WO2013082337A1 - One component self-adhesive dental composition, process of production and use thereof - Google Patents

One component self-adhesive dental composition, process of production and use thereof Download PDF

Info

Publication number
WO2013082337A1
WO2013082337A1 PCT/US2012/067159 US2012067159W WO2013082337A1 WO 2013082337 A1 WO2013082337 A1 WO 2013082337A1 US 2012067159 W US2012067159 W US 2012067159W WO 2013082337 A1 WO2013082337 A1 WO 2013082337A1
Authority
WO
WIPO (PCT)
Prior art keywords
component
composition
copper
meth
composition according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2012/067159
Other languages
English (en)
French (fr)
Inventor
Reinhold Hecht
Andrea Stippschild
Vitore HASANAJ
Gioacchino Raia
Manfred Ludsteck
Rainer Guggenberger
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Priority to EP12798129.8A priority Critical patent/EP2785307B1/en
Priority to JP2014544899A priority patent/JP6139551B2/ja
Priority to US14/360,373 priority patent/US9132069B2/en
Priority to CN201280059074.1A priority patent/CN104114142B/zh
Priority to BR112014013111A priority patent/BR112014013111A2/pt
Priority to RU2014121153/15A priority patent/RU2600814C2/ru
Publication of WO2013082337A1 publication Critical patent/WO2013082337A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00Preparations for dentistry
    • A61K6/50Preparations specially adapted for dental root treatment
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J133/00Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
    • C09J133/04Homopolymers or copolymers of esters
    • C09J133/06Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09J133/10Homopolymers or copolymers of methacrylic acid esters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61CDENTISTRY; APPARATUS OR METHODS FOR ORAL OR DENTAL HYGIENE
    • A61C19/00Dental auxiliary appliances
    • A61C19/003Apparatus for curing resins by radiation
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00Preparations for dentistry
    • A61K6/15Compositions characterised by their physical properties
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00Preparations for dentistry
    • A61K6/60Preparations for dentistry comprising organic or organo-metallic additives
    • A61K6/62Photochemical radical initiators
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00Preparations for dentistry
    • A61K6/70Preparations for dentistry comprising inorganic additives
    • A61K6/71Fillers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00Preparations for dentistry
    • A61K6/80Preparations for artificial teeth, for filling teeth or for capping teeth
    • A61K6/884Preparations for artificial teeth, for filling teeth or for capping teeth comprising natural or synthetic resins
    • A61K6/887Compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J133/00Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
    • C09J133/04Homopolymers or copolymers of esters
    • C09J133/14Homopolymers or copolymers of esters of esters containing halogen, nitrogen, sulfur or oxygen atoms in addition to the carboxy oxygen
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J175/00Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
    • C09J175/04Polyurethanes
    • C09J175/14Polyurethanes having carbon-to-carbon unsaturated bonds
    • C09J175/16Polyurethanes having carbon-to-carbon unsaturated bonds having terminal carbon-to-carbon unsaturated bonds

Definitions

  • (meth) acryl is a shorthand term referring to "acryl” and/or "methacryl".
  • a "nano-sized filler” is a filler, the individual particles thereof have a size in the region of nanometers, e.g. an average particle diameter of less than about 200 nm. Useful examples are given in US 6,899,948 and US 6,572,693, the content of which especially with regard to nano- sized silica particles is herein incorporated by reference.
  • Viscosity from about 0.1 to about 10 Pa * s, or from about 0.2 to about 5 Pa * s or from about 0.5 to about 2 Pa * s measured at 23°C, and/or
  • the second component in a ternary photoinitiator system is a sensitizer.
  • the sensitizer desirably is soluble in the monomer, and is capable of light absorption somewhere within the range of wavelengths of greater than 400 to 1200 nanometers, more preferably greater than 400 to 700 nanometers and most preferably greater than 400 to about 600 nanometers.
  • the sensitizer may also be capable of sensitizing 2-methyl-4,6-bis(trichloromethyl)-s-triazine, using the test procedure described in US 3,729,313, which is incorporated herein by reference.
  • a sensitizer is also selected based in part upon shelf stability considerations. Accordingly, selection of a particular sensitizer may depend to some extent upon the particular monomer, oligomer or polymer, iodonium salt and donor chosen.
  • Suitable acylphosphine oxides can be described by the general formula
  • Further examples include: bis-(2,6-dichlorobenzoyl)phenylphosphine oxide, bis-(2,6- dichlorobenzoyl)-2,5-dimethylphenylphosphine oxide, bis-(2,6-dichlorobenzoyl)-4-ethoxy- phenylphosphine oxide, bis-(2,6-dichlorobenzoyl)-4-biphenylylphosphine oxide, bis-(2,6- dichlorobenzoyl)-4-propylphenylphosphine oxide, bis-(2,6-dichlorobenzoyl)-2-naphthyl- phosphine oxide, bis-(2,6-dichlorobenzoyl)-1 -napthylphosphine oxide, bis-(2,6-dichlorobenzoyl)- 4-chlorophenylphosphine oxide, bis-(2,6-dichlorobenzoyl)-2,4

Landscapes

  • Health & Medical Sciences (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plastic & Reconstructive Surgery (AREA)
  • Dentistry (AREA)
  • Inorganic Chemistry (AREA)
  • Biophysics (AREA)
  • Dental Preparations (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Adhesives Or Adhesive Processes (AREA)
PCT/US2012/067159 2011-12-01 2012-11-30 One component self-adhesive dental composition, process of production and use thereof Ceased WO2013082337A1 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
EP12798129.8A EP2785307B1 (en) 2011-12-01 2012-11-30 One component self-adhesive dental composition, process of production and use thereof
JP2014544899A JP6139551B2 (ja) 2011-12-01 2012-11-30 一成分自己接着性歯科用組成物、その製造方法、及び使用
US14/360,373 US9132069B2 (en) 2011-12-01 2012-11-30 One component self-adhesive dental composition, process of production and use thereof
CN201280059074.1A CN104114142B (zh) 2011-12-01 2012-11-30 单组分自粘合牙科组合物、其制备和使用方法
BR112014013111A BR112014013111A2 (pt) 2011-12-01 2012-11-30 composição dental autoadesiva de componente único, processo de produção e utilização do mesmo
RU2014121153/15A RU2600814C2 (ru) 2011-12-01 2012-11-30 Однокомпонентный самоклеющийся стоматологический состав, способ его изготовления и применения

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP11191541 2011-12-01
EP11191541.9 2011-12-01

Publications (1)

Publication Number Publication Date
WO2013082337A1 true WO2013082337A1 (en) 2013-06-06

Family

ID=47297485

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2012/067159 Ceased WO2013082337A1 (en) 2011-12-01 2012-11-30 One component self-adhesive dental composition, process of production and use thereof

Country Status (7)

Country Link
US (1) US9132069B2 (enExample)
EP (1) EP2785307B1 (enExample)
JP (1) JP6139551B2 (enExample)
CN (1) CN104114142B (enExample)
BR (1) BR112014013111A2 (enExample)
RU (1) RU2600814C2 (enExample)
WO (1) WO2013082337A1 (enExample)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2015126666A1 (en) * 2014-02-18 2015-08-27 3M Innovative Properties Company Dental composition and use thereof
CN106029044A (zh) * 2014-02-18 2016-10-12 3M创新有限公司 粘合剂粘结组合物及其用途
WO2017079189A1 (en) * 2015-11-06 2017-05-11 3M Innovative Properties Company Redox polymerizable dental composition with photolabile transition metal complexes
WO2017078883A1 (en) * 2015-11-06 2017-05-11 3M Innovative Properties Company Redox polymerizable composition with photolabile transition metal complexes
WO2019211724A2 (en) 2018-05-02 2019-11-07 3M Innovative Properties Company One-part dental adhesive composition for fixing dental composite materials
GB2583920A (en) * 2019-05-10 2020-11-18 Henkel IP & Holding GmbH Method for bonding three-dimensional articles made by additive manufacturing
US10987281B2 (en) 2016-10-21 2021-04-27 Kuraray Noritake Dental Inc. Self-adhesive dental composite resin
CN112996472A (zh) * 2018-11-14 2021-06-18 3M创新有限公司 储存稳定的双组分双固化牙科组合物

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CN106029045B (zh) * 2014-02-18 2020-04-03 3M创新有限公司 牙科组合物及其用途
CN104592927B (zh) * 2015-02-09 2017-02-22 哈尔滨理工大学 一种点胶纸用水溶性粘合剂的制备方法
EP3153756B1 (en) * 2015-10-08 2020-05-06 Crompton Technology Group Limited Electrical isolator
CN108368202B (zh) * 2015-12-03 2020-10-16 3M创新有限公司 具有光不稳定还原剂的氧化还原可聚合组合物
EP3386462B1 (en) * 2015-12-08 2024-10-23 Solventum Intellectual Properties Company Two-component self-adhesive dental composition, storage stable initiator system, and use thereof
CN106726623B (zh) * 2016-12-28 2020-12-04 日照沪鸽生物材料有限公司 用于牙体修复具有氟离子释放特性的单组分光固化复合材料及其应用
JP6793106B2 (ja) * 2017-11-14 2020-12-02 株式会社ジーシー 歯科用光重合性組成物及び光重合開始剤
CN111491600A (zh) 2017-12-26 2020-08-04 德山齿科株式会社 牙科用修复材料和由其构成的牙科切削加工用树脂材料
US11325993B2 (en) 2017-12-26 2022-05-10 Tokuyama Dental Corporation Chemical polymerization initiator, adhesive composition, adhesive composition kit, dental material, dental material kit, and method of storing adhesive composition
JP6779506B2 (ja) * 2018-09-21 2020-11-04 株式会社トクヤマデンタル 光硬化性組成物
CN110051542B (zh) * 2019-04-25 2022-02-01 北京海吉雅医疗器材有限公司 一种齿科藻酸盐印模材料及其制备方法
CN112316200A (zh) * 2020-07-20 2021-02-05 北京奥凯伟迪生物科技有限公司 一种用于骨头粘结的双固化粘结剂及其制备方法
WO2023136337A1 (ja) 2022-01-14 2023-07-20 クラレノリタケデンタル株式会社 歯科用組成物及びその製造方法並びに歯科用表面処理フィラー

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Cited By (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106029044A (zh) * 2014-02-18 2016-10-12 3M创新有限公司 粘合剂粘结组合物及其用途
CN106029046A (zh) * 2014-02-18 2016-10-12 3M创新有限公司 牙科用组合物及其用途
JP2017506245A (ja) * 2014-02-18 2017-03-02 スリーエム イノベイティブ プロパティズ カンパニー 歯科用組成物及びその使用
US10010488B2 (en) 2014-02-18 2018-07-03 3M Innovative Properties Company Dental composition and use thereof
CN106029046B (zh) * 2014-02-18 2019-04-05 3M创新有限公司 牙科用组合物及其用途
WO2015126666A1 (en) * 2014-02-18 2015-08-27 3M Innovative Properties Company Dental composition and use thereof
CN106029044B (zh) * 2014-02-18 2019-12-31 3M创新有限公司 粘合剂粘结组合物及其用途
US10617607B2 (en) 2015-11-06 2020-04-14 3M Innovative Properties Company Redox polymerizable dental composition with photolabile transition metal complexes
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EP2785307A1 (en) 2014-10-08
US9132069B2 (en) 2015-09-15
RU2014121153A (ru) 2016-02-10
CN104114142B (zh) 2016-12-21
CN104114142A (zh) 2014-10-22
US20140329205A1 (en) 2014-11-06
RU2600814C2 (ru) 2016-10-27
EP2785307B1 (en) 2019-06-26
JP6139551B2 (ja) 2017-05-31
JP2015507610A (ja) 2015-03-12
BR112014013111A2 (pt) 2017-06-13

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