WO2016008367A1 - High vacuum electric arc pump and air extraction unit thereof - Google Patents

High vacuum electric arc pump and air extraction unit thereof Download PDF

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Publication number
WO2016008367A1
WO2016008367A1 PCT/CN2015/083276 CN2015083276W WO2016008367A1 WO 2016008367 A1 WO2016008367 A1 WO 2016008367A1 CN 2015083276 W CN2015083276 W CN 2015083276W WO 2016008367 A1 WO2016008367 A1 WO 2016008367A1
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Prior art keywords
pump
vacuum
high vacuum
chamber
arc
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PCT/CN2015/083276
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French (fr)
Chinese (zh)
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储继国
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储继国
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Publication of WO2016008367A1 publication Critical patent/WO2016008367A1/en

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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/24Vacuum evaporation
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F04POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
    • F04BPOSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS
    • F04B37/00Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00
    • F04B37/10Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00 for special use
    • F04B37/14Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00 for special use to obtain high vacuum

Definitions

  • the invention belongs to the technical field of vacuum acquisition, and in particular relates to a high vacuum arc pump and an air extraction unit thereof.
  • Patent 201210170072.1 (a pumping system and process)
  • Patent 201310241954.7 vacuum furnace pumping system and its pumping process
  • Patent 201310242244.6 (evaporation coating equipment and its pumping process)
  • Patent 201310241939.2 plasma coating equipment and its pumping process
  • the above four patents propose an arc pump that uses chemical discharge to extract gas by arc discharge (usually using titanium as an adsorbent), as well as its pumping unit, pumping process and typical applications.
  • the arc titanium pump has a large pumping speed (easy to obtain tens of thousands of L / s large pumping speed), low energy consumption (about 1/3 of the conventional diffusion pump), quick start (a few seconds to a few minutes), no oil vapor pollution Significantly improve the quality of vacuum products.
  • the arc titanium pump has the following disadvantages:
  • the object of the present invention is to overcome the above-mentioned deficiencies of the prior art and to provide a high vacuum arc pump which can expand the high vacuum operating range, increase the ultimate vacuum, and use more reliable.
  • a high vacuum arc pump comprising a pump casing and a power source on the pump casing a pump port is provided, and a base is fixed on the openable panel on one side of the pump casing, the base is insulated from the panel, and the base is electrically connected to the negative pole of the power source, the base The inner end is fixedly connected to the cathode target, the positive pole of the power source is electrically connected to the pump casing, and the pump casing is further provided with a metal baffle between the cathode target and the panel, the metal baffle and the metal baffle The surrounding components are insulated.
  • a thermal conductive thin layer having a material characteristic spectrum different from a characteristic spectrum of the cathode target is disposed between the cathode target and the susceptor.
  • the material of the heat conductive thin layer is iron or copper, and the heat conductive thin layer has a thickness of 0.5 to 2 mm.
  • the material of the cathode target is titanium.
  • the cathode target is doped with other materials, and the other material is magnesium, aluminum, zinc, calcium or a mixture of any two of them, and the weight percentage of the other materials in the cathode target is 0.5. ⁇ 80%.
  • the invention also provides a high vacuum arc pump unit, comprising a vacuum chamber, which is respectively connected with a rough pump, a traction molecular pump and a high vacuum arc pump as described above;
  • the vacuum chamber is connected to the rough pump through a first vacuum valve, the vacuum chamber is connected to the traction molecular pump through a second vacuum valve, and the traction molecular pump is connected to the foreline pump through a third vacuum valve.
  • the vacuum chamber is sequentially connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the vacuum chamber is further connected with a gas release valve and a vacuum gauge.
  • the invention also provides a high vacuum arc pump unit, comprising a vacuum chamber, which is respectively connected with a rough pump, a traction molecular pump and a high vacuum arc pump as described above;
  • the vacuum chamber is connected to the rough pump through a first vacuum valve, the vacuum chamber is connected to the traction molecular pump through a second vacuum valve, and the traction molecular pump is connected to the foreline pump through a third vacuum valve.
  • the vacuum chamber is sequentially connected to the high vacuum arc pump via a fourth vacuum valve and a dust shield, and the vacuum chamber is further connected with a gas release valve and a vacuum gauge.
  • the invention also provides a cryogenic high vacuum arc pump unit, comprising a vacuum chamber, which is respectively connected with a cryogenic pump, a rough pump, a traction molecular pump and a high vacuum arc pump as described above;
  • the vacuum chamber is connected to the rough pump through a first vacuum valve, and the vacuum chamber is respectively connected to the cryogenic pump and the traction molecular pump through a second vacuum valve, and the traction molecular pump passes through a third vacuum
  • the valve is connected to the foreline pump, and the vacuum chamber is connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the vacuum chamber is further connected with a vent valve and a vacuum gauge, respectively.
  • the invention also provides a cryogenic arc pump evaporation coating unit, comprising a coating chamber, the coating chamber A rough pump, a traction molecular pump, and a high vacuum arc pump as described above are respectively connected;
  • the coating chamber is connected to the rough pump through a first vacuum valve, and the coating chamber is respectively connected to a cryogenic pump and the traction molecular pump through a second vacuum valve, and the traction molecular pump passes through a third vacuum valve
  • the front stage pump is connected, and the coating chamber is connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the coating chamber is further connected with a gas release valve and a vacuum gauge.
  • the arc pump provided by the invention has a high ultimate vacuum, and the high vacuum operating range is more than 100 times higher than that of the conventional arc pump.
  • the arc pump provided by the invention is reliable in operation, and can issue an early warning signal when the cathode target is exhausted, thereby avoiding a cooling water jacket burn-through accident of the arc pump base.
  • the arc pump provided by the present invention also has a large instantaneous pumping speed and instantaneous pumping flow rate.
  • the high vacuum arc pump unit provided by the invention can replace the large-scale diffusion pump + Roots pump unit with high energy consumption and high oil vapor pollution which is widely used at present, saves 80% of pumping energy consumption, eliminates oil vapor pollution, and improves vacuum. product quality.
  • FIG. 1 is a schematic view of a high vacuum arc pump according to a first embodiment of the present invention.
  • FIG. 2 is a schematic view of a high vacuum arc pump unit according to a second embodiment of the present invention.
  • FIG 3 is a schematic view of a cryogenic high vacuum arc pump unit according to a third embodiment of the present invention.
  • Embodiment 4 is a schematic view of a high vacuum evaporation coating unit provided in Embodiment 4 of the present invention.
  • FIG. 5 is a schematic view of a cryogenic arc pump evaporation coating unit provided in Embodiment 5 of the present invention.
  • Embodiment 1 High Vacuum Arc Pump
  • a high vacuum arc pump 1 includes a pump casing 11 .
  • the upper part of the pump casing 11 is provided with a pump port 12
  • the right side of the pump casing 11 is a panel 13 that can be opened and closed.
  • the base 13 is fixed with a base 14 and the base 14 is insulated from the panel 13.
  • the base 14 is electrically connected to the negative pole of the power source 15.
  • the base 14 is provided with a cooling water jacket 16 and the cooling water jacket 16 is cooled. The water is cooled to the susceptor 14.
  • the inner end of the susceptor 14 is fixedly connected to the cathode target 17, the positive pole of the power source 15 is electrically connected to the pump casing 11, and the pump casing 11 is further provided with a metal between the cathode target 17 and the panel 13.
  • the baffle 18, the metal baffle 18 is preferably stainless steel or aluminum, and the metal baffle 18 is insulated from surrounding components.
  • the metal baffle 18 Since the metal baffle 18 is disposed between the cathode target 17 and the panel 13, the metal baffle 18 can prevent electrons emitted from the cathode target 17 from flowing into the panel 13, so that the temperature of the panel 13 does not rise, and the panel 13 does not need water cooling, The phenomenon of massive desorption of adsorbed gas occurs again.
  • the electron flow from the cathode target 17 flows into the metal baffle 18, but the metal baffle 18 is insulated from the surrounding components, electrons flowing into the metal baffle 18 cannot be separated, and the metal baffle 18 generates a negative voltage, preventing subsequent electrons from continuing to flow.
  • the temperature of the metal baffle 18 does not rise.
  • the cathode target 17 is made of a material capable of chemically reacting with a gas to form a solid phase material (that is, capable of obtaining chemisorption and pumping).
  • the material of the cathode target 17 is preferably titanium, and the cathode target 17 is also doped with high vapor at a high temperature.
  • Other materials which are pressed and also have partial pumping action preferably metal, aluminum, zinc, calcium or a mixture of any two of them, the metal material being present in the cathode target 17 in a weight percentage of from 0.5 to 80%.
  • the cathode target 17 is doped with a high vapor pressure metal material, when the arc discharge is performed, the metal material is mixed with the titanium atom to evaporate at the same time, and a thin layer of metal vapor having a higher pressure (>0.1 Pa) is formed on the surface of the cathode target 17 when When the pressure inside the pump casing 11 is lowered and the arc discharge cannot be maintained, the thin metal vapor layer is used to maintain the arc discharge, thereby greatly expanding the high vacuum operation range of the arc pump 1. Since the vapor pressure of the metal material incorporated at room temperature is less than 10 -9 Pa, the ultimate pressure of the arc pump 1 is not affected, and the measured results show that the present embodiment can be in a high vacuum region of ⁇ 10 -4 Pa.
  • the segment runs stably. Further, since the doped metal material can also remove gases such as O 2 and H 2 O at a high temperature, the cathode target 17 of the present embodiment does not significantly decrease in pumping speed after the metal material is incorporated. In addition, since the price of the incorporated metal material is relatively low, the cost of the cathode target 17 can be reduced, and the running cost of the embodiment can be reduced.
  • a heat conducting thin layer 19 having a characteristic spectrum different from that of the cathode target 17 is further disposed between the cathode target 17 and the susceptor 14.
  • the material of the heat conductive thin layer 19 is preferably iron or copper, and the thermal conductive thin layer The thickness of 19 is preferably 0.5 to 2 mm.
  • the outer wall of the pump casing 11 is provided with a water-cooling passage 110 in addition to the panel 19, and the water-cooling passage 110 is provided with cooling water for cooling the pump casing 11.
  • the arc pump 1 provided in the first embodiment can be used for a high vacuum arc pump unit, a cryogenic high vacuum arc pump unit, a high vacuum device (for example, a high vacuum evaporation coating unit, a brazing furnace, a melting furnace, a sintering furnace, an epitaxial furnace, and a heat treatment). And de-hydrogen furnaces, etc., cryogenic high vacuum equipment (such as cryogenic arc pump evaporation coating unit, brazing furnace, melting furnace, sintering furnace, epitaxial furnace, heat treatment and dehydrogenation furnace, etc.).
  • a high vacuum device for example, a high vacuum evaporation coating unit, a brazing furnace, a melting furnace, a sintering furnace, an epitaxial furnace, and a heat treatment.
  • de-hydrogen furnaces, etc. cryogenic high vacuum equipment (such as cryogenic arc pump evaporation coating unit, brazing furnace, melting furnace, sintering furnace, epitaxial furnace, heat treatment and dehydrogenation
  • Embodiment 2 High vacuum arc pump unit
  • a high vacuum arc pump unit includes a vacuum chamber 21 connected to a rough pump 22, a traction molecular pump 23, and a high as described in the first embodiment.
  • the vacuum chamber 21 is connected to the rough pump 22 through the first vacuum valve 24, the vacuum chamber 21 is connected to the traction molecular pump 23 through the second vacuum valve 25, and the traction molecular pump 23 is passed through the third vacuum valve 26 and the foreline pump 27
  • the vacuum chamber 21 is connected to the high vacuum arc pump 1 via the dust shield 28 and the fourth vacuum valve 29, and the dust shield 28 is preferably an electrostatic dust shield.
  • the vacuum chamber 21 is also connected with a vent valve 210 and a vacuum gauge 211, respectively. .
  • the arc pump 1 is mainly used for extracting the active gas in the fine pumping stage
  • the traction molecular pump 23 is used for extracting the inert gas in the fine pumping stage and the pumping in the medium vacuum stage
  • the rough pump 22 is only used in the rough pumping stage. Pumping, running time only accounts for 1/10 of the total pumping time.
  • Roughing stage 22 gas is pumped by the rough pump, and the pressure of the vacuum chamber 21 is pumped from atmospheric pressure to about 10 2 Pa, and then no longer runs;
  • Fine extraction stage The arc pump 1 + the traction molecular pump 23 + the foreline pump 27 is evacuated, and the pressure of the vacuum chamber 21 is drawn from 0.1 Pa to a high vacuum.
  • the high vacuum arc pump unit provided in the second embodiment can replace the traditional large diffusion pump + Roots pump + rough pump unit (referred to as diffusion pump unit), obtain high vacuum better than 10 -4 Pa, and save energy consumption. More than 80%, reduce operating costs by more than 60%, and can eliminate oil vapor pollution and improve the quality of vacuum products.
  • Embodiment 3 cryogenic high vacuum arc pump unit
  • the third embodiment provides a cryogenic high vacuum arc pump unit, including a vacuum chamber 31.
  • the vacuum chamber 31 is connected with a rough pump 32, a traction molecular pump 33, and the same as described in the first embodiment.
  • the vacuum chamber 31 is connected to the rough pump 32 through the first vacuum valve 34, and the vacuum chamber 31 is connected to the cryogenic pump 36 and the traction molecular pump 33 directly or through the second vacuum valve 35, respectively, and the traction molecular pump 33 passes through the third
  • the vacuum valve 37 is connected to the foreline pump 38, and the vacuum chamber 31 is connected to the high vacuum arc pump 1 through the dust shield 39 and the fourth vacuum valve 310, respectively, and the vacuum chamber 31 is also connected with a deflation valve 311 and a vacuum gauge 312, respectively.
  • cryogenic pump 36 is used for pumping out the medium and high vacuum condensable gas
  • the arc pump 1 is mainly used for extracting the active gas in the fine pumping stage
  • the traction molecular pump 33 is used for extracting the inert gas in the fine pumping stage and
  • the rough pump 32 is only used for pumping in the rough pumping stage, and the running time is only 1/5 of the total pumping time.
  • (1) rough pumping stage pumping by the rough pump 32, pumping the pressure of the vacuum chamber 31 from atmospheric pressure to about 10 2 Pa;
  • Fine pumping stage pumping by arc pump 1 + fore pump 38 + traction molecular pump 33 + cryogenic pump 36, or pumping by arc pump 1 + traction molecular pump 33 + cryogenic pump 36, vacuum chamber
  • the pressure of 31 was drawn from a pressure of about 0.1 Pa to a high vacuum.
  • the fourth vacuum valve 310 connected to the arc pump 1 is turned off 0.5 to 5 minutes earlier, and the arc pump 1 is turned on, and after the accumulation of more active titanium film is completed, the fourth vacuum valve is opened.
  • the 310 starts pumping and obtains a huge instantaneous pumping speed and pumping flow.
  • the cryogenic high vacuum arc pump unit provided in the third embodiment has high pumping efficiency, and the pumping time is about 1/2 of that of the high vacuum arc pump unit described in the second embodiment.
  • Embodiment 4 high vacuum evaporation coating unit
  • a high vacuum evaporation coating unit includes a coating chamber 41 connected to a rough pump 42, a traction molecular pump 43, and a high as described in the first embodiment.
  • the coating chamber 41 is connected to the rough pump 42 through the first vacuum valve 44, the coating chamber 41 is connected to the traction molecular pump 43 through the second vacuum valve 45, and the traction molecular pump 43 is passed through the third vacuum valve 46 and the front.
  • the pumping unit 47 is connected, and the coating chamber 41 is connected to the high vacuum arc pump 1 via the dust shield 48 and the fourth vacuum valve 49 in sequence.
  • the dust shield 48 is preferably an electrostatic dust shield, and the coating chamber 41 is also connected with a vent valve 410 and Vacuum gauge 411.
  • the arc pump 1 is mainly used for extracting the active gas in the fine pumping stage, the traction molecular pump 43 is used for pumping out the inert gas in the fine pumping stage and the pumping in the medium vacuum stage, and the rough pump 42 is only used in the rough pumping stage. Pumping, running time only accounts for 1/10 of the total pumping time.
  • the rough pump 42 is only used for pumping in the rough pumping stage
  • the arc pump 1 is mainly used for pumping in the fine pumping stage
  • the traction molecular pump 43 and the foreline pump 47 are used for pumping in the middle vacuum stage and the fine pumping stage. .
  • the pumping process of the high vacuum evaporation coating unit of the fourth embodiment of the present invention includes the following steps:
  • Preparation stage loading the workpiece into the coating chamber 41, closing the coating chamber 41 and all the vacuum valves, sequentially opening the foreline pump 47, the third vacuum valve 46, and the traction molecular pump 43, and the traction molecular pump 43 is in a standby state;
  • the high vacuum evaporation coating unit provided in the fourth embodiment saves 80% of the energy consumption of the pumping, significantly improves the product quality, and has significant economic benefits.
  • Embodiment 5 cryogenic arc pump evaporation coating unit
  • a cryogenic arc pump evaporation coating unit provided in Embodiment 5 of the present invention includes a coating chamber 51, and the coating chamber 51 is respectively connected with a rough pump 52, a traction molecular pump 53, and the first embodiment.
  • the coating chamber 51 is connected to the rough pump 52 through the first vacuum valve 54, and the coating chamber 51 is connected to the cryogenic pump 56 and the traction molecular pump 53 through the second vacuum valve 55, respectively, and the cryogenic pump 56 is used for pumping.
  • the condensing gas, the traction molecular pump 53 is connected to the foreline pump 58 through the third vacuum valve 57, and the coating chamber 51 is connected to the high vacuum arc pump 1 via the dust shield 59 and the fourth vacuum valve 510, respectively, and the coating chamber 51 is also respectively A vent valve 511 and a vacuum gauge 512 are connected.
  • the rough pump 52 is only used for pumping in the rough pumping stage
  • the arc pump 1 is mainly used for pumping in the fine pumping stage
  • the traction molecular pump 53 and the foreline pump 58 are used for pumping in the middle vacuum stage and the fine pumping stage. .
  • Fine pumping stage pumping by the traction molecular pump 53 + the foreline pump 58 + the cryogenic pump 56 + the arc pump 1 , and pumping the pressure of the coating chamber 51 from 100 to 0.1 Pa to 0.1 to 5 ⁇ 10 -2 Pa.
  • the pumping process of the cryogenic arc pump evaporation coating unit of the fifth embodiment of the present invention includes the following steps:
  • Preparation stage the workpiece to be plated is loaded into the coating chamber 51, the coating chamber 51 and all the vacuum valves are closed, and the foreline pump 58, the third vacuum valve 57, the traction molecular pump 53 and the cryogenic pump 56 are sequentially turned on, and the traction molecules are pulled.
  • the pump 53 and the cryogenic pump 56 are in a standby state;
  • the cooling is performed for about 1 minute, the fourth vacuum valve 510 and the second vacuum valve 55 are closed, the arc pump 1 is turned off, and then the deflation valve 511 is opened to deflate, and the atmosphere is injected into the coating chamber 51 to open the coating chamber 51. , the plated workpiece is taken out, and the coating cycle is completed.
  • the cryogenic arc pump evaporation coating unit provided in the fifth embodiment adopts a cryogenic pump 56 to remove the medium and high vacuum condensable gas, and the arc pump 1 is used to remove the high vacuum active gas, and the pumping efficiency is remarkably improved, and the conventional Compared with the diffusion pump evaporation coating equipment, the energy consumption of pumping is up to 80%, the vacuum coating quality of the product is significantly improved, and the production efficiency is doubled. Moreover, the equipment cost of the same capacity is slightly reduced, and the economic benefit is remarkable.

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Abstract

Disclosed are a high vacuum electric arc pump (1), and a high vacuum electric arc pump unit, a cryogenic high vacuum electric arc pump unit, a high vacuum evaporation coating unit and a cryogenic electric arc pump evaporation coating unit comprising the high vacuum electric arc pump, which belong to the field of vacuum production techniques. A high vapour pressure material is doped into a cathode target of a traditional electric arc pump, which substantially extends the high vacuum operating scope of the electric arc pump, and the high vapour pressure material is magnesium, aluminium, zinc or calcium, or a mixture of at least two thereof, and the high vapour pressure material has a weight percentage of 0.5-80% in the cathode target. A metal baffle plate (18) is provided between a cathode target (17) and an openable and closable panel (13) of the electric arc pump (1), and the metal baffle plate (18) is insulated from surrounding components, which eliminates the temperature rise of the panel (13), notably reduces the desorption of an adsorbed gas in the panel (13), and further improves the ultimate vacuum of the electric arc pump (1). In addition, the electric arc pump (1) is provided with a consumption forewarning measure for the cathode target (17), which effectively avoids the accident of burning through a cooling water jacket of the electric arc pump (1), and improves the reliability of the electric arc pump (1).

Description

高真空电弧泵及其抽气机组High vacuum arc pump and its air pumping unit 技术领域Technical field
本发明属于真空获得技术领域,尤其涉及一种高真空电弧泵及其抽气机组。The invention belongs to the technical field of vacuum acquisition, and in particular relates to a high vacuum arc pump and an air extraction unit thereof.
背景技术Background technique
专利201210170072.1(一种抽气系统及工艺)Patent 201210170072.1 (a pumping system and process)
专利201310241954.7(真空炉抽气系统及其抽气工艺)Patent 201310241954.7 (vacuum furnace pumping system and its pumping process)
专利201310242244.6(蒸发镀膜设备及其抽气工艺)Patent 201310242244.6 (evaporation coating equipment and its pumping process)
专利201310241939.2(等离子体镀膜设备及其抽气工艺)Patent 201310241939.2 (plasma coating equipment and its pumping process)
以上四件专利提出了一种利用弧光放电实现化学吸附抽气的电弧泵(通常采用金属钛作吸附物质),及其抽气机组、抽气工艺和典型应用。该电弧钛泵具有抽速大(容易获得几万L/s大抽速),能耗低(约为传统扩散泵的1/3),启动迅速(几秒~几分钟),无油蒸汽污染,显著提高真空产品质量等优点。然而,该电弧钛泵存在如下缺点:The above four patents propose an arc pump that uses chemical discharge to extract gas by arc discharge (usually using titanium as an adsorbent), as well as its pumping unit, pumping process and typical applications. The arc titanium pump has a large pumping speed (easy to obtain tens of thousands of L / s large pumping speed), low energy consumption (about 1/3 of the conventional diffusion pump), quick start (a few seconds to a few minutes), no oil vapor pollution Significantly improve the quality of vacuum products. However, the arc titanium pump has the following disadvantages:
1.压强≤10-2Pa区段,空间气体分子的密度很低,电子与气体分子发生碰撞、电离几率很小,无法维持弧光放电。1. The pressure ≤10-2Pa section, the density of the space gas molecules is very low, the electrons collide with the gas molecules, the ionization probability is small, and the arc discharge cannot be maintained.
2.电弧钛泵的钛靶发出的部分电子会绕到钛靶后侧,流入固定电弧泵基座的泵壳面板上,泵壳面板上通常安装多个电弧泵基座,因此,难以实现有效冷却,导致产生局部升温,释放出大量解吸气体,降低了电弧钛泵的抽气效率和极限真空。2. Part of the electrons emitted by the titanium target of the arc titanium pump will be wound around the back side of the titanium target and flow into the pump casing panel of the fixed arc pump base. The arc pump base is usually installed on the pump casing panel, so it is difficult to achieve effective Cooling results in localized temperature rise, releasing a large amount of desorbed gas, reducing the pumping efficiency and ultimate vacuum of the arc titanium pump.
3.阴极靶接近耗尽时,若不及时更换新靶,电弧会烧穿电弧泵基座的冷却水套,导致生产事故。3. When the cathode target is nearly exhausted, if the new target is not replaced in time, the arc will burn through the cooling water jacket of the arc pump base, resulting in a production accident.
上述缺点,限制了电弧泵的推广应用。The above shortcomings limit the promotion and application of the arc pump.
发明内容Summary of the invention
本发明的目的在于克服上述现有技术的不足,提供一种能拓展高真空运行范围、提高极限真空、使用更可靠的高真空电弧泵。SUMMARY OF THE INVENTION The object of the present invention is to overcome the above-mentioned deficiencies of the prior art and to provide a high vacuum arc pump which can expand the high vacuum operating range, increase the ultimate vacuum, and use more reliable.
本发明是这样实现的,一种高真空电弧泵,包括泵壳和电源,所述泵壳上 设有泵口,所述泵壳一侧的可开合的面板上固设有基座,所述基座与所述面板绝缘,所述基座与所述电源负极电连接,所述基座内侧端与阴极靶固定连接,所述电源正极与所述泵壳电连接,所述泵壳内还设有位于所述阴极靶和所述面板之间的金属挡板,所述金属挡板与周围部件绝缘。The present invention is achieved by a high vacuum arc pump comprising a pump casing and a power source on the pump casing a pump port is provided, and a base is fixed on the openable panel on one side of the pump casing, the base is insulated from the panel, and the base is electrically connected to the negative pole of the power source, the base The inner end is fixedly connected to the cathode target, the positive pole of the power source is electrically connected to the pump casing, and the pump casing is further provided with a metal baffle between the cathode target and the panel, the metal baffle and the metal baffle The surrounding components are insulated.
进一步地,所述阴极靶与基座之间设有材质特征光谱与所述阴极靶的特征光谱相异的导热薄层。Further, a thermal conductive thin layer having a material characteristic spectrum different from a characteristic spectrum of the cathode target is disposed between the cathode target and the susceptor.
优选地,所述导热薄层的材料为铁或铜,所述导热薄层的厚度为0.5~2mm。Preferably, the material of the heat conductive thin layer is iron or copper, and the heat conductive thin layer has a thickness of 0.5 to 2 mm.
优选地,所述阴极靶的材料为钛。Preferably, the material of the cathode target is titanium.
进一步地,所述阴极靶中掺入有其它材料,所述其它材料为镁、铝、锌、钙或其中任意至少两种的混合,所述其它材料在所述阴极靶中的重量百分比为0.5~80%。Further, the cathode target is doped with other materials, and the other material is magnesium, aluminum, zinc, calcium or a mixture of any two of them, and the weight percentage of the other materials in the cathode target is 0.5. ~80%.
本发明还提供了一种高真空电弧泵机组,包括真空室,所述真空室分别连接有粗抽泵、牵引分子泵以及如前所述的高真空电弧泵;The invention also provides a high vacuum arc pump unit, comprising a vacuum chamber, which is respectively connected with a rough pump, a traction molecular pump and a high vacuum arc pump as described above;
所述真空室通过第一真空阀与所述粗抽泵连接,所述真空室通过第二真空阀与所述牵引分子泵连接,所述牵引分子泵通过第三真空阀与前级泵连接,所述真空室依次经挡尘板、第四真空阀与所述高真空电弧泵连接,所述真空室还分别连接有放气阀和真空规。The vacuum chamber is connected to the rough pump through a first vacuum valve, the vacuum chamber is connected to the traction molecular pump through a second vacuum valve, and the traction molecular pump is connected to the foreline pump through a third vacuum valve. The vacuum chamber is sequentially connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the vacuum chamber is further connected with a gas release valve and a vacuum gauge.
本发明还提供了一种高真空电弧泵机组,包括真空室,所述真空室分别连接有粗抽泵、牵引分子泵以及如前所述的高真空电弧泵;The invention also provides a high vacuum arc pump unit, comprising a vacuum chamber, which is respectively connected with a rough pump, a traction molecular pump and a high vacuum arc pump as described above;
所述真空室通过第一真空阀与所述粗抽泵连接,所述真空室通过第二真空阀与所述牵引分子泵连接,所述牵引分子泵通过第三真空阀与前级泵连接,所述真空室依次经第四真空阀、挡尘板与所述高真空电弧泵连接,所述真空室还分别连接有放气阀和真空规。The vacuum chamber is connected to the rough pump through a first vacuum valve, the vacuum chamber is connected to the traction molecular pump through a second vacuum valve, and the traction molecular pump is connected to the foreline pump through a third vacuum valve. The vacuum chamber is sequentially connected to the high vacuum arc pump via a fourth vacuum valve and a dust shield, and the vacuum chamber is further connected with a gas release valve and a vacuum gauge.
本发明还提供了一种深冷高真空电弧泵机组,包括真空室,所述真空室分别连接有深冷泵、粗抽泵、牵引分子泵以及如前所述的高真空电弧泵;The invention also provides a cryogenic high vacuum arc pump unit, comprising a vacuum chamber, which is respectively connected with a cryogenic pump, a rough pump, a traction molecular pump and a high vacuum arc pump as described above;
所述真空室通过第一真空阀与所述粗抽泵连接,所述真空室直接或通过第二真空阀分别与所述深冷泵和牵引分子泵连接,所述牵引分子泵通过第三真空阀与前级泵连接,所述真空室经挡尘板和第四真空阀与所述高真空电弧泵连接,所述真空室还分别连接有放气阀和真空规。The vacuum chamber is connected to the rough pump through a first vacuum valve, and the vacuum chamber is respectively connected to the cryogenic pump and the traction molecular pump through a second vacuum valve, and the traction molecular pump passes through a third vacuum The valve is connected to the foreline pump, and the vacuum chamber is connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the vacuum chamber is further connected with a vent valve and a vacuum gauge, respectively.
本发明还提供了一种深冷电弧泵蒸发镀膜机组,包括镀膜室,所述镀膜室 分别连接有粗抽泵、牵引分子泵以及如前所述的高真空电弧泵;The invention also provides a cryogenic arc pump evaporation coating unit, comprising a coating chamber, the coating chamber A rough pump, a traction molecular pump, and a high vacuum arc pump as described above are respectively connected;
所述镀膜室通过第一真空阀与所述粗抽泵连接,所述镀膜室通过第二真空阀分别与深冷泵和所述牵引分子泵连接,所述牵引分子泵通过第三真空阀与前级泵连接,所述镀膜室依次经挡尘板、第四真空阀与所述高真空电弧泵连接,所述镀膜室还分别连接有放气阀和真空规。The coating chamber is connected to the rough pump through a first vacuum valve, and the coating chamber is respectively connected to a cryogenic pump and the traction molecular pump through a second vacuum valve, and the traction molecular pump passes through a third vacuum valve The front stage pump is connected, and the coating chamber is connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the coating chamber is further connected with a gas release valve and a vacuum gauge.
本发明的优点如下:The advantages of the invention are as follows:
(1)本发明提供的电弧泵极限真空高,高真空运行范围比传统电弧泵提高100倍以上。(1) The arc pump provided by the invention has a high ultimate vacuum, and the high vacuum operating range is more than 100 times higher than that of the conventional arc pump.
(2)本发明提供的电弧泵运行可靠,能在阴极靶耗尽时,发出预警信号,避免电弧泵基座发生冷却水套烧穿事故。(2) The arc pump provided by the invention is reliable in operation, and can issue an early warning signal when the cathode target is exhausted, thereby avoiding a cooling water jacket burn-through accident of the arc pump base.
(3)本发明提供的电弧泵还具有巨大的瞬时抽速和瞬时抽气流量。(3) The arc pump provided by the present invention also has a large instantaneous pumping speed and instantaneous pumping flow rate.
(4)本发明提供的高真空电弧泵机组可取代目前广泛使用的高能耗、高油蒸汽污染的大型扩散泵+罗茨泵机组,节省抽气能耗80%,消除油蒸汽污染,提高真空产品质量。(4) The high vacuum arc pump unit provided by the invention can replace the large-scale diffusion pump + Roots pump unit with high energy consumption and high oil vapor pollution which is widely used at present, saves 80% of pumping energy consumption, eliminates oil vapor pollution, and improves vacuum. product quality.
附图说明DRAWINGS
为了更清楚地说明本发明的技术方案,下面将对实施例中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the technical solutions of the present invention, the drawings used in the embodiments will be briefly described below. It is obvious that the drawings in the following description are only some embodiments of the present invention, which are common in the art. For the skilled person, other drawings can be obtained from these drawings without any creative work.
图1是本发明实施例一提供的高真空电弧泵的示意图。1 is a schematic view of a high vacuum arc pump according to a first embodiment of the present invention.
图2是本发明实施例二提供的高真空电弧泵机组的示意图。2 is a schematic view of a high vacuum arc pump unit according to a second embodiment of the present invention.
图3是本发明实施例三提供的深冷高真空电弧泵机组的示意图。3 is a schematic view of a cryogenic high vacuum arc pump unit according to a third embodiment of the present invention.
图4是本发明实施例四提供的高真空蒸发镀膜机组的示意图。4 is a schematic view of a high vacuum evaporation coating unit provided in Embodiment 4 of the present invention.
图5是本发明实施例五提供的深冷电弧泵蒸发镀膜机组的示意图。5 is a schematic view of a cryogenic arc pump evaporation coating unit provided in Embodiment 5 of the present invention.
具体实施方式detailed description
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述。The technical solutions in the embodiments of the present invention will be clearly and completely described in the following with reference to the accompanying drawings.
实施例一高真空电弧泵 Embodiment 1 High Vacuum Arc Pump
如图1所示,本发明实施例一提供的一种高真空电弧泵1,包括泵壳11,泵壳11上部开设有泵口12,泵壳11的右侧为可开合的面板13,面板13上固设有基座14,基座14与面板13之间绝缘,基座14与电源15的负极电连接,基座14上开设有冷却水套16,冷却水套16内通有冷却水实现对基座14的冷却,基座14的内侧端与阴极靶17固定连接,电源15正极与泵壳11电连接,泵壳11内还设有位于阴极靶17和面板13之间的金属挡板18,金属挡板18优选不锈钢或铝,金属挡板18与周围部件绝缘。As shown in FIG. 1 , a high vacuum arc pump 1 according to a first embodiment of the present invention includes a pump casing 11 . The upper part of the pump casing 11 is provided with a pump port 12 , and the right side of the pump casing 11 is a panel 13 that can be opened and closed. The base 13 is fixed with a base 14 and the base 14 is insulated from the panel 13. The base 14 is electrically connected to the negative pole of the power source 15. The base 14 is provided with a cooling water jacket 16 and the cooling water jacket 16 is cooled. The water is cooled to the susceptor 14. The inner end of the susceptor 14 is fixedly connected to the cathode target 17, the positive pole of the power source 15 is electrically connected to the pump casing 11, and the pump casing 11 is further provided with a metal between the cathode target 17 and the panel 13. The baffle 18, the metal baffle 18 is preferably stainless steel or aluminum, and the metal baffle 18 is insulated from surrounding components.
由于阴极靶17和面板13之间设有金属挡板18,金属挡板18可以阻止阴极靶17发出的电子流入面板13,因此,面板13的温度不会升高,面板13不需要水冷,不再发生吸附气体大量解吸的现象。阴极靶17发出的电子流会流入金属挡板18,但金属挡板18与周围部件绝缘,流入金属挡板18的电子无法离开,金属挡板18会产生负电压,阻止后续电子继续流入,因此,金属挡板18的温度也不会升高。Since the metal baffle 18 is disposed between the cathode target 17 and the panel 13, the metal baffle 18 can prevent electrons emitted from the cathode target 17 from flowing into the panel 13, so that the temperature of the panel 13 does not rise, and the panel 13 does not need water cooling, The phenomenon of massive desorption of adsorbed gas occurs again. The electron flow from the cathode target 17 flows into the metal baffle 18, but the metal baffle 18 is insulated from the surrounding components, electrons flowing into the metal baffle 18 cannot be separated, and the metal baffle 18 generates a negative voltage, preventing subsequent electrons from continuing to flow. The temperature of the metal baffle 18 does not rise.
所述阴极靶17采用能与气体产生化学反应、生成固相物质(即能获得化学吸附抽气)的材料,阴极靶17的材料优选钛,阴极靶17还掺入在高温下具有较高蒸汽压并且也具有部分抽气作用的其它材料,该金属材料优选镁、铝、鋅、钙或其中任意至少两种的混合,该金属材料在阴极靶17中的重量百分比为0.5~80%。The cathode target 17 is made of a material capable of chemically reacting with a gas to form a solid phase material (that is, capable of obtaining chemisorption and pumping). The material of the cathode target 17 is preferably titanium, and the cathode target 17 is also doped with high vapor at a high temperature. Other materials which are pressed and also have partial pumping action, preferably metal, aluminum, zinc, calcium or a mixture of any two of them, the metal material being present in the cathode target 17 in a weight percentage of from 0.5 to 80%.
由于阴极靶17中掺入高蒸汽压金属材料,弧光放电时,掺入金属材料与钛原子同时蒸散出来,在阴极靶17的表面形成较高压强(>0.1Pa)的金属蒸汽薄层,当泵壳11内压强下降,无法维持弧光放电时,利用该金属蒸汽薄层,维持弧光放电继续进行,从而大幅拓展电弧泵1的高真空运行范围。由于所述掺入金属材料在室温下的蒸汽压均小于10-9Pa,因此,不会影响电弧泵1的极限压强,实测结果表明,本实施例能在≤10-4Pa的高真空区段稳定运行。另外,由于所述掺入金属材料在高温下也能抽除O2、H2O等气体,因此,本实施例的阴极靶17掺入上述金属材料后,抽速未有明显下降。另外,由于所述掺入金属材料的价格比较低廉,还能降低阴极靶17的成本,降低本实施例的运行费用。Since the cathode target 17 is doped with a high vapor pressure metal material, when the arc discharge is performed, the metal material is mixed with the titanium atom to evaporate at the same time, and a thin layer of metal vapor having a higher pressure (>0.1 Pa) is formed on the surface of the cathode target 17 when When the pressure inside the pump casing 11 is lowered and the arc discharge cannot be maintained, the thin metal vapor layer is used to maintain the arc discharge, thereby greatly expanding the high vacuum operation range of the arc pump 1. Since the vapor pressure of the metal material incorporated at room temperature is less than 10 -9 Pa, the ultimate pressure of the arc pump 1 is not affected, and the measured results show that the present embodiment can be in a high vacuum region of ≤10 -4 Pa. The segment runs stably. Further, since the doped metal material can also remove gases such as O 2 and H 2 O at a high temperature, the cathode target 17 of the present embodiment does not significantly decrease in pumping speed after the metal material is incorporated. In addition, since the price of the incorporated metal material is relatively low, the cost of the cathode target 17 can be reduced, and the running cost of the embodiment can be reduced.
进一步地,所述阴极靶17和基座14之间还设有一材质的特征光谱与阴极靶17的特征光谱相异的导热薄层19,导热薄层19的材料优选铁或铜,导热薄层19的厚度优选0.5~2mm。当电弧泵1的阴极靶17耗尽时,导热薄层19的原 子开始蒸散,弧光放电的色泽会发生相应变化,警示阴极靶17耗尽,需及时更换新靶,从而,有效避免冷却水套16烧穿事故。Further, between the cathode target 17 and the susceptor 14, a heat conducting thin layer 19 having a characteristic spectrum different from that of the cathode target 17 is further disposed. The material of the heat conductive thin layer 19 is preferably iron or copper, and the thermal conductive thin layer The thickness of 19 is preferably 0.5 to 2 mm. When the cathode target 17 of the arc pump 1 is exhausted, the original of the heat conductive thin layer 19 When the child begins to evade, the color of the arc discharge will change accordingly, warning that the cathode target 17 is exhausted, and it is necessary to replace the new target in time, thereby effectively avoiding the burning of the cooling water jacket 16 .
进一步地,所述泵壳11的外壁除面板19之外,还设有水冷通道110,水冷通道110内通有冷却水,用于对泵壳11进行冷却。Further, the outer wall of the pump casing 11 is provided with a water-cooling passage 110 in addition to the panel 19, and the water-cooling passage 110 is provided with cooling water for cooling the pump casing 11.
本实施例一提供的电弧泵1可用于高真空电弧泵机组、深冷高真空电弧泵机组、高真空设备(例如高真空蒸发镀膜机组、钎焊炉、熔炼炉、烧结炉、外延炉、热处理和脱羟炉等)、深冷高真空设备(例如深冷电弧泵蒸发镀膜机组、钎焊炉、熔炼炉、烧结炉、外延炉、热处理和脱羟炉等)。The arc pump 1 provided in the first embodiment can be used for a high vacuum arc pump unit, a cryogenic high vacuum arc pump unit, a high vacuum device (for example, a high vacuum evaporation coating unit, a brazing furnace, a melting furnace, a sintering furnace, an epitaxial furnace, and a heat treatment). And de-hydrogen furnaces, etc., cryogenic high vacuum equipment (such as cryogenic arc pump evaporation coating unit, brazing furnace, melting furnace, sintering furnace, epitaxial furnace, heat treatment and dehydrogenation furnace, etc.).
实施例二高真空电弧泵机组Embodiment 2 High vacuum arc pump unit
如图2所示,本发明实施例二提供的一种高真空电弧泵机组,包括真空室21,真空室21分别连接有粗抽泵22、牵引分子泵23以及如实施例一所述的高真空电弧泵1;As shown in FIG. 2, a high vacuum arc pump unit according to a second embodiment of the present invention includes a vacuum chamber 21 connected to a rough pump 22, a traction molecular pump 23, and a high as described in the first embodiment. Vacuum arc pump 1;
具体地,真空室21通过第一真空阀24与粗抽泵22连接,真空室21通过第二真空阀25与牵引分子泵23连接,牵引分子泵23通过第三真空阀26与前级泵27连接,真空室21依次经挡尘板28、第四真空阀29与高真空电弧泵1连接,挡尘板28优选静电挡尘板,真空室21还分别连接有放气阀210和真空规211。Specifically, the vacuum chamber 21 is connected to the rough pump 22 through the first vacuum valve 24, the vacuum chamber 21 is connected to the traction molecular pump 23 through the second vacuum valve 25, and the traction molecular pump 23 is passed through the third vacuum valve 26 and the foreline pump 27 The vacuum chamber 21 is connected to the high vacuum arc pump 1 via the dust shield 28 and the fourth vacuum valve 29, and the dust shield 28 is preferably an electrostatic dust shield. The vacuum chamber 21 is also connected with a vent valve 210 and a vacuum gauge 211, respectively. .
其中,电弧泵1主要用于抽除精抽阶段的活性气体,牵引分子泵23用于抽除精抽阶段的惰性气体和中真空阶段的抽气,粗抽泵22仅用于粗抽阶段的抽气,运行时间仅占总抽气时间的1/10。Wherein, the arc pump 1 is mainly used for extracting the active gas in the fine pumping stage, the traction molecular pump 23 is used for extracting the inert gas in the fine pumping stage and the pumping in the medium vacuum stage, and the rough pump 22 is only used in the rough pumping stage. Pumping, running time only accounts for 1/10 of the total pumping time.
本实施例二的高真空电弧泵机组的抽气工艺,包括如下步骤:The pumping process of the high vacuum arc pump unit of the second embodiment includes the following steps:
(1)粗抽阶段:由粗抽泵抽22气,将真空室21压强从大气压抽至约102Pa,之后不再运行;(1) Roughing stage: 22 gas is pumped by the rough pump, and the pressure of the vacuum chamber 21 is pumped from atmospheric pressure to about 10 2 Pa, and then no longer runs;
(2)中真空阶段:由牵引分子泵23+前级泵27抽气,将真空室21压强由102Pa抽至约0.1Pa;(2) medium vacuum stage: pumping by the traction molecular pump 23 + the foreline pump 27, the pressure of the vacuum chamber 21 is pumped from 10 2 Pa to about 0.1 Pa;
(3)精抽阶段:由电弧泵1+牵引分子泵23+前级泵27抽气,将真空室21压强由0.1Pa抽至高真空。(3) Fine extraction stage: The arc pump 1 + the traction molecular pump 23 + the foreline pump 27 is evacuated, and the pressure of the vacuum chamber 21 is drawn from 0.1 Pa to a high vacuum.
本实施例二提供的高真空电弧泵机组,可取代传统大型扩散泵+罗茨泵+粗抽泵机组(简称扩散泵机组),获得优于10-4Pa的高真空,节省抽气能耗80%以上,降低运行成本60%以上,并能消除油蒸汽污染,提高真空产品质量。 The high vacuum arc pump unit provided in the second embodiment can replace the traditional large diffusion pump + Roots pump + rough pump unit (referred to as diffusion pump unit), obtain high vacuum better than 10 -4 Pa, and save energy consumption. More than 80%, reduce operating costs by more than 60%, and can eliminate oil vapor pollution and improve the quality of vacuum products.
实施例三深冷高真空电弧泵机组Embodiment 3 cryogenic high vacuum arc pump unit
如图3所示,本实施例三提供了一种深冷高真空电弧泵机组,包括真空室31,真空室31分别连接有粗抽泵32、牵引分子泵33以及如实施例一所述的高真空电弧泵1;As shown in FIG. 3, the third embodiment provides a cryogenic high vacuum arc pump unit, including a vacuum chamber 31. The vacuum chamber 31 is connected with a rough pump 32, a traction molecular pump 33, and the same as described in the first embodiment. High vacuum arc pump 1;
具体地,真空室31通过第一真空阀34与粗抽泵32连接,真空室31直接或通过第二真空阀35分别与深冷泵36和牵引分子泵33连接,牵引分子泵33通过第三真空阀37与前级泵38连接,真空室31分别通过挡尘板39和第四真空阀310与高真空电弧泵1连接,真空室31还分别连接有放气阀311和真空规312。Specifically, the vacuum chamber 31 is connected to the rough pump 32 through the first vacuum valve 34, and the vacuum chamber 31 is connected to the cryogenic pump 36 and the traction molecular pump 33 directly or through the second vacuum valve 35, respectively, and the traction molecular pump 33 passes through the third The vacuum valve 37 is connected to the foreline pump 38, and the vacuum chamber 31 is connected to the high vacuum arc pump 1 through the dust shield 39 and the fourth vacuum valve 310, respectively, and the vacuum chamber 31 is also connected with a deflation valve 311 and a vacuum gauge 312, respectively.
其中,深冷泵36用于抽除中、高真空的可凝性气体,电弧泵1主要用于抽除精抽阶段的活性气体,牵引分子泵33用于抽除精抽阶段的惰性气体和中真空阶段的抽气,粗抽泵32仅用于粗抽阶段的抽气,运行时间仅占总抽气时间的1/5。Wherein, the cryogenic pump 36 is used for pumping out the medium and high vacuum condensable gas, the arc pump 1 is mainly used for extracting the active gas in the fine pumping stage, and the traction molecular pump 33 is used for extracting the inert gas in the fine pumping stage and In the middle vacuum stage, the rough pump 32 is only used for pumping in the rough pumping stage, and the running time is only 1/5 of the total pumping time.
本发明实施例三的深冷电弧泵机组的抽气工艺,包括如下步骤:The pumping process of the cryogenic arc pump unit of the third embodiment of the present invention comprises the following steps:
(1)粗抽阶段:由粗抽泵32抽气,将真空室31压强从大气压抽至约102Pa;(1) rough pumping stage: pumping by the rough pump 32, pumping the pressure of the vacuum chamber 31 from atmospheric pressure to about 10 2 Pa;
(2)中真空阶段:由牵引分子泵33+前级泵38+深冷泵36抽气,或者由牵引分子泵33+深冷泵36抽气,将真空室31压强由约102Pa抽至约0.1Pa;(2) Medium vacuum stage: pumping by the traction molecular pump 33+ fore pump 38+ cryogenic pump 36, or pumping by the traction molecular pump 33+ cryogenic pump 36, pumping the pressure of the vacuum chamber 31 from about 10 2 Pa Up to about 0.1 Pa;
(3)精抽阶段:由电弧泵1+前级泵38+牵引分子泵33+深冷泵36抽气,或者由电弧泵1+牵引分子泵33+深冷泵36抽气,将真空室31压强由约0.1Pa抽至高真空。(3) Fine pumping stage: pumping by arc pump 1 + fore pump 38 + traction molecular pump 33 + cryogenic pump 36, or pumping by arc pump 1 + traction molecular pump 33 + cryogenic pump 36, vacuum chamber The pressure of 31 was drawn from a pressure of about 0.1 Pa to a high vacuum.
进一步地,在电弧泵1运行前,提前0.5~5min关闭与电弧泵1连接的第四真空阀310,并开启电弧泵1,等到积聚了较多的活性钛膜后,再打开第四真空阀310开始抽气,获得巨大的瞬时抽速和抽气流量。Further, before the arc pump 1 is operated, the fourth vacuum valve 310 connected to the arc pump 1 is turned off 0.5 to 5 minutes earlier, and the arc pump 1 is turned on, and after the accumulation of more active titanium film is completed, the fourth vacuum valve is opened. The 310 starts pumping and obtains a huge instantaneous pumping speed and pumping flow.
本实施例三提供的深冷高真空电弧泵机组,抽气效率很高,抽气时间约为实施例二所述的高真空电弧泵机组的1/2。The cryogenic high vacuum arc pump unit provided in the third embodiment has high pumping efficiency, and the pumping time is about 1/2 of that of the high vacuum arc pump unit described in the second embodiment.
实施例四高真空蒸发镀膜机组Embodiment 4 high vacuum evaporation coating unit
如图4所示,本发明实施例四提供的一种高真空蒸发镀膜机组,包括镀膜室41,镀膜室41分别连接有粗抽泵42、牵引分子泵43以及如实施例一所述的高真空电弧泵1;As shown in FIG. 4, a high vacuum evaporation coating unit according to a fourth embodiment of the present invention includes a coating chamber 41 connected to a rough pump 42, a traction molecular pump 43, and a high as described in the first embodiment. Vacuum arc pump 1;
具体地,镀膜室41通过第一真空阀44与粗抽泵42连接,镀膜室41通过第二真空阀45与牵引分子泵43连接,牵引分子泵43通过第三真空阀46与前 级泵47连接,镀膜室41依次经挡尘板48、第四真空阀49与高真空电弧泵1连接,挡尘板48优选静电挡尘板,镀膜室41还分别连接有放气阀410和真空规411。Specifically, the coating chamber 41 is connected to the rough pump 42 through the first vacuum valve 44, the coating chamber 41 is connected to the traction molecular pump 43 through the second vacuum valve 45, and the traction molecular pump 43 is passed through the third vacuum valve 46 and the front. The pumping unit 47 is connected, and the coating chamber 41 is connected to the high vacuum arc pump 1 via the dust shield 48 and the fourth vacuum valve 49 in sequence. The dust shield 48 is preferably an electrostatic dust shield, and the coating chamber 41 is also connected with a vent valve 410 and Vacuum gauge 411.
其中,电弧泵1主要用于抽除精抽阶段的活性气体,牵引分子泵43用于抽除精抽阶段的惰性气体和中真空阶段的抽气,粗抽泵42仅用于粗抽阶段的抽气,运行时间仅占总抽气时间的1/10。The arc pump 1 is mainly used for extracting the active gas in the fine pumping stage, the traction molecular pump 43 is used for pumping out the inert gas in the fine pumping stage and the pumping in the medium vacuum stage, and the rough pump 42 is only used in the rough pumping stage. Pumping, running time only accounts for 1/10 of the total pumping time.
其中,粗抽泵42仅用于粗抽阶段的抽气,电弧泵1主要用于精抽阶段的抽气,牵引分子泵43和前级泵47用于中真空阶段以及精抽阶段的抽气。Among them, the rough pump 42 is only used for pumping in the rough pumping stage, the arc pump 1 is mainly used for pumping in the fine pumping stage, and the traction molecular pump 43 and the foreline pump 47 are used for pumping in the middle vacuum stage and the fine pumping stage. .
具体地,本发明实施例四的高真空蒸发镀膜机组的抽气工艺包括如下步骤:Specifically, the pumping process of the high vacuum evaporation coating unit of the fourth embodiment of the present invention includes the following steps:
(1)准备阶段:向镀膜室41内装入工件,关闭镀膜室41和所有真空阀,依次开启前级泵47、第三真空阀46和牵引分子泵43,牵引分子泵43处于待机状态;(1) Preparation stage: loading the workpiece into the coating chamber 41, closing the coating chamber 41 and all the vacuum valves, sequentially opening the foreline pump 47, the third vacuum valve 46, and the traction molecular pump 43, and the traction molecular pump 43 is in a standby state;
(2)启动粗抽泵42,打开第一真空阀44,镀膜室41由粗抽泵42抽气;(2) starting the rough pump 42, opening the first vacuum valve 44, and the coating chamber 41 is pumped by the rough pump 42;
(3)当镀膜室41的压强降至120Pa,打开第四真空阀49,粗抽泵42同时对电弧泵1抽气;(3) When the pressure of the coating chamber 41 is reduced to 120 Pa, the fourth vacuum valve 49 is opened, and the rough pump 42 simultaneously pumps the arc pump 1;
(4)当镀膜室41压强降至100Pa时,依次关闭第一真空阀44、粗抽泵42,打开第二真空阀45,镀膜室41由牵引分子泵43抽气;(4) When the pressure of the coating chamber 41 is reduced to 100 Pa, the first vacuum valve 44, the rough pump 42 are sequentially closed, the second vacuum valve 45 is opened, and the coating chamber 41 is evacuated by the traction molecular pump 43;
(5)当镀膜室41压强降至0.15Pa时,关闭第四真空阀49,开启电弧泵1;(5) when the pressure of the coating chamber 41 is reduced to 0.15 Pa, the fourth vacuum valve 49 is closed, and the arc pump 1 is turned on;
(6)当镀膜室41压强降至0.1Pa时,打开第四真空阀49,镀膜室41由电弧泵1+牵引分子泵43抽气;(6) When the pressure of the coating chamber 41 is reduced to 0.1 Pa, the fourth vacuum valve 49 is opened, and the coating chamber 41 is evacuated by the arc pump 1 + the traction molecular pump 43;
(7)当镀膜室41压强降至镀膜所需的真空度(例如10-3Pa)时,开始镀膜常规运行操作;(7) When the pressure of the coating chamber 41 is reduced to the degree of vacuum required for the coating (for example, 10 -3 Pa), the normal operation of the coating is started;
(8)当镀膜常规运行操作结束,先后关闭第四真空阀49和第二真空阀45,关闭电弧泵1,然后打开放气阀410放气,向镀膜室41注入大气,打开镀膜室41,取出工件,完成镀膜运行周期。(8) When the normal operation of the coating is finished, the fourth vacuum valve 49 and the second vacuum valve 45 are closed, the arc pump 1 is turned off, then the deflation valve 410 is opened to deflate, the atmosphere is injected into the coating chamber 41, and the coating chamber 41 is opened. The workpiece is taken out to complete the coating operation cycle.
本实施例四提供的高真空蒸发镀膜机组,与传统扩散泵机组的真空镀膜设备相比,节省抽气能耗80%,显著提高产品质量,经济效益显著。Compared with the vacuum coating equipment of the conventional diffusion pump unit, the high vacuum evaporation coating unit provided in the fourth embodiment saves 80% of the energy consumption of the pumping, significantly improves the product quality, and has significant economic benefits.
实施例五深冷电弧泵蒸发镀膜机组Embodiment 5 cryogenic arc pump evaporation coating unit
如图5所示,本发明实施例五提供的一种深冷电弧泵蒸发镀膜机组,包括镀膜室51,镀膜室51分别连接有粗抽泵52、牵引分子泵53以及如实施例一所 述的高真空电弧泵1;As shown in FIG. 5, a cryogenic arc pump evaporation coating unit provided in Embodiment 5 of the present invention includes a coating chamber 51, and the coating chamber 51 is respectively connected with a rough pump 52, a traction molecular pump 53, and the first embodiment. High vacuum arc pump 1;
具体地,镀膜室51通过第一真空阀54与粗抽泵52连接,镀膜室51通过第二真空阀55分别与深冷泵56和牵引分子泵53连接,深冷泵56用于抽除可凝性气体,牵引分子泵53通过第三真空阀57与前级泵58连接,镀膜室51分别依次经挡尘板59、第四真空阀510与高真空电弧泵1连接,镀膜室51还分别连接有放气阀511和真空规512。Specifically, the coating chamber 51 is connected to the rough pump 52 through the first vacuum valve 54, and the coating chamber 51 is connected to the cryogenic pump 56 and the traction molecular pump 53 through the second vacuum valve 55, respectively, and the cryogenic pump 56 is used for pumping. The condensing gas, the traction molecular pump 53 is connected to the foreline pump 58 through the third vacuum valve 57, and the coating chamber 51 is connected to the high vacuum arc pump 1 via the dust shield 59 and the fourth vacuum valve 510, respectively, and the coating chamber 51 is also respectively A vent valve 511 and a vacuum gauge 512 are connected.
其中,粗抽泵52仅用于粗抽阶段的抽气,电弧泵1主要用于精抽阶段的抽气,牵引分子泵53和前级泵58用于中真空阶段以及精抽阶段的抽气。Among them, the rough pump 52 is only used for pumping in the rough pumping stage, the arc pump 1 is mainly used for pumping in the fine pumping stage, and the traction molecular pump 53 and the foreline pump 58 are used for pumping in the middle vacuum stage and the fine pumping stage. .
本发明实施例五的深冷电弧泵蒸发镀膜机组的抽气工艺,包括如下步骤:The pumping process of the cryogenic arc pump evaporation coating unit of the fifth embodiment of the present invention comprises the following steps:
(1)粗抽阶段:由粗抽泵52抽气,将镀膜室51压强从大气压抽至105~100Pa;(1) rough pumping stage: pumping by the rough pump 52, pumping chamber 51 pressure from atmospheric pressure to 10 5 ~ 100Pa;
(2)中真空阶段:由牵引分子泵53+前级泵58+深冷泵56抽气,将镀膜室51压强由105~100Pa抽至100~0.1Pa;(2) Medium vacuum stage: pumping by the traction molecular pump 53 + the foreline pump 58 + the cryogenic pump 56, pumping the pressure of the coating chamber 51 from 10 5 to 100 Pa to 100 to 0.1 Pa;
(3)精抽阶段:由牵引分子泵53+前级泵58+深冷泵56+电弧泵1抽气,将镀膜室51压强由100~0.1Pa抽至0.1~5×10-2Pa。(3) Fine pumping stage: pumping by the traction molecular pump 53 + the foreline pump 58 + the cryogenic pump 56 + the arc pump 1 , and pumping the pressure of the coating chamber 51 from 100 to 0.1 Pa to 0.1 to 5 × 10 -2 Pa.
具体地,本发明实施例五的深冷电弧泵蒸发镀膜机组的抽气工艺包括如下步骤:Specifically, the pumping process of the cryogenic arc pump evaporation coating unit of the fifth embodiment of the present invention includes the following steps:
(1)准备阶段:向镀膜室51内装入待镀工件,关闭镀膜室51和所有真空阀,依次开启前级泵58、第三真空阀57和牵引分子泵53和深冷泵56,牵引分子泵53和深冷泵56处于待机状态;(1) Preparation stage: the workpiece to be plated is loaded into the coating chamber 51, the coating chamber 51 and all the vacuum valves are closed, and the foreline pump 58, the third vacuum valve 57, the traction molecular pump 53 and the cryogenic pump 56 are sequentially turned on, and the traction molecules are pulled. The pump 53 and the cryogenic pump 56 are in a standby state;
(2)启动粗抽泵52,打开第一真空阀54,镀膜室51由粗抽泵52抽气;(2) starting the rough pump 52, opening the first vacuum valve 54, and the coating chamber 51 is pumped by the rough pump 52;
(3)当镀膜室51的压强降至1000Pa,打开第四真空阀510,粗抽泵52同时对电弧泵1抽气;(3) When the pressure of the coating chamber 51 is lowered to 1000 Pa, the fourth vacuum valve 510 is opened, and the rough pump 52 simultaneously pumps the arc pump 1;
(4)当镀膜室51压强降至100Pa时,依次关闭第一真空阀54、粗抽泵52,打开第二真空阀55,镀膜室51由牵引分子泵53+深冷泵56抽气;(4) When the pressure of the coating chamber 51 is reduced to 100 Pa, the first vacuum valve 54 and the rough pump 52 are sequentially closed, the second vacuum valve 55 is opened, and the coating chamber 51 is evacuated by the traction molecular pump 53 + the cryogenic pump 56;
(5)当镀膜室51压强降至0.15Pa时,关闭第四真空阀510,开启电弧泵1;(5) when the pressure of the coating chamber 51 is reduced to 0.15 Pa, the fourth vacuum valve 510 is closed, and the arc pump 1 is turned on;
(6)镀膜室51压强降至0.1Pa时,打开第四真空阀510,镀膜室51由电弧泵1+牵引分子泵53+深冷泵56抽气;(6) When the pressure of the coating chamber 51 is reduced to 0.1 Pa, the fourth vacuum valve 510 is opened, and the coating chamber 51 is evacuated by the arc pump 1 + the traction molecular pump 53 + the cryogenic pump 56;
(7)当镀膜室51压强降至蒸发镀膜所需的真空度(例如5×10-2Pa)时, 开始预熔,镀膜;(7) when the pressure of the coating chamber 51 is reduced to the degree of vacuum required for the evaporation coating (for example, 5 × 10 -2 Pa), pre-melting is started, and the coating is performed;
(8)镀膜结束,冷却约1分钟,先后关闭第四真空阀510和第二真空阀55,关闭电弧泵1,然后打开放气阀511放气,向镀膜室51注入大气,打开镀膜室51,取出已镀工件,完成镀膜周期。(8) After the coating is completed, the cooling is performed for about 1 minute, the fourth vacuum valve 510 and the second vacuum valve 55 are closed, the arc pump 1 is turned off, and then the deflation valve 511 is opened to deflate, and the atmosphere is injected into the coating chamber 51 to open the coating chamber 51. , the plated workpiece is taken out, and the coating cycle is completed.
本实施例五提供的深冷电弧泵蒸发镀膜机组,采用深冷泵56抽除中、高真空的可凝气体,采用电弧泵1抽除高真空的活性气体,抽气效率显著提高,与传统扩散泵蒸发镀膜设备相比,节省抽气能耗高达80%,显著提高产品真空镀膜质量,还能提高生产效率约一倍,而且,相同产能的设备费用还略有下降,经济效益显著。The cryogenic arc pump evaporation coating unit provided in the fifth embodiment adopts a cryogenic pump 56 to remove the medium and high vacuum condensable gas, and the arc pump 1 is used to remove the high vacuum active gas, and the pumping efficiency is remarkably improved, and the conventional Compared with the diffusion pump evaporation coating equipment, the energy consumption of pumping is up to 80%, the vacuum coating quality of the product is significantly improved, and the production efficiency is doubled. Moreover, the equipment cost of the same capacity is slightly reduced, and the economic benefit is remarkable.
以上所述是本发明的优选实施方式,应当指出,对于本技术领域的普通技术人员来说,在不脱离本发明原理的前提下,还可以做出若干改进和润饰,这些改进和润饰也视为本发明的保护范围。 The above is a preferred embodiment of the present invention, and it should be noted that those skilled in the art can also make several improvements and retouchings without departing from the principles of the present invention. It is the scope of protection of the present invention.

Claims (9)

  1. 一种高真空电弧泵,包括泵壳和电源,所述泵壳上设有泵口,所述泵壳一侧的可开合的面板上固设有基座,所述基座与所述面板绝缘,所述基座与所述电源负极电连接,所述基座内侧端与阴极靶固定连接,所述电源正极与所述泵壳电连接,其特征在于,所述泵壳内还设有位于所述阴极靶和所述面板之间的金属挡板,所述金属挡板与周围部件绝缘。A high vacuum arc pump includes a pump casing and a power source, a pump port is disposed on the pump casing, and a base is fixed on the openable panel on one side of the pump casing, and the base and the panel are Insulation, the pedestal is electrically connected to the negative pole of the power source, the inner end of the pedestal is fixedly connected to the cathode target, and the positive pole of the power source is electrically connected to the pump casing, wherein the pump casing is further provided A metal baffle between the cathode target and the panel, the metal baffle being insulated from surrounding components.
  2. 如权利要求1所述的高真空电弧泵,其特征在于,所述阴极靶与基座之间设有材质特征光谱与所述阴极靶的特征光谱相异的导热薄层。The high vacuum arc pump according to claim 1, wherein a heat conductive thin layer having a material characteristic spectrum different from a characteristic spectrum of the cathode target is disposed between the cathode target and the susceptor.
  3. 如权利要求2所述的高真空电弧泵,其特征在于,所述导热薄层的材料为铁或铜,所述导热薄层的厚度为0.5~2mm。The high vacuum arc pump according to claim 2, wherein the heat conductive thin layer is made of iron or copper, and the heat conductive thin layer has a thickness of 0.5 to 2 mm.
  4. 如权利要求1所述的高真空电弧泵,其特征在于,所述阴极靶的材料为钛。A high vacuum arc pump according to claim 1 wherein the material of the cathode target is titanium.
  5. 如权利要求1~4中任一项所述的高真空电弧泵,其特征在于,所述阴极靶中掺入有其它材料,所述其它材料为镁、铝、锌、钙或其中任意至少两种的混合,所述其它材料在所述阴极靶中的重量百分比为0.5~80%。The high vacuum arc pump according to any one of claims 1 to 4, wherein the cathode target is doped with other materials, and the other materials are magnesium, aluminum, zinc, calcium or at least two of them. Kind of mixing, the weight percentage of the other material in the cathode target is 0.5-80%.
  6. 一种高真空电弧泵机组,包括真空室,其特征在于,所述真空室分别连接有粗抽泵、牵引分子泵以及如权利要求1~5中任一项所述的高真空电弧泵;A high vacuum arc pump unit, comprising a vacuum chamber, wherein the vacuum chamber is respectively connected with a rough pump, a traction molecular pump, and the high vacuum arc pump according to any one of claims 1 to 5;
    所述真空室通过第一真空阀与所述粗抽泵连接,所述真空室通过第二真空阀与所述牵引分子泵连接,所述牵引分子泵通过第三真空阀与前级泵连接,所述真空室依次经挡尘板、第四真空阀与所述高真空电弧泵连接,所述真空室还分别连接有放气阀和真空规。The vacuum chamber is connected to the rough pump through a first vacuum valve, the vacuum chamber is connected to the traction molecular pump through a second vacuum valve, and the traction molecular pump is connected to the foreline pump through a third vacuum valve. The vacuum chamber is sequentially connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the vacuum chamber is further connected with a gas release valve and a vacuum gauge.
  7. 一种深冷高真空电弧泵机组,包括真空室,其特征在于,所述真空室分别连接有深冷泵、粗抽泵、牵引分子泵以及如权利要求1~5中任一项所述的高真空电弧泵;A cryogenic high vacuum arc pump unit comprising a vacuum chamber, wherein the vacuum chamber is respectively connected with a cryogenic pump, a rough pump, a traction molecular pump, and the method according to any one of claims 1 to 5 High vacuum arc pump;
    所述真空室通过第一真空阀与所述粗抽泵连接,所述真空室直接或通过第二真空阀分别与所述深冷泵和牵引分子泵连接,所述牵引分子泵通过第三真空阀与前级泵连接,所述真空室经挡尘板和第四真空阀与所述高真空电弧泵连接,所述真空室还分别连接有放气阀和真空规。The vacuum chamber is connected to the rough pump through a first vacuum valve, and the vacuum chamber is respectively connected to the cryogenic pump and the traction molecular pump through a second vacuum valve, and the traction molecular pump passes through a third vacuum The valve is connected to the foreline pump, and the vacuum chamber is connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the vacuum chamber is further connected with a vent valve and a vacuum gauge, respectively.
  8. 一种高真空蒸发镀膜机组,包括镀膜室,其特征在于,所述镀膜室分别连接有粗抽泵、牵引分子泵以及如权利要求1~5中任一项所述的高真空电弧泵; A high vacuum evaporation coating unit comprising a coating chamber, wherein the coating chamber is respectively connected with a rough pump, a traction molecular pump and the high vacuum arc pump according to any one of claims 1 to 5;
    所述镀膜室通过第一真空阀与所述粗抽泵连接,所述镀膜室通过第二真空阀与所述牵引分子泵连接,所述牵引分子泵通过第三真空阀与前级泵连接,所述镀膜室经挡尘板和第四真空阀与所述高真空电弧泵连接,所述镀膜室还分别连接有放气阀和真空规。The coating chamber is connected to the rough pump through a first vacuum valve, the coating chamber is connected to the traction molecular pump through a second vacuum valve, and the traction molecular pump is connected to the foreline pump through a third vacuum valve. The coating chamber is connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the coating chamber is also connected with a vent valve and a vacuum gauge, respectively.
  9. 一种深冷电弧泵蒸发镀膜机组,包括镀膜室,其特征在于,所述镀膜室分别连接有粗抽泵、牵引分子泵以及如权利要求1~5中任一项所述的高真空电弧泵;A cryogenic arc pump evaporation coating unit, comprising a coating chamber, wherein the coating chamber is respectively connected with a rough pump, a traction molecular pump, and the high vacuum arc pump according to any one of claims 1 to 5. ;
    所述镀膜室通过第一真空阀与所述粗抽泵连接,所述镀膜室通过第二真空阀分别与深冷泵和所述牵引分子泵连接,所述牵引分子泵通过第三真空阀与前级泵连接,所述镀膜室依次经挡尘板、第四真空阀与所述高真空电弧泵连接,所述镀膜室还分别连接有放气阀和真空规。 The coating chamber is connected to the rough pump through a first vacuum valve, and the coating chamber is respectively connected to a cryogenic pump and the traction molecular pump through a second vacuum valve, and the traction molecular pump passes through a third vacuum valve The front stage pump is connected, and the coating chamber is connected to the high vacuum arc pump via a dust shield and a fourth vacuum valve, and the coating chamber is further connected with a gas release valve and a vacuum gauge.
PCT/CN2015/083276 2014-07-17 2015-07-03 High vacuum electric arc pump and air extraction unit thereof WO2016008367A1 (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104100492B (en) * 2014-07-17 2017-07-25 储继国 High vacuum electric arc pump and its pumping unit

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2239511Y (en) * 1995-10-24 1996-11-06 袁哲 Vacuum electric arc Ti pump
DE10241549B4 (en) * 2002-09-05 2004-07-22 Nawotec Gmbh Orbitron pump
CN101294270A (en) * 2008-06-06 2008-10-29 东北大学 Equipment and method for producing nichrome composite plate with vacuum arc ion plating
CN101936278A (en) * 2010-09-13 2011-01-05 储继国 Electric arc titanium pump and vacuum air pump group comprising same
CN201891569U (en) * 2010-11-26 2011-07-06 黄瑞安 Vacuum electric arc titanium pump
CN103290388A (en) * 2013-06-19 2013-09-11 储昕 Plasma coating equipment and air extraction process thereof
CN104100492A (en) * 2014-07-17 2014-10-15 储继国 High vacuum arc pump and pumping unit thereof
CN204061092U (en) * 2014-07-17 2014-12-31 储继国 High vacuum electric arc pump and unit of bleeding thereof

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202131364U (en) * 2011-06-27 2012-02-01 肇庆市科润真空设备有限公司 Glass film plating technical chamber
CN102978577A (en) * 2011-09-06 2013-03-20 鸿富锦精密工业(深圳)有限公司 Intermediate-frequency magnetron sputtering coating device
CN102691640B (en) * 2012-05-29 2015-12-02 储琦 A kind of extract system and technique

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2239511Y (en) * 1995-10-24 1996-11-06 袁哲 Vacuum electric arc Ti pump
DE10241549B4 (en) * 2002-09-05 2004-07-22 Nawotec Gmbh Orbitron pump
CN101294270A (en) * 2008-06-06 2008-10-29 东北大学 Equipment and method for producing nichrome composite plate with vacuum arc ion plating
CN101936278A (en) * 2010-09-13 2011-01-05 储继国 Electric arc titanium pump and vacuum air pump group comprising same
CN201891569U (en) * 2010-11-26 2011-07-06 黄瑞安 Vacuum electric arc titanium pump
CN103290388A (en) * 2013-06-19 2013-09-11 储昕 Plasma coating equipment and air extraction process thereof
CN104100492A (en) * 2014-07-17 2014-10-15 储继国 High vacuum arc pump and pumping unit thereof
CN204061092U (en) * 2014-07-17 2014-12-31 储继国 High vacuum electric arc pump and unit of bleeding thereof

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