WO2018139068A1 - Procédé de fabrication de matière première de tabac, et matière première de tabac - Google Patents

Procédé de fabrication de matière première de tabac, et matière première de tabac Download PDF

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Publication number
WO2018139068A1
WO2018139068A1 PCT/JP2017/044045 JP2017044045W WO2018139068A1 WO 2018139068 A1 WO2018139068 A1 WO 2018139068A1 JP 2017044045 W JP2017044045 W JP 2017044045W WO 2018139068 A1 WO2018139068 A1 WO 2018139068A1
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Prior art keywords
tobacco
raw material
content
leaf
smoke
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PCT/JP2017/044045
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English (en)
Japanese (ja)
Inventor
真里那 藤平
研児 伊藤
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日本たばこ産業株式会社
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Application filed by 日本たばこ産業株式会社 filed Critical 日本たばこ産業株式会社
Priority to JP2018564143A priority Critical patent/JP6832960B2/ja
Priority to EP17893982.3A priority patent/EP3556227A4/fr
Priority to CN201780085103.4A priority patent/CN110290713B/zh
Publication of WO2018139068A1 publication Critical patent/WO2018139068A1/fr
Priority to US16/524,807 priority patent/US20190350251A1/en

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    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/183—Treatment of tobacco products or tobacco substitutes sterilization, preservation or biological decontamination
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00—Preparing tobacco in the factory
    • A24B3/12—Steaming, curing, or flavouring tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B9/00—Control of the moisture content of tobacco products, e.g. cigars, cigarettes, pipe tobacco

Definitions

  • the present invention relates to a method for producing a tobacco raw material and a tobacco raw material.
  • Non-Patent Document 1 a cigarette chopstick or wood smoke is passed through to give a unique scent, and at that time, the rice husk is slowly heated, burned slowly and scalded, and smoked.
  • DFC Dark Fire Cured
  • the general manufacturing method includes a step of performing smoke treatment with smoke generated by burning wood or the like at a heating / combustion temperature of about 600 to 900 ° C. on a fresh tobacco leaf that has not undergone a drying treatment, and thereafter It is known to include a fermentation process and a process of storing it through a aging process.
  • Patent Document 1 describes a tobacco product using an extract of fire-cured tobacco, and the content of benzo [a] pyrene contained in normal fire-dried tobacco is described in the document, It is described to be about 150 to about 800 ng / g.
  • Patent Document 2 an alcohol such as ethyl alcohol is added to smoked dried leaf tobacco, and thereafter, the organic acid added by smoked processing is stored by storing the alcohol-added leaf tobacco. It is described that an esterification reaction is caused with an alcohol added in step 1 to form an ester compound.
  • Non-Patent Document 1 only describes a normal smoking means as a method for imparting a unique scent to a tobacco raw material such as cigarette chopping.
  • smoked processing is performed on dry leaf tobacco by providing the organic acid contained in the smoke to dry leaf tobacco, thereby providing the substrate in the subsequent esterification reaction to dry leaf tobacco. Therefore, the object of the invention is to increase the ester compound in the tobacco raw material.
  • the adhesion of benzo [a] pyrene to leaf tobacco which may occur when performing a conventional smoke treatment that has been conventionally performed, is suppressed, the content of low-molecular carboxylic acid is reduced, It is an object to provide a tobacco raw material with a specific flavor component increased and a method for producing the same.
  • the dried leaf tobacco before deboning has a product temperature of 400 to A step of smoking treatment with smoke obtained by pyrolyzing the smoke generating material in a range of 500 ° C., and a step of storing the smoked and processed leaf tobacco under semi-sealed conditions following the step of smoking.
  • the present invention has been found to provide a tobacco raw material that contains a small amount of benzo [a] pyrene and low-molecular carboxylic acid and contains a lot of specific flavor components.
  • the embodiment of the present invention is as follows. [1] A step of drying leaf tobacco before harvesting before removing bone until the water content becomes 10 to 25% by weight, and the dried leaf tobacco before removing bone in a range where the product temperature is 400 to 500 ° C. A process for smoking a smoke-producing material with pyrolyzed smoke, and a process for storing the smoked smoking-treated leaf tobacco under a semi-sealed condition following the smoking process. Production method. [2] The method for producing a tobacco raw material according to [1], wherein when the leaf tobacco after harvesting is dried, the leaf tobacco is dried until the water content becomes 15 to 25% by weight.
  • the content of benzo [a] pyrene is 100 ng / g or less based on the dry weight of the tobacco material
  • the content of acetic acid is 20 mg / g or less based on the dry weight of the tobacco material (3 )
  • the content of guaiacol is 5 to 5000 ⁇ g / g based on the dry weight of the tobacco raw material
  • the content of 2,6-dimethoxyphenol is 10 to 10,000 ⁇ g / g based on the dry weight of the tobacco raw material
  • the content of benzo [a] pyrene is 100 ng / g or less based on the dry weight of the tobacco material
  • the content of acetic acid is 20 mg / g or less based on the dry weight of the tobacco material (3 )
  • the content of guaiacol is 5 to 5000 ⁇ g / g based on the dry weight of the tobacco raw material
  • the content of 2,6-dimethoxyphenol is 10 to 10,000 ⁇ g / g based on the dry weight of the tobacco raw material
  • a tobacco product comprising the tobacco raw material described in [5].
  • the tobacco product according to [6] which is a cigarette or a heated flavor inhaler.
  • a tobacco raw material having a low content of benzo [a] pyrene and a low-molecular carboxylic acid and containing a large amount of specific flavor components, and a method for producing the same.
  • FIG. 1 shows a normal manufacturing process of a smoking article such as a cigarette.
  • the harvested tobacco is stored in a warehouse through a process called curing.
  • This curing is a process performed at an early stage on harvested leaf tobacco, and usually includes processes such as drying and humidity conditioning, and may activate the functions of various enzymes contained in leaf tobacco. is there. Curing is performed mainly for the following purposes. (1) Enhancing the action of the enzyme and promoting the change in leaf color. (2) Dry the mesophyll and fix the leaf color. (3) Drain the water from the middle bone and dry the entire leaf. After this curing, leaf tobacco is transported to a raw material factory after being stored in a warehouse for a certain period. In addition, when curing is performed, the deboning or separation operation of the leaf tobacco is not performed, and the processing such as the deboning is performed in the raw material factory.
  • the production method according to the embodiment of the present invention is performed in place of the above-described curing process, and the tobacco raw material obtained through the production method according to the embodiment of the present invention is usually stored in a warehouse. After that, it is transported to the raw material factory.
  • the manufacturing method described in Patent Document 2 is performed on a tobacco raw material that has been processed in the raw material factory shown in FIG. This is because when the tobacco raw material obtained by the production method described in Patent Document 2 is subjected to a treatment usually performed in the raw material factory shown in FIG. 1, the ester compound contained in the tobacco raw material is heated by re-drying or the like. It is because it will volatilize by performing the process accompanied by.
  • leaf tobacco processed by the manufacturing method described in Patent Document 2 is a “cigarette cut” that is assumed to have been processed at the raw material factory in FIG. From this, the manufacturing method described in Patent Document 2 and the manufacturing method according to the embodiment of the present invention are completely different from each other.
  • leaf tobacco refers to the one before or during the processing of the steps included in the production method of the present invention, and “tobacco raw material” is processed. Point to.
  • the leaf tobacco before harvesting which is used for the tobacco raw material according to the embodiment of the present invention, is the one before discoloration such as yellowing after “harvest” shown in FIG. 1, and Leaf tobacco before the “curing” process is performed, and is before deboning.
  • the leaf tobacco used in the production method according to the embodiment of the present invention and the tobacco raw material described below is not particularly limited, and belongs to the genus Nicotiana, Nicotiana tabacum Burley species, yellow species, Orient species, native species, Nicotiana rustica Can be mentioned.
  • leaf tobacco after harvesting it is particularly preferable to use the leaf tobacco immediately after harvesting, and it is preferable to perform the drying treatment described later on such leaf tobacco immediately after harvesting.
  • the water content of leaf tobacco (raw leaves) after harvesting is usually high and has a water content of 80 to 90% by weight with respect to the total amount of leaf tobacco. Such leaf tobacco is dried until the water content becomes 10 to 25% by weight.
  • the lower limit of the water content of the leaf tobacco obtained through the drying treatment is more preferably 12% by weight, and particularly preferably 15% by weight.
  • the range of the moisture content of the leaf tobacco is 15 to 25% by weight, the effect of increasing the content (attachment amount) of a specific flavor component imparted by soot is particularly excellent.
  • 20 weight% can also be mentioned as an upper limit of the moisture content of leaf tobacco.
  • Specific flavor components include guaiacol and 2,6-dimethoxyphenol.
  • the sample is heated at 100 ° C. for 1 hour under normal pressure, allowed to cool in a desiccator for 40 minutes, and moisture is determined from the weight difference before and after heating.
  • the specific procedure is as follows. (1) Measure the empty weight of the sample container stored in the desiccator. (2) Weigh the required amount of tobacco and place it in the sample container and cover it. (3) Open the lid of the sample container, arrange in a rotary dryer, and heat at 100 ° C. for 1 hour. (4) After 1 hour, the lid of the sample container is closed and taken out and allowed to cool in a desiccator. (5) After 40 minutes, the weight of the sample container is measured. The moisture is obtained from the following formula.
  • the method for the drying treatment is not particularly limited, and examples thereof include the following methods. Leave the cigarettes in a dry room where the direct sunlight such as a pipe house is non-permeable for about 1 month, 20-50, so that the air is convection naturally and the dryness is not uneven.
  • a method of natural drying at about 25 ° C. to 35 ° C. is preferable although it varies depending on the production area.
  • Another example is a method of drying for about 5 days at a temperature of about 30 to 70 ° C. and a relative humidity of about 20 to 100% in an apparatus such as a circulating bulk dryer capable of controlling temperature and humidity. Moreover, you may use both said methods together.
  • a method of drying for several hours by an apparatus having a drying temperature in the apparatus cabinet of about 100 ° C. can be mentioned.
  • the smoke generating material is heated so that the smoke producing material such as wood has a temperature of 400 to 500 ° C. in order to generate smoke.
  • a specific polycyclic aromatic compound with a large amount of adhering to leaf tobacco is used in DFC by heating in a range where the product temperature of the smoke generating material is 400 to 500 ° C.
  • the adhesion amount of hydrocarbons such as benzo [a] pyrene can be reduced.
  • by heating the smoke generating material so as to have a product temperature of 400 ° C.
  • Wood can be used as the soot generation material, and the type thereof is not particularly limited, and examples thereof include white oak, cherry blossom, walnut, apple, beach beech, oak and hickory.
  • the time for the smoke treatment can be appropriately adjusted, for example, for about 10 minutes to 6 months. Any of the smoking processes can be performed using a known smoking apparatus or a heating device. In the smoke treatment, there can be exemplified an aspect in which leaf tobacco is stacked and an aspect in which leaf tobacco is continuously dried or trunk-dried.
  • the DFC manufacturing method described above includes a fermentation process and an aging process before the storing process after the smoke treatment, but in the present invention, such a fermentation process and an aging process are included. Not included.
  • the manufacturing method of this invention does not include the process of adding alcohol in order to produce
  • the step of storing the smoked and processed bone tobacco before deboning is performed under semi-sealed conditions so that low molecular carboxylic acids such as acetic acid are volatilized during storage.
  • Semi-sealed conditions include, for example, a mode in which smoked leaf tobacco is placed in an air permeable packaging material such as a plastic bag and the inlet of the packaging material is folded to prevent air inflow and out to some extent. it can.
  • a large number of leaf tobaccos may be stored at a time by preparing a plurality of packaging materials containing leaf tobacco and stacking and storing them in a storage container.
  • the low molecular carboxylic acid such as acetic acid that can cause irritation
  • the storage period is not particularly limited as long as the low molecular carboxylic acid such as acetic acid is sufficiently reduced, but is preferably 3 months or more.
  • the upper limit of the storage period is preferably about 24 months in consideration of the period until the produced tobacco raw material is shipped to the raw material factory.
  • the temperature at the time of storage is preferably a temperature at which volatilization of the low-molecular carboxylic acid occurs sufficiently.
  • Specific temperature can include room temperature.
  • a specific temperature range a range of 5 to 60 ° C. can be exemplified, and an embodiment in which the temperature is appropriately set within a range of 10 to 55 ° C. can also be exemplified.
  • additives such as essential oils and extract fragrances can be added in any amount in any step except between the step of smoke treatment and the step of storing.
  • the moisture content of the tobacco raw material can be adjusted to 10 to 20% by weight, preferably 10 to 15% by weight, based on the total amount of the tobacco raw material.
  • the manufacturing method according to the embodiment of the present invention is performed before the processing at the tobacco raw material factory shown in FIG.
  • the tobacco raw material obtained with the manufacturing method of this invention is normally transported to a tobacco raw material factory through storage in a warehouse (refer FIG. 1).
  • the storage in the warehouse at that time is usually about 10 to 180 days.
  • a tobacco raw material having the same component content as the ⁇ tobacco raw material> described below can be obtained.
  • the tobacco raw material concerning embodiment of this invention can be manufactured by the manufacturing method of the tobacco raw material of this invention demonstrated above, for example.
  • the leaf tobacco which comprises the tobacco raw material concerning embodiment of this invention it is a thing before performing the deboning in the raw material factory shown in FIG. 1, and the lamina and the middle bone are not separation-processed (it is not stressed) ) Consists of leaf tobacco.
  • the kind of leaf tobacco which comprises the tobacco raw material concerning embodiment of this invention it may be the same kind as what is used with said manufacturing method.
  • the tobacco raw material according to the embodiment of the present invention has the following configurations (1) to (4).
  • the content of benzo [a] pyrene is 100 ng / g or less based on the dry weight of the tobacco raw material.
  • the acetic acid content is 20 mg / g or less based on the dry weight of the tobacco raw material.
  • the content of guaiacol is 5 to 5000 ⁇ g / g based on the dry weight of the tobacco raw material.
  • the content of 2,6-dimethoxyphenol is 10 to 10,000 ⁇ g / g based on the dry weight of the tobacco raw material.
  • the content of benzo [a] pyrene is more preferably 50 ng / g or less on a dry weight basis, and particularly preferably the detection limit or less.
  • the content of benzo [a] pyrene is within such a range, the added amount of harmful substances contained in the smoke is small.
  • the content of benzo [a] pyrene in the tobacco raw material according to the embodiment of the present invention adjusts the product temperature of the smoke generating material when performing the smoke treatment when producing the tobacco raw material by the above-described manufacturing method. You can adjust it.
  • the content of the specific polycyclic aromatic hydrocarbon is adjusted within the above range by adjusting the product temperature to be in the range of 400 to 500 ° C. Can fit inside.
  • the content of acetic acid is preferably 20 mg / g or less, particularly preferably 15 mg / g or less, on a dry weight basis.
  • the tobacco raw material of the present invention may contain 10 ⁇ g / g or more of acetic acid.
  • the content of propionic acid is preferably 1 mg / g or less, particularly preferably 0.5 mg / g or less, on a dry weight basis.
  • the tobacco raw material of the present invention can include an embodiment in which 10 ⁇ g / g or more of propionic acid is contained.
  • the content of acetic acid and propionic acid in the tobacco raw material according to the embodiment of the present invention can be adjusted by adjusting the storage temperature and time when the tobacco raw material is produced by the above-described production method. For example, if the storage time is lengthened, the amount of the low molecular carboxylic acid to be volatilized increases, so that the content of the low molecular carboxylic acid in the tobacco raw material can be further reduced.
  • the tobacco raw material concerning embodiment of this invention can be manufactured by the manufacturing method concerning embodiment of this invention demonstrated above, in the manufacturing method concerning embodiment of this invention, it describes in patent document 2 It does not include a step of adding an alcohol for producing an ester compound. Therefore, the tobacco raw material according to the embodiment of the present invention does not substantially contain the ester compound described in Patent Document 2, such as ethyl acetate and ethyl valerate. “Substantially free” means below the detection limit.
  • the content of guaiacol is more preferably 5 to 5000 ⁇ g / g, and particularly preferably 100 to 1500 ⁇ g / g, based on the dry weight.
  • the content of 2,6-dimethoxyphenol is more preferably 10 to 10,000 ⁇ g / g, and particularly preferably 500 to 2000 ⁇ g / g, based on the dry weight.
  • Guaiacol and 2,6-dimethoxyphenol are components unique to soot and give the user a smoky, scent, taste, and savory taste that impacts the perception of the mouth through the nasal cavity It is an ingredient.
  • the content of guaiacol and 2,6-dimethoxyphenol in the tobacco raw material according to the embodiment of the present invention can be adjusted by adjusting the time required for the smoke treatment when producing the tobacco raw material by the above-described manufacturing method. For example, when it is desired to add more of these components, the time for the smoke treatment is increased.
  • the content ratio of 2,6-dimethoxyphenol and guaiacol (hereinafter also referred to as 2,6-DMP / G ratio) is preferably 1-20. 2 to 15 is more preferable, and 2 to 10 is particularly preferable.
  • 2,6-DMP / G ratio is in the above range, it is possible to give the user a good balance of smokyness, impact on the scent and taste peculiar to tobacco materials, and perception from the oral cavity to the nasal cavity.
  • the 2,6-DMP / G ratio can be adjusted, for example, by changing (smoked conditions (wood chip type, thermal decomposition temperature, etc.) and storage conditions (temperature, degree of contact with air, duration, etc.). it can.
  • the temperature of the smoke generating material in the smoking process is increased, the temperature is lowered, and when the temperature is increased among the storage conditions, the 2,6-DMP / G ratio is increased.
  • the 2,6-DMP / G ratio increases as the degree of contact with air increases. Further, when the storage period is lengthened, the 2,6-DMP / G ratio is increased.
  • the moisture content of the leaf tobacco is considerably higher than that of the leaf tobacco of the present invention, and the amount of 2,6-dimethoxyphenol attached to the leaf tobacco is reduced.
  • the product temperature of the smoke generating material during the smoke treatment is higher than that of the present invention, and this tends to decrease 2,6-DMP / G. Therefore, in the conventional DFC, the 2,6-DMP / G ratio is estimated to be smaller than 1, which is the lower limit value of the above range.
  • the ratio of the content of 2,6-dimethoxyphenol to phenol is preferably 1 to 100, and preferably 5 to 70 is more preferable, and 20 to 50 is particularly preferable.
  • the 2,6-DMP / P ratio is in such a range, the smoky feeling is more emphasized.
  • This 2,6-DMP / P ratio becomes lower, for example, when the product temperature of the smoke generating material in the process of smoking is increased, and becomes lower as the storage period is extended. Moreover, if the temperature at the time of storage is made high, it will become low.
  • the drying process is not performed before the smoke treatment, the moisture content of the leaf tobacco is considerably higher than that of the leaf tobacco of the present invention, and the amount of 2,6-dimethoxyphenol attached to the leaf tobacco is reduced. Therefore, in the conventional DFC, the 2,6-DMP / P ratio is estimated to be smaller than 1, which is the lower limit value of the above range.
  • the ratio of the content of guaiacol and phenol is preferably 0.5 to 12.0, and preferably 0.5 to 6.0. Is more preferable, and 2.0 to 5.0 is particularly preferable.
  • G / P ratio is in such a range, a smoky feeling is emphasized.
  • the G / P ratio decreases as the product temperature of the smoke generating material in the process of smoking is increased, and the G / P ratio decreases as the temperature increases in the storage conditions.
  • the moisture content in the tobacco raw material according to the embodiment of the present invention may be 10 to 20% by weight, and preferably 10 to 15% by weight.
  • the content of polycyclic aromatic hydrocarbons (benzo [a] pyrene) in tobacco raw materials can be determined by the following method. Accurately weigh 0.5 g of dried tobacco into a glass screw vial (20 ml capacity), add 200 ⁇ l of internal standard substance (deuterium of each polycyclic aromatic hydrocarbon), and add 10 ml of cyclohexane as an extraction solvent. Cover and extract with shaking at 190 rpm for 30 minutes at room temperature. The supernatant is filtered through a 0.45 ⁇ m membrane filter, concentrated to 1 ml, purified and concentrated with an SPE solid phase extraction column (SPE: Si 2 g / 12 cc, Na 2 SO 4 ), and dispensed into a GC vial.
  • SPE SPE solid phase extraction column
  • the sample is analyzed by GCMS with an autosampler, and the amount of each target component in the sample is quantified by an internal standard method.
  • the following conditions can be used for GC / MS conditions.
  • ⁇ GC / MS analysis conditions> Apparatus: Gas chromatograph analyzer (5975N) manufactured by Agilent Inlet conditions: inlet temperature -300 ° C, injection method-pulsed splitless, injection volume-1 ⁇ L Analytical column: DB-17ms manufactured by Agilent, Inc. 30 m ⁇ 0.25 mm ⁇ 0.25 ⁇ m Column flow rate: 1.2 mL / min. (He) Temperature rising condition: 60 ° C. (1 min.)-15 ° C./min.-150° C. (0.5 min.)-5 ° C./min. -320 ° C (18.5 min.) Run time (60 min.) MS conditions: ion source -300 ° C, quadrupole -180 ° C, SIM mode
  • the content of low-molecular carboxylic acids such as acetic acid in tobacco raw materials and the content of flavor components (guaiacol, 2,6-dimethoxyphenol, phenol) in tobacco raw materials can be determined by the following methods. Accurately weigh 0.5 g of the dried and ground tobacco material into a glass screw vial (20 ml capacity), and add 0.05 ⁇ g of quinoline as an internal standard substance. Add 10 ml of methanol as an extraction solvent, cap and extract with shaking at 200 rpm for 60 minutes at room temperature. The supernatant is filtered through a 0.45 ⁇ m membrane filter, transferred to a GC vial, and analyzed by GC / MS with an autosampler.
  • the ratio of the analysis target component of the obtained GC chromatogram and the peak area of quinoline is obtained, and the amount of the analysis target component contained in each sample is quantified.
  • the following conditions can be used for GC / MS conditions.
  • Apparatus Gas chromatograph analyzer manufactured by Agilent (6890N), mass detector manufactured by Agilent (5973N) Injection volume: 1 ⁇ l (injected in pulsed splitless mode) Column: HP-INNOWAX (30 m ⁇ 0.25 mm (film thickness 0.25 ⁇ m)) manufactured by Agilent Oven: 40 ° C. ⁇ 260 ° C. (5 ° C./min) Mass detector: TIC mode (mass number 29-550)
  • the tobacco raw material according to the embodiment of the present invention is the one before the bone removal, and the lamina and the middle bone remain as they are. Therefore, when the tobacco raw material according to the embodiment of the present invention is used for the manufacture of the tobacco product exemplified below, the raw material factory shown in FIG. Available. That is, the manufacturing method of said tobacco raw material can mention the aspect which includes the process of deboning and isolation
  • the raw material shipped from the raw material factory shown in FIG. 1 may be mixed with an ordinary tobacco raw material, for example, at an arbitrary ratio in the manufacturing factory, and a cigarette may be produced using the mixed raw material.
  • the tobacco raw material concerning embodiment of this invention in the filter part of a well-known cigarette, for example, mixing with a normal tobacco engraving in arbitrary ratios.
  • an arrangement of the filter portion for example, an arrangement in the cavity or an arrangement in which the filter portion is dispersed in the filter fiber can be used.
  • the tobacco raw material concerning embodiment of this invention can also be used for a heating type flavor suction device or a non-heating type flavor suction device. When the tobacco raw material concerning embodiment of this invention is applied to a cigarette or a heating-type flavor suction device, a user can enjoy the flavor resulting from said specific flavor component.
  • the “heated flavor inhaler” is an aspirator that heats a tobacco material without burning it, and allows the user to taste the flavor of the heated tobacco material by suction, for example, heating the tobacco material with the combustion heat of a carbon heat source Carbon heat source aspirator (see for example WO 2006/073065); an electrically heated aspirator with an aspirator and a heating device for electrically heating the aspirator (for example see WO 2010/110226); or containing tobacco material And a liquid atomizing type aspirator that atomizes a liquid aerosol source by heating (see, for example, WO2015 / 046385).
  • the electric heating type flavor inhaler includes a mouthpiece, a container in which a composition containing a tobacco raw material and a main body including an electronic heater, a temperature controller for adjusting the temperature of the electronic heater, and the like.
  • a container in which a composition containing a tobacco raw material and a main body including an electronic heater, a temperature controller for adjusting the temperature of the electronic heater, and the like.
  • the one described in JP 2014-524313 A can be used.
  • a pod can be mentioned as a container in which a composition containing a tobacco raw material is stored, for example.
  • the tobacco raw material according to the embodiment of the present invention is mixed in an arbitrary ratio with, for example, a normal tobacco cut and stored in the above container. Also good.
  • the material of the container in which the tobacco raw material concerning the embodiment of this invention is accommodated is not restrict
  • the tobacco raw material according to the embodiment of the present invention is applied to the above-described heating type flavor inhaler, for example, the tobacco raw material according to the embodiment of the present invention is mixed with, for example, a normal tobacco engraver at an arbitrary ratio. It is accommodated in said container as a composition containing what mixed, polyhydric alcohols, such as glycerol and / or propylene glycol, a thickener, and other components, such as a fragrance
  • an embodiment including a tobacco raw material according to an embodiment of the present invention, a polyhydric alcohol, and a thickener can be preferably exemplified.
  • a tobacco raw material according to an embodiment of the present invention a polyhydric alcohol, and a thickener
  • the weight percentage of the tobacco raw material according to the embodiment of the present invention in the composition filled in the container can be about 10 to 40%.
  • a liquid atomization type aspirator that atomizes a liquid aerosol source containing a tobacco raw material by heating
  • a raw material for producing a liquid flavor source incorporated in a liquid container the embodiment of the present invention is used.
  • tobacco raw materials may be used.
  • the tobacco raw material according to the embodiment of the present invention is an oral tobacco product
  • snus can be cited as an example.
  • the tobacco raw material produced by the above-described manufacturing method is filled with, for example, a normal tobacco engraved in an arbitrary ratio into a packaging material using a raw material such as a nonwoven fabric by a known method. It is obtained with.
  • the amount of tobacco material is adjusted and filled, and sealed by means such as heat sealing to obtain snus.
  • the packaging material can be used without any particular limitation, but a cellulose-based nonwoven fabric is preferably used.
  • the gum when used as the oral tobacco product, it is obtained by mixing the tobacco raw material obtained using the production method according to the embodiment of the present invention with a known gum base and a known method.
  • Chewing tobacco, snuff, and compressed tobacco can also be obtained using a known method, except that the tobacco raw material obtained using the production method according to the embodiment of the present invention is used.
  • an edible film can also be obtained using a known material or method, except that the tobacco raw material obtained using the production method according to the embodiment of the present invention is used.
  • the production method according to the embodiment of the present invention has been a problem with tobacco raw materials that have undergone conventional smoke processing such as DFC, for example, polycyclic aroma contained in smoke produced at a temperature at which incomplete combustion is likely to occur. While the problem of aromatic hydrocarbons adhering to leaf tobacco and the problem of generating substances that give irritating sensations such as acetic acid have been solved, tobacco raw materials with increased components that have the characteristic flavor of smoke Can be provided. Moreover, you may use the tobacco raw material manufactured by the method of this invention as a part of tobacco raw material in tobacco products.
  • the tobacco raw material obtained by this invention can be used in arbitrary ratios, when using it as a part of tobacco raw material in tobacco products.
  • Example 1 Drying of leaf tobacco Leaf tobacco immediately after harvesting was dried or trunk-dried, and then naturally dried in a drying room where direct sunlight was not permeable in the range of 25 ° C. to 35 ° C. for about one month. The water content of the dried leaf tobacco was adjusted to 5 to 50% by weight for each sample.
  • a compact smoker (manufactured by Snow Peak Co., Ltd.) was used for the smoked and smoked tobacco apparatus. About 20 g of wood chips were put on the bottom surface, and about 10 g of the leaf tobacco before deboning, which had been dried as described above, was stacked on top and covered. It was installed on a heating device capable of controlling the temperature (manufactured by ASONE Co., Ltd., hot plate CHR-250DN) so that the bottom surface of the smoke-making device was grounded. Next, the preset temperature of the heating device was set to 500 ° C., and the wood chips were pyrolyzed. The thermal decomposition time of the wood chip was 10 minutes, and white oak, walnut, hickory, oak or walnut was used as the smoke generating material. The product temperature of the smoke generating material was adjusted to be about 300 ° C to 600 ° C.
  • the raw material after smoked processing was put into a plastic bag with a storage processing zipper for leaf tobacco (produced by Nihon-sha) and lamizip AL-E (produced by Nihon-sha).
  • the upper part of the plastic bag with the zipper was closed to a slight degree to make it a semi-sealed system.
  • the upper part of Lam Zip AL-E was heat-sealed to make a completely sealed system.
  • FIG. 3 shows the measurement results of guaiacol. As is apparent from FIG. 3, it was found that a large amount of guaiacol was contained in the leaf tobacco when the product temperature of the smoke generating material was 400 to 500 ° C., and the most guaiacol was contained at 450 ° C. FIG. 3 also shows the content of guaiacol contained in the original raw material and the content of guaiacol contained in the conventional DFC for comparison. As shown in FIG. 3, guaiacol is hardly contained in the original raw material. This is because guaiacol is produced by thermal decomposition of lignin and is imparted to leaf tobacco by smoke processing.
  • FIG. 4 shows the content of 2,6-dimethoxyphenol contained in the original raw material and the content of 2,6-dimethoxyphenol contained in the conventional DFC for comparison. As shown in FIG. 4, the raw material is almost free of 2,6-dimethoxyphenol. This is because 2,6-dimethoxyphenol is produced by thermal decomposition of lignin and is given to leaf tobacco by smoke treatment.
  • Table 2 The contents of guaiacol and 2,6-dimethoxyphenol are summarized in Table 2 below.
  • the smoked product 1 is heated using a hot plate 2 to be smoked, and the amounts of guaiacol and 2,6-dimethoxyphenol adhering to the leaf tobacco 3 and guaiacol and 2,6-dimethoxyphenol adhering to the filter 4 are measured. Each was measured.
  • the adhesion efficiency was calculated by the following formula.
  • Adhesion efficiency (%) Amount of guaiacol or 2,6-dimethoxyphenol adhering to leaf tobacco / (Amount of guaiacol or 2,6-dimethoxyphenol adhering to leaf tobacco + Amount of guaiacol or 2,6-dimethoxyphenol adhering to filter) ⁇ 100
  • the horizontal axis represents the moisture content after the drying treatment (before the smoke treatment)
  • the vertical axis represents the deposition efficiency as FIGS. 6 and 7, respectively.
  • a tobacco raw material having a low content of low-molecular carboxylic acids such as benzo [a] pyrene and acetic acid or propionic acid and containing a large amount of specific flavor components. it can.
  • low-molecular carboxylic acids such as benzo [a] pyrene and acetic acid or propionic acid

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

L'invention concerne une matière première de tabac ayant une faible teneur en hydrocarbures aromatiques polycycliques spécifiés et en acides carboxyliques de faible poids moléculaire et contenant une grande quantité de composants aromatiques spécifiés, ainsi qu'un procédé de fabrication de la matière première de tabac. L'objectif est atteint grâce à un procédé de fabrication comprenant : une étape consistant à sécher le tabac à feuilles préalablement écôtées après récolte jusqu'à ce que sa teneur en humidité atteigne 10 à 25 % en poids ; une étape consistant à traiter par de la fumée le tabac séché préalablement écôté à l'aide de fumée décomposée thermiquement à 400-500 °C ; et une étape consistant, après l'étape de traitement par de la fumée, à stocker le tabac à feuilles préalablement écoté et traité par de la fumée dans des conditions partiellement hermétiques.
PCT/JP2017/044045 2017-01-30 2017-12-07 Procédé de fabrication de matière première de tabac, et matière première de tabac WO2018139068A1 (fr)

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JP2018564143A JP6832960B2 (ja) 2017-01-30 2017-12-07 たばこ原料の製造方法及びたばこ原料
EP17893982.3A EP3556227A4 (fr) 2017-01-30 2017-12-07 Procédé de fabrication de matière première de tabac, et matière première de tabac
CN201780085103.4A CN110290713B (zh) 2017-01-30 2017-12-07 烟草原料的制造方法及烟草原料
US16/524,807 US20190350251A1 (en) 2017-01-30 2019-07-29 Method for manufacturing tobacco raw material, and tobacco raw material

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WO2021220790A1 (fr) * 2020-04-28 2021-11-04 日本たばこ産業株式会社 Procédé de fabrication de tabac en feuilles traité et procédé de stockage de tabac en feuilles
WO2022138261A1 (fr) 2020-12-24 2022-06-30 日本たばこ産業株式会社 Composition de tabac, segment contenant du tabac, inhalateur d'arôme de type à chauffage sans combustion, et système d'inhalation d'arôme de type à chauffage sans combustion
WO2022138260A1 (fr) 2020-12-24 2022-06-30 日本たばこ産業株式会社 Composition de tabac, segment contenant du tabac, inhalateur d'arôme de type à chauffage sans combustion, et système d'inhalation d'arôme de type à chauffage sans combustion

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CN110973686B (zh) * 2019-12-13 2022-02-08 红云红河烟草(集团)有限责任公司 一种制丝过程水分精准控制模型的建立方法
CN110973687B (zh) * 2019-12-13 2022-03-08 红云红河烟草(集团)有限责任公司 一种制丝过程水分精准控制方法
CN113234509A (zh) * 2021-04-26 2021-08-10 河南中烟工业有限责任公司 一种烟秸生物质炭复合颗粒及制备方法
CN113331459A (zh) * 2021-07-09 2021-09-03 中国农业科学院烟草研究所(中国烟草总公司青州烟草研究所) 一种烟叶智能烘烤控制方法
KR20240059487A (ko) 2022-10-27 2024-05-07 홍재명 바디스윙 보조기구

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WO2021220790A1 (fr) * 2020-04-28 2021-11-04 日本たばこ産業株式会社 Procédé de fabrication de tabac en feuilles traité et procédé de stockage de tabac en feuilles
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WO2022138261A1 (fr) 2020-12-24 2022-06-30 日本たばこ産業株式会社 Composition de tabac, segment contenant du tabac, inhalateur d'arôme de type à chauffage sans combustion, et système d'inhalation d'arôme de type à chauffage sans combustion
WO2022138262A1 (fr) 2020-12-24 2022-06-30 日本たばこ産業株式会社 Composition de tabac, segment contenant du tabac, inhalateur d'arôme de type à chauffage sans combustion, et système d'inhalation d'arôme de type à chauffage sans combustion
WO2022138260A1 (fr) 2020-12-24 2022-06-30 日本たばこ産業株式会社 Composition de tabac, segment contenant du tabac, inhalateur d'arôme de type à chauffage sans combustion, et système d'inhalation d'arôme de type à chauffage sans combustion

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EP3556227A1 (fr) 2019-10-23
CN110290713B (zh) 2022-02-08
CN110290713A (zh) 2019-09-27
JPWO2018139068A1 (ja) 2019-11-07
US20190350251A1 (en) 2019-11-21
JP6832960B2 (ja) 2021-02-24

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