WO2016126059A1 - Composition antibactérienne et lingette humide comprenant la composition antibactérienne - Google Patents

Composition antibactérienne et lingette humide comprenant la composition antibactérienne Download PDF

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Publication number
WO2016126059A1
WO2016126059A1 PCT/KR2016/001057 KR2016001057W WO2016126059A1 WO 2016126059 A1 WO2016126059 A1 WO 2016126059A1 KR 2016001057 W KR2016001057 W KR 2016001057W WO 2016126059 A1 WO2016126059 A1 WO 2016126059A1
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WIPO (PCT)
Prior art keywords
weight
antimicrobial composition
antibacterial composition
wet tissue
present
Prior art date
Application number
PCT/KR2016/001057
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English (en)
Korean (ko)
Inventor
임호
Original Assignee
임호
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from KR1020160011579A external-priority patent/KR20160096022A/ko
Application filed by 임호 filed Critical 임호
Publication of WO2016126059A1 publication Critical patent/WO2016126059A1/fr

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Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • A01N37/22—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides
    • A01N37/24—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides containing at least one oxygen or sulfur atom being directly attached to the same aromatic ring system
    • A—HUMAN NECESSITIES
    • A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47K—SANITARY EQUIPMENT NOT OTHERWISE PROVIDED FOR; TOILET ACCESSORIES
    • A47K10/00—Body-drying implements; Toilet paper; Holders therefor
    • A47K10/02—Towels
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/185—Acids; Anhydrides, halides or salts thereof, e.g. sulfur acids, imidic, hydrazonic or hydroximic acids
    • A61K31/19—Carboxylic acids, e.g. valproic acid
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings

Definitions

  • the present invention relates to an antimicrobial composition and a wet tissue including the antimicrobial composition, and more specifically, 5 to 20% by weight of P-Anisic acid, 10 to 40% by weight of glycerin (Glycerin), and 0.5 to 6 bases. It relates to an antimicrobial composition comprising a weight percent, 1 to 10 weight percent glycerin monoglyceride ester (Caprylic monoglyceride CMG) and 30 to 50 weight percent water, and a wet tissue including the composition.
  • microorganisms such as bacteria and molds in daily life are not only diverse but also widely distributed in the natural environment, and can be grown and reproduced at any time, increasing damage to human diseases, housing, and clothing industrial products. It is a situation.
  • the wet tissue is prepared by impregnating a predetermined amount of a solution containing purified water, a surfactant, an alcohol, a humectant, a perfume, and the like on a base such as a nonwoven fabric prepared using cotton fibers, synthetic fibers, or the like. Since wet wipes are mostly used to wipe contaminants by direct contact with human skin, they must be excellent in safety as well as the ability to remove foreign substances. In addition, wet tissues should be able to suppress the growth of these microorganisms because they are suitable for the growth of bacteria and fungi when the non-woven fabric is only impregnated with water to grow microorganisms.
  • Chloromethylisothiazolinone (CMIT), Benzalkonium Chloride, 3-Iodine-2-propynylbutylcarbamate (IPBC), Polyhexamethylene guanidine (PHMG), Polyhexamethylene biguanidine (PHMB), Oligo (2- (2-ethoxy) ethoxyethyl guanidine chloride), and PGH (alcohol) are used as antibacterial and antiseptics.
  • CMIT Chloromethylisothiazolinone
  • IPBC 3-Iodine-2-propynylbutylcarbamate
  • PHMG Polyhexamethylene guanidine
  • PHMB Polyhexamethylene biguanidine
  • Oligo (2- (2-ethoxy) ethoxyethyl guanidine chloride
  • PGH alcohol
  • iodine-2-propynylbutyl carbamate is mainly used as an auxiliary ingredient, but the above-mentioned substances have strong skin irritation and Guanidine-based chemical that is a cause of acute lung injury syndrome caused by moisture cleaner, and 3-iodine-2-propynylbutyl carbamate is a social problem such as regulated for infant products by the Ministry of Health, Labor and Welfare. Development of antibacterial and antiseptic substances that can be done is required.
  • Korean Patent No. 152531 discloses 3-butoxy-1,2-propanediol, and the content of 3-butoxy-1,2-propanediol is 0.01 to 10% by weight based on the total weight of the composition. A composition for wet wipes is disclosed. In addition, the patent publication of Korean Patent No.
  • 1189344 includes 0.1 to 2.0 wt% of organic acid and 0.1 to 2.0 wt% of moisturizing raw material, based on the total weight of the skin care composition, wherein the organic acid is cinnamic acid, p- Group consisting of p-anisic acid, levulinic acid, sorbic acid, benzoic acid, acetic acid, citric acid and lactic acid
  • the moisturizing raw material is caprylyl glycol (caprylyl glycol), pentylene glycol (pentylene glycol), propylene glycol (propylene glycol), glycerin (glycerine), glyceryl caprylate (glyceryl caprylate), butyl
  • a self-preserving skin care composition is disclosed, which is at least one selected from the group consisting of butylene glycol, 1,2-hexanediol, and methylpropanediol.
  • hexanediol, Octaneol, Glyceryl Caprylate, P-anisic Acid, etc. are mainly used in wet tissues that use 'preservative-free' materials.
  • (ICID) is not registered as a preservative, but as a raw material with antiseptic properties, registration has recently been promoted as a preservative.
  • the technical problem to be achieved by the present invention is to provide an antimicrobial composition that is non-irritating and harmless to the human body to be suitable for wet tissues or cosmetics, which is a product in direct contact with the body, in place of the existing preservatives having side effects such as skin irritation.
  • another technical problem to be achieved by the present invention is to provide a wet wipe comprising the composition.
  • the present invention provides a P-anisic acid (P-Anisic acid) 5 to 20% by weight, glycerin (Glycerin) 10 to 40% by weight, base 0.5 to 6% by weight, glycerin caprylic acid ester (Caprylic monoglyceride CMG) to provide an antimicrobial composition comprising 1 to 10% by weight and 30 to 50% by weight of water.
  • P-Anisic acid P-anisic acid
  • Glycerin glycerin
  • Caprylic monoglyceride CMG glycerin caprylic acid ester
  • the present invention provides an antimicrobial composition, characterized in that it further comprises 0.05 to 1% by weight of 1,10-dicarboxydecane (1,10-Dicarboxydecane).
  • the present invention provides an antimicrobial composition, characterized in that the base is NaOH or KOH.
  • the present invention provides an antimicrobial composition further comprising 5 to 12% by weight propionic acid.
  • the present invention provides a wet tissue comprising the antimicrobial composition.
  • the present invention replaces the existing preservatives that had side effects such as skin irritation and provides an antimicrobial composition that is non-irritating to the human body and suitable for wet tissues with frequent physical contact, and a wet tissue including the composition.
  • the antimicrobial composition of the present invention is P-anisic acid (P-Anisic acid) 5 to 20% by weight, glycerin (Glycerin) 10 to 40% by weight, base 0.5 to 6% by weight, glycerin caprylic acid ester (Caprylic monoglyceride CMG) 1 To 10% by weight and 30 to 50% by weight of water.
  • 'antibacterial' is used as a meaning including antibacterial and antifungal as well as antiseptic effect.
  • P-anisic acid has been applied to cosmetics in recent years because it is used as a natural-derived preservative raw material is excellent antifungal effect.
  • the P-anisic acid is preferably included in the range of 5 to 20% by weight. This is because when the content of the P-anisic acid is less than 5% by weight based on the total weight of the total antimicrobial composition, the antiseptic performance is lowered, whereas when the P-anisic acid content exceeds 20% by weight, the solubility is lowered to precipitate crystals.
  • Monoglycerine caprylic acid ester (Caprylic monoglyceride CMG) is used as a skin softener and has antibacterial, antiviral, and antifungal effects.
  • Antimicrobial composition of the present invention preferably comprises a glycerin caprylic acid ester (Caprylic monoglyceride CMG) in the range of 1 to 10% by weight. If the content of the glycerin caprylic acid ester is less than 1% by weight based on the total weight of the antimicrobial composition, the antimicrobial activity is reduced, whereas if the content of more than 10% by weight causes problems in mixing with purified water.
  • the antimicrobial composition of the present invention contains 10 to 40% by weight glycerin.
  • polyols such as 1,3-butylene glycol (BG), propylene glycol (PG), dipropylene glycol (DPG), and the like are widely used as moisturizing ingredients and solvents.
  • BG 1,3-butylene glycol
  • PG propylene glycol
  • DPG dipropylene glycol
  • the results of the inventors of the present invention can only reduce the amount of antibacterial and preservatives up to 10% and improve the usability and product stability while only glycerin in the polyol has a skin moisturizing and antibacterial synergistic effect when using a certain amount.
  • the glycerin is preferably included in the range of 10 to 40% by weight. If the content of the glycerin is less than 10% by weight based on the total weight of the antimicrobial composition is less moisturizing, whereas if it exceeds 40% by weight is to prevent the antiseptic composition of the antimicrobial composition.
  • the antimicrobial composition of the present invention comprises a base in the range of 0.5 to 6% by weight.
  • P-anisic acid P-Anisic acid
  • Antimicrobial composition of the present invention may further comprise 0.05 to 1% by weight of 1,10-dicarboxydecane (1,10-Dicarboxydecane).
  • 1,10-dicarboxydecane not only has excellent antibacterial properties, but also has excellent anticorrosive properties, which can prevent corrosion of machinery for manufacturing wet tissues.
  • the content of the 1,10-dicarboxydecane is less than 0.05% by weight based on the total weight of the antimicrobial composition, the antiseptic force is lowered, whereas when the content of 1,10-dicarboxydecane exceeds 1% by weight, 1,10-di
  • the content of carboxydecane is preferably in the above range.
  • the antimicrobial composition of the present invention may further comprise 5 to 12% by weight propionic acid.
  • Propionic acid is known to have an antibacterial antiseptic effect, and its content is preferably in the range of 5 to 12% by weight based on the total antimicrobial composition.
  • the antimicrobial composition of the present invention When the antimicrobial composition of the present invention is applied to wet tissues or cosmetics, the antimicrobial composition may be used by itself or by diluting the antimicrobial composition with a mother liquor.
  • the antimicrobial composition when the antimicrobial composition of the present invention is applied to a wet tissue, since the wet tissue itself has an amount of water to be contained, the antimicrobial composition is added to the purified water in a ratio of 0.5 to 3% by weight and diluted to the wet tissue through the nozzle device. It can be prepared by spraying or impregnating the diluted antimicrobial composition liquid.
  • composition is prepared as described in Table 1 below.
  • the prepared NaOH (98%) was added to purified water and dissolved, and then glycerin (Glycerin) and P-anisic acid and 1,10-Dicarboxydecane and / or propionic acid were added and stirred if necessary.
  • glycerin Glycerin
  • P-anisic acid and 1,10-Dicarboxydecane and / or propionic acid were added and stirred if necessary.
  • glycerine caprylic acid ester Caprylic monoglyceride CMG
  • Preparation Example 1 Preparation Example 2
  • Preparation Example 3 Preparation Example 4
  • Preparation Example 5 P-Anisic acid 100 150 180 200 120 Glycerin 400 350 320 300 300 NaOH (98%) 30 40 50 60 60 1,10-Dicarboxydecane One - - 0.5 0.5 Purified water 429 430 430 429.5 429.5 Glycerine Caprylic Acid Ester (Caprylic monoglyceride CMG) 40 30 20 10 10 Propionic acid - - - - 80
  • Example 1 0.5 g of the antimicrobial composition prepared in Example 1 was used as a mother liquor and 99.5 g of purified water was mixed and stirred to prepare a dilution of the antimicrobial composition.
  • the wet tissue fabric passed through the converting machine through the wet tissue maker, the diluent was sprayed onto the fabric with a spray device, and the wet tissue fabric was cut to the standard to prepare the wet tissue.
  • the antimicrobial activity test evaluation method of the antimicrobial composition of the present invention was cultured in a liquid medium, and then the cultured bacteria were diluted and used for the adjustment test so that the initial bacterial count was (1-9) ⁇ 10 6 CFU / mL.
  • 0.2 mL of the test bacteria was added to 20 mL of the diluted antimicrobial composition prepared in Example 2, and the mixture was left to stand at room temperature for 24 hours, and then the number of viable cells was measured. The number of bacteria was measured to determine the antimicrobial reduction rate for the control bacteria.
  • the initial dilution of all experiments was carried out by neutralizing with D / E Neutralizing broth (DIFCO) .
  • DIFCO D / E Neutralizing broth
  • the number of bacteria on the medium multiplied by the dilution factor is less than 10 ( ⁇ 10).
  • the bacterial counts at all stages were measured using TSA (see Section 2.2), and the viable cell count was determined according to 3.2 [Equation 1] and the antimicrobial reduction rate was determined according to [Equation 2].
  • Test strain Escherichia coli ATCC 25922
  • N Number of viable cells
  • C Number of colonies (mean number of two colonies)
  • D Dilution factor (dilution factor of diluent)
  • Test Items unit Sample classification Result Antibacterial test (Escherichia coli) CFU / mL contrast 4.4 ⁇ 10 5 Antibacterial test (Escherichia coli) CFU / mL 24 hours later ⁇ 10 (99.9% or more) Antibacterial test (Staphylococcus aureus) CFU / mL contrast 2.6 ⁇ 10 5 Antibacterial test (Staphylococcus aureus) CFU / mL 24 hours later ⁇ 10 (99.9% or more)
  • the antimicrobial composition solution of the present invention 0.5 wt% purified water 99.5% by weight dilution solution was carried out according to the antibacterial test according to the conditions presented in the test method Escherichia coli (Escherichia coli) and Staphylococcus aureus (Staphylococcus Aureus showed more than 99.9% antibacterial activity after 24 hours.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Environmental Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Emergency Medicine (AREA)
  • Dentistry (AREA)
  • Plant Pathology (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Cosmetics (AREA)

Abstract

La présente invention concerne une composition antibactérienne et une lingette humide comprenant la composition antibactérienne et, plus spécifiquement, une composition antibactérienne comprenant de 5 à 20 % en massique d'acide P-anisique, 10 à 40 % en masse de glycérine, 0,5 à 6 % en masse de base, 1 à 10 % en masse de monoglycéride d'acide caprylique (CMG) et 30 à 50 % en masse d'eau, et une lingette humide comprenant la composition antibactérienne. La présente invention concerne : une composition antibactérienne qui ne provoque pas d'irritation de la peau et est sans danger pour le corps humain de manière à être appropriée pour une lingette humide qui est fréquemment en contact avec le corps humain en remplaçant des agents de conservation classiques ayant des effets secondaires tels que l'irritation de la peau ; et une lingette humide comprenant la composition antibactérienne.
PCT/KR2016/001057 2015-02-04 2016-02-01 Composition antibactérienne et lingette humide comprenant la composition antibactérienne WO2016126059A1 (fr)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
KR20150017619 2015-02-04
KR10-2015-0017619 2015-02-04
KR10-2016-0011579 2016-01-29
KR1020160011579A KR20160096022A (ko) 2015-02-04 2016-01-29 항균조성물 및 상기 항균조성물을 포함한 물티슈

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109381091A (zh) * 2017-08-04 2019-02-26 天津市艳胜工贸有限公司 擦拭巾的制备方法和擦拭巾
CN114983833A (zh) * 2021-07-31 2022-09-02 铜陵天天纸品科技有限公司 一种湿滑乳霜纸及其制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050245608A1 (en) * 2003-12-12 2005-11-03 Florence Baranger Compositions with anisic acid and glycerides
US20060229291A1 (en) * 2005-04-08 2006-10-12 Dr. Straetmans Gmbh Concentrated, aqueous solutions of p-methoxybenzoic acid for use in cosmetic and dermatologic formulations
KR20130136332A (ko) * 2012-06-04 2013-12-12 지준홍 레불린산과 ｐ-아니식산의 혼합물을 포함하는 방부제 조성물
KR20140062838A (ko) * 2012-11-15 2014-05-26 지준홍 p-아니식산, 레불린산 및 글리세릴 카프릴레이트의 혼합물을 포함하는 방부제 조성물
JP2014533725A (ja) * 2011-11-28 2014-12-15 株式会社アモーレパシフィックＡｍｏｒｅｐａｃｉｆｉｃ Ｃｏｒｐｏｒａｔｉｏｎ 防腐力に優れた皮膚外用剤組成物

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050245608A1 (en) * 2003-12-12 2005-11-03 Florence Baranger Compositions with anisic acid and glycerides
US20060229291A1 (en) * 2005-04-08 2006-10-12 Dr. Straetmans Gmbh Concentrated, aqueous solutions of p-methoxybenzoic acid for use in cosmetic and dermatologic formulations
JP2014533725A (ja) * 2011-11-28 2014-12-15 株式会社アモーレパシフィックＡｍｏｒｅｐａｃｉｆｉｃ Ｃｏｒｐｏｒａｔｉｏｎ 防腐力に優れた皮膚外用剤組成物
KR20130136332A (ko) * 2012-06-04 2013-12-12 지준홍 레불린산과 ｐ-아니식산의 혼합물을 포함하는 방부제 조성물
KR20140062838A (ko) * 2012-11-15 2014-05-26 지준홍 p-아니식산, 레불린산 및 글리세릴 카프릴레이트의 혼합물을 포함하는 방부제 조성물

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109381091A (zh) * 2017-08-04 2019-02-26 天津市艳胜工贸有限公司 擦拭巾的制备方法和擦拭巾
CN114983833A (zh) * 2021-07-31 2022-09-02 铜陵天天纸品科技有限公司 一种湿滑乳霜纸及其制备方法
CN114983833B (zh) * 2021-07-31 2023-12-01 铜陵天天纸品科技有限公司 一种湿滑乳霜纸及其制备方法

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