.38份，搅拌10min，之后温度设定为260℃，压力在45min内逐步降至50Pa，继续反应105min，即得所述聚酰胺酯纤维。
按照GB 12014-2009标准，所述速干型无熔滴面料洗涤100次后的点对点电阻为5.3*106。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗前的蒸发速率为0.30g/h。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗5次后的蒸发速率为0.32g/h。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗前的透湿量为11800[g/(㎡•24h)]。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗5次后的透湿量为12130[g/(㎡•24h)]。按照GB/T 5455-2014标准，所述速干型无熔滴面料在径向和纬向上均无熔融、滴落.
本发明中，生产出的所述混纺速干型无熔滴针织汗布面料具有速干性好以及燃烧无熔滴的优点，即使在烧通情况下仍然没有滴落风险。
实施例4
如附图1所示，速干型无熔滴针织珠地网眼布面料，面料组成包括聚酰胺酯纤维、棉纤维以及聚酯纤维，所述聚酰胺酯纤维的含量为10-50wt%，所述棉纤维的含量为30-85wt%，所述聚酯纤维的含量为5-20wt%，所述聚酰胺酯纤维内含有占纤维总量3wt%以上的聚酰胺。
本申请中的速干是指根据GB/T21655.1-2008的速干性中的蒸发速率和透湿量。无熔滴是指根据GB8965.1-2009 熔融、滴落项。
所述速干型无熔滴面料中含有聚酰胺分子的聚酰胺酯纤维，即所述聚酰胺酯纤维的重量含量若低于10wt%，则根据GBT21655.1-2008标准，速干型无熔滴面料的蒸发速率和透湿量下降，若超过50wt%，则由于其它纤维的配合量变的过少，根据GB8965.1-2009 标准该面料将有熔融，滴落，因此确定了上述10-50 wt%的范围。
所述速干型无熔滴面料用于制作服装。
一种速干型无熔滴面料的制备方法，其特征在于依次包括以下步骤：
S1、分别制备所述聚酰胺酯纤维、棉纤维以及聚酯纤维这三种纤维的棉条；
S2、经过并条、粗纱、细纱以及络筒工序制得纱线三种纤维混纺的32S纱线；
S3、所述纱线经过牵经、上机织造以及染色步骤，混纺织造制得所述速干型无熔滴针织珠地网眼布面料。
步骤S2中，并条工艺将所述聚酰胺酯纤维、棉纤维以及聚酯纤维制得混纺用所述纱线，制纱工艺可以采用环锭纺、赛洛纺、紧密纺、气流纺以及涡流纺的纺纱设备与工艺，通过使用针织经编等方式制得混纺针织速干型无熔滴针织珠地网眼布面料。步骤S3中，所述混纺针织珠地网眼布面料织造完成后进行染色操作，所述后整操作包括前处理、丝光、染色、开副、定型以及打卷。
所述聚酰胺酯纤维的制备方法如下：
不锈钢反应釜中投入按重量计的100份对苯二甲酸、60份乙二醇、三醋酸锑0.05份，反应温度控制235℃、反应压力0.25MPa，进行酯化反应2h；反应后投入相对粘度为2.0的PA6尼龙30份、L11抗氧化剂0.57份、亚磷酸三甲酯增白剂0.38份，搅拌10min，之后温度设定为260℃，压力在45min内逐步降至50Pa，继续反应105min，即得所述聚酰胺酯纤维。
按照GB 12014-2009标准，所述速干型无熔滴面料洗涤100次后的点对点电阻为5.3*106。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗前的蒸发速率为0.33g/h。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗5次后的蒸发速率为0.36g/h。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗前的透湿量为13750[g/(㎡•24h)]。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗5次后的透湿量为13620[g/(㎡•24h)]按照GB/T 5455-2014标准，所述速干型无熔滴面料在径向和纬向上均无熔融、滴落。
本发明中，生产出的所述混纺速干型无熔滴针织珠地网眼布面料具有速干性好以及燃烧无熔滴的优点，即使在烧通情况下仍然没有滴落风险。
实施例5
如附图1所示，速干型无熔滴针织珠地网眼弹力布面料，面料组成包括聚酰胺酯纤维、棉纤维以及聚酯纤维，所述聚酰胺酯纤维的含量为10-50wt%，所述棉纤维的含量为30-85wt%，所述聚酯纤维的含量为5-20wt%，所述聚酰胺酯纤维内含有占纤维总量3wt%以上的聚酰胺。
本申请中的速干是指根据GB/T21655.1-2008的速干性中的蒸发速率和透湿量。无熔滴是指根据GB8965.1-2009 熔融、滴落项。
所述速干型无熔滴面料中含有聚酰胺分子的聚酰胺酯纤维，即所述聚酰胺酯纤维的重量含量若低于10wt%，则根据GBT21655.1-2008标准，速干型无熔滴面料的蒸发速率和透湿量下降，若超过50wt%，则由于其它纤维的配合量变的过少，根据GB8965.1-2009 标准该面料将有熔融，滴落，因此确定了上述10-50 wt%的范围。
所述速干型无熔滴针织珠地网眼弹力布面料用于制作服装。
一种速干型无熔滴面料的制备方法，其特征在于依次包括以下步骤：
S1、分别制备所述改性、、聚酰胺酯纤维、棉纤维以及聚酯纤维这三种纤维的棉条；
S2、经过并条、粗纱、细纱以及络筒工序制得纱线三种纤维混纺的32S纱线；
S3、所述纱线经过牵经、添加氨纶弹力丝上机织造以及染色步骤，混纺织造制得所述速干型无熔滴针织珠地网眼弹力布面料。
步骤S2中，并条工艺将所述聚酰胺酯纤维、棉纤维以及聚酯纤维制得混纺用所述纱线，制纱工艺可以采用环锭纺、赛洛纺、紧密纺、气流纺以及涡流纺的纺纱设备与工艺，通过使用针织经编等方式并且在织造过程中添加氨纶弹力纱制得混纺针织速干型无熔滴针织珠地网眼弹力布面料。步骤S3中，所述混纺针织珠地网眼布弹力面料织造时添加氨纶弹力丝，织造完成后进行染色操作，所述后整操作包括前处理、丝光、染色、开副、定型以及打卷。。
所述聚酰胺酯纤维的制备方法如下：
不锈钢反应釜中投入按重量计的100份对苯二甲酸、60份乙二醇、三醋酸锑0.05份，反应温度控制235℃、反应压力0.25MPa，进行酯化反应2h；反应后投入相对粘度为2.0的PA6尼龙30份、L11抗氧化剂0.57份、亚磷酸三甲酯增白剂0.38份，搅拌10min，之后温度设定为260℃，压力在45min内逐步降至50Pa，继续反应105min，即得所述聚酰胺酯纤维。
按照GB 12014-2009标准，所述速干型无熔滴面料洗涤100次后的点对点电阻为5.3*106。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗前的蒸发速率为0.32g/h。按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗5次后的蒸发速率为0.35g/h。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗前的透湿量为13260[g/(㎡•24h)]。按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗5次后的透湿量为13540[g/(㎡•24h)]按照GB/T 5455-2014标准，所述速干型无熔滴面料在径向和纬向上均无熔融、滴落.
本发明中，生产出的所述混纺速干型无熔滴针织珠地网眼布面料具有速干性好以及燃烧无熔滴的优点，即使在烧通情况下仍然没有滴落风险。
对本发明中最终的所述速干性无熔滴面料依照GB8965.1-2009进行燃烧测试，看是否有熔滴现象。
对本发明中最终的所述速干性无熔滴面料依照GB/T21655.1-2008的速干性中的蒸发速率和透湿量进行速干性测试，看是否有速干性能。
上述实施例的速干性测试数据如下：
Figure 783703dest_path_image001
以上对本发明的实施方式作了详细说明，但是本发明并不限于上述实施方式，在所述技术领域普通技术人员所具备的知识范围内，还可以在不脱离本发明宗旨的前提下做出各种修改。这些都是不具有创造性的修改，只要在本发明的权利要求范围内均受到专利法的保护。

Claims (10)

  1. 速干型无熔滴面料，其特征在于：面料组成包括聚酰胺酯纤维、棉纤维以及聚酯纤维，所述聚酰胺酯纤维的含量为10-50wt%，所述棉纤维的含量为30-85wt%，所述聚酯纤维的含量为5-20wt%，所述聚酰胺酯纤维内含有占纤维总量3wt%以上的聚酰胺。
  2. 根据权利要求1所述的速干型无熔滴面料，其特征在于：按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗前的蒸发速率为≥0.18g/h。
  3. 根据权利要求1所述的速干型无熔滴面料，其特征在于：按照GB/T 21655.1-2008 条款8.3标准，所述速干型无熔滴面料洗5次后的蒸发速率为≥0.18g/h。
  4. 根据权利要求1所述的速干型无熔滴面料，其特征在于：按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗前的透湿量为≥10000g/(㎡•24h)。
  5. 根据权利要求1所述的速干型无熔滴面料，其特征在于：按照GB/T 21655.1-2008 标准，所述速干型无熔滴面料洗5次后的透湿量为≥8000g/(㎡•24h)；按照GB/T5455-2014 标准，所述速干型无熔滴面料经纬向无熔滴。
  6. 一种如权利要求1所述的速干型无熔滴面料的制备方法，其特征在于依次包括以下步骤：
    S1、分别制备所述聚酰胺酯纤维、棉纤维以及聚酯纤维这三种纤维的棉条；
    S2、经过并条、粗纱、细纱以及络筒工序制得纱线；
    S3、所述纱线经过整经、浆纱、穿筘、上机织造以及后整步骤，混纺织造制得所述速干型无熔滴面料。
  7. 根据权利要求6所述的速干型无熔滴面料的制备方法，其特征在于：步骤S1中，三种纤维制备时加入抗静电剂、平滑剂以及集束剂。
  8. 根据权利要求6所述的速干型无熔滴面料的制备方法，其特征在于：步骤S2中，并条工艺将所述聚酰胺酯纤维、棉纤维以及聚酯纤维制得混纺用所述纱线，制纱工艺可以采用环锭纺、赛洛纺、紧密纺、气流纺以及涡流纺的纺纱设备与工艺，通过剑杆织机或是喷气织机单一纱线经纬交织或是经纬不同纱线交织制得混纺机织面料，也可以使用针织经编方式制得混纺针织面料。
  9. 根据权利要求6所述的速干型无熔滴面料的制备方法，其特征在于：步骤S3中，所述后整操作包括退浆、烧毛、漂白、丝光、染色、后整以及打卷；所述纱线也可以进行针织以及针织后整操作，所述针织后整操作包括前处理、丝光、染色、开副、定型以及打卷。
  10. 如权利要求1所述的速干型无熔滴面料的应用，其特征在于：用于制作服装。
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