WO2012068277A3 - Processus, procédé et système d'élimination de métaux lourds présents dans des fluides - Google Patents

Processus, procédé et système d'élimination de métaux lourds présents dans des fluides Download PDF

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Publication number
WO2012068277A3
WO2012068277A3 PCT/US2011/061035 US2011061035W WO2012068277A3 WO 2012068277 A3 WO2012068277 A3 WO 2012068277A3 US 2011061035 W US2011061035 W US 2011061035W WO 2012068277 A3 WO2012068277 A3 WO 2012068277A3
Authority
WO
WIPO (PCT)
Prior art keywords
heavy metals
crude oil
salts
water phase
group
Prior art date
Application number
PCT/US2011/061035
Other languages
English (en)
Other versions
WO2012068277A2 (fr
Inventor
Sujin Yean
Original Assignee
Chevron U.S.A. Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US12/950,060 external-priority patent/US8728303B2/en
Priority claimed from US12/950,170 external-priority patent/US8721873B2/en
Priority claimed from US12/950,637 external-priority patent/US8721874B2/en
Priority to CA2818273A priority Critical patent/CA2818273A1/fr
Priority to AU2011328930A priority patent/AU2011328930A1/en
Priority to EP11841430.9A priority patent/EP2640810B1/fr
Application filed by Chevron U.S.A. Inc. filed Critical Chevron U.S.A. Inc.
Priority to RU2013127659/04A priority patent/RU2013127659A/ru
Priority to CN2011800589006A priority patent/CN103249814A/zh
Priority to SG2013035829A priority patent/SG190775A1/en
Priority to BR112013012087A priority patent/BR112013012087A2/pt
Publication of WO2012068277A2 publication Critical patent/WO2012068277A2/fr
Publication of WO2012068277A3 publication Critical patent/WO2012068277A3/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G27/00—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation
    • C10G27/04—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen
    • C10G27/10—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen in the presence of metal-containing organic complexes, e.g. chelates, or cationic ion-exchange resins
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G27/00—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation
    • C10G27/02—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with halogen or compounds generating halogen; Hypochlorous acid or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G27/00—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation
    • C10G27/04—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen
    • C10G27/12—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen with oxygen-generating compounds, e.g. per-compounds, chromic acid, chromates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G27/00—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation
    • C10G27/04—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen
    • C10G27/14—Refining of hydrocarbon oils in the absence of hydrogen, by oxidation with oxygen or compounds generating oxygen with ozone-containing gases
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G29/00—Refining of hydrocarbon oils, in the absence of hydrogen, with other chemicals
    • C10G29/06—Metal salts, or metal salts deposited on a carrier
    • C10G29/12—Halides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1033—Oil well production fluids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/205—Metal content
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/30—Physical properties of feedstocks or products
    • C10G2300/308—Gravity, density, e.g. API
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/80—Additives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/80—Additives
    • C10G2300/805—Water

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

Cette invention concerne la réduction de métaux lourds présents à l'état de trace, tels que le mercure ou l'arsenic, dans du pétrole brut en mettant en contact le pétrole brut avec un agent oxydant, et en extrayant les métaux lourds dans une phase hydrique pour une séparation ultérieure du pétrole brut. Dans un mode de réalisation, l'agent oxydant est choisi dans le groupe constitué par les hydroperoxydes, les peroxydes organiques, les peracides inorganiques et leurs sels, les peracides organiques et leurs sels, les halogènes comme l'iode (I2), le brome (Br2) et l'ozone. Dans un autre mode de réalisation, au moins un agent complexant choisi dans le groupe constitué par les halogénures métallisés et/ou les composés soufrés peut être ajouté pour faciliter l'élimination des métaux lourds présents dans le pétrole brut en formant des complexes de métaux lourds solubles dans la phase aqueuse.
PCT/US2011/061035 2010-11-19 2011-11-16 Processus, procédé et système d'élimination de métaux lourds présents dans des fluides WO2012068277A2 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
BR112013012087A BR112013012087A2 (pt) 2010-11-19 2011-11-16 processo, método, e sistema para a remoção de metais pesados de fluidos
SG2013035829A SG190775A1 (en) 2010-11-19 2011-11-16 Process, method, and system for removing heavy metals from fluids
CN2011800589006A CN103249814A (zh) 2010-11-19 2011-11-16 从流体中脱除重金属的工艺、方法和系统
AU2011328930A AU2011328930A1 (en) 2010-11-19 2011-11-16 Process, method, and system for removing heavy metals from fluids
EP11841430.9A EP2640810B1 (fr) 2010-11-19 2011-11-16 Procédé d'élimination de métaux lourds présents dans des fluides
CA2818273A CA2818273A1 (fr) 2010-11-19 2011-11-16 Processus, procede et systeme d'elimination de metaux lourds presents dans des fluides
RU2013127659/04A RU2013127659A (ru) 2010-11-19 2011-11-16 Процесс, способ и система для удаления тяжелых металлов из жидкостей

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
US12/950,170 2010-11-19
US12/950,060 US8728303B2 (en) 2010-11-19 2010-11-19 Process, method, and system for removing heavy metals from fluids
US12/950,637 2010-11-19
US12/950,637 US8721874B2 (en) 2010-11-19 2010-11-19 Process, method, and system for removing heavy metals from fluids
US12/950,060 2010-11-19
US12/950,170 US8721873B2 (en) 2010-11-19 2010-11-19 Process, method, and system for removing heavy metals from fluids

Publications (2)

Publication Number Publication Date
WO2012068277A2 WO2012068277A2 (fr) 2012-05-24
WO2012068277A3 true WO2012068277A3 (fr) 2012-09-07

Family

ID=46084624

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2011/061035 WO2012068277A2 (fr) 2010-11-19 2011-11-16 Processus, procédé et système d'élimination de métaux lourds présents dans des fluides

Country Status (8)

Country Link
EP (1) EP2640810B1 (fr)
CN (1) CN103249814A (fr)
AU (1) AU2011328930A1 (fr)
BR (1) BR112013012087A2 (fr)
CA (1) CA2818273A1 (fr)
RU (1) RU2013127659A (fr)
SG (1) SG190775A1 (fr)
WO (1) WO2012068277A2 (fr)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104093819A (zh) * 2011-12-30 2014-10-08 雪佛龙美国公司 液体中去除重金属的工艺、方法和系统
US9023196B2 (en) * 2013-03-14 2015-05-05 Chevron U.S.A. Inc. Process, method, and system for removing heavy metals from fluids
CN103450930B (zh) * 2013-03-26 2016-06-29 湖南长岭石化科技开发有限公司 一种原油脱金属脱水的方法
CN103263835B (zh) * 2013-05-24 2015-05-20 上海交通大学 一种溴化铁除汞复配液及用其进行烟气除汞的方法
US9523043B2 (en) 2013-09-16 2016-12-20 Chevron U.S.A. Inc. Process, method, and system for removing heavy metals from fluids
CN103848523B (zh) * 2014-04-01 2016-01-13 哈尔滨工业大学 一种强化锰氧化物去除水中Hg(Ⅱ)的络合剂的方法
CN104032137B (zh) * 2014-06-05 2016-06-22 东北大学 一种以硒化物形式从含汞尾渣中回收汞的方法
CN104032138B (zh) * 2014-06-05 2016-04-20 东北大学 一种堆浸-沉淀稳定化处理含汞尾渣的方法
RU2688992C1 (ru) * 2017-12-25 2019-05-23 Публичное акционерное общество "Татнефть" имени В.Д. Шашина Состав для удаления отложений неорганических солей в скважине (варианты)
CN108659947B (zh) * 2018-06-12 2022-02-22 山东蓝奥生物技术有限公司 一种采用南极磷虾制备南极磷虾油和蛋白粉的方法、南极磷虾油及蛋白粉
SG11202105464XA (en) * 2018-12-03 2021-06-29 Ecolab Usa Inc Use of peroxyacids/hydrogen peroxide for removal of metal components from petroleum and hydrocarbon streams for downstream applications
RU2691070C1 (ru) * 2018-12-27 2019-06-10 Акционерное общество "Всероссийский научно-исследовательский институт по переработке нефти" (АО "ВНИИ НП") Способ получения каталитически-сорбционного материала и способ извлечения мышьяка в его присутствии
CN113564357A (zh) * 2021-07-29 2021-10-29 南昌航空大学 一种湿法冶金用复合药剂及其制备方法和应用
CN114059989B (zh) * 2021-11-09 2024-04-26 青海省柴达木综合地质矿产勘查院 一种低品位固体钾盐矿的溶采方法
CN115178242B (zh) * 2022-06-28 2023-06-06 中国地质大学（武汉） 一种固定五价砷离子的吸附膜及其制备方法和应用

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US4552646A (en) * 1984-12-24 1985-11-12 Phillips Petroleum Company Dearsenating of shale oil with metal chlorates
US5173286A (en) * 1991-07-19 1992-12-22 Mobil Oil Corporation Fixation of elemental mercury present in spent molecular sieve desiccant for disposal
JPH10216476A (ja) * 1997-01-31 1998-08-18 Kawasaki Heavy Ind Ltd 排ガス処理方法及び装置
US5908557A (en) * 1997-05-12 1999-06-01 Ntec Solutions, Inc. Process for the removal of pentavalent arsenic from water
US6117333A (en) * 1997-04-22 2000-09-12 Union Oil Company Of California Removal of hydrocarbons, mercury and arsenic from oil-field produced water
US6197269B1 (en) * 1995-07-07 2001-03-06 Nederlandse Organisatie Voor Toegepast-Natuurwetenschappelijk Onderzoek (Tno) Method for absorbing gaseous oxidizable or reducible constituents through a membrane
US20060239877A1 (en) * 2005-04-21 2006-10-26 Envirosolv Energy Llc Method for removing sulfur dioxide, mercury, and nitrogen oxides from a gas stream
US20100000910A1 (en) * 2008-07-03 2010-01-07 Chevron U.S.A. Inc. System and method for separating a trace element from a liquid hydrocarbon feed
US20100078358A1 (en) * 2008-09-30 2010-04-01 Erin E Tullos Mercury removal process
US20100210889A1 (en) * 2009-02-17 2010-08-19 Conocophillips Company Mercury removal from hydrocarbons

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US4552646A (en) * 1984-12-24 1985-11-12 Phillips Petroleum Company Dearsenating of shale oil with metal chlorates
US5173286A (en) * 1991-07-19 1992-12-22 Mobil Oil Corporation Fixation of elemental mercury present in spent molecular sieve desiccant for disposal
US6197269B1 (en) * 1995-07-07 2001-03-06 Nederlandse Organisatie Voor Toegepast-Natuurwetenschappelijk Onderzoek (Tno) Method for absorbing gaseous oxidizable or reducible constituents through a membrane
JPH10216476A (ja) * 1997-01-31 1998-08-18 Kawasaki Heavy Ind Ltd 排ガス処理方法及び装置
US6117333A (en) * 1997-04-22 2000-09-12 Union Oil Company Of California Removal of hydrocarbons, mercury and arsenic from oil-field produced water
US5908557A (en) * 1997-05-12 1999-06-01 Ntec Solutions, Inc. Process for the removal of pentavalent arsenic from water
US20060239877A1 (en) * 2005-04-21 2006-10-26 Envirosolv Energy Llc Method for removing sulfur dioxide, mercury, and nitrogen oxides from a gas stream
US20100000910A1 (en) * 2008-07-03 2010-01-07 Chevron U.S.A. Inc. System and method for separating a trace element from a liquid hydrocarbon feed
US20100078358A1 (en) * 2008-09-30 2010-04-01 Erin E Tullos Mercury removal process
US20100210889A1 (en) * 2009-02-17 2010-08-19 Conocophillips Company Mercury removal from hydrocarbons

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Title
See also references of EP2640810A4 *

Also Published As

Publication number Publication date
RU2013127659A (ru) 2014-12-27
EP2640810A2 (fr) 2013-09-25
WO2012068277A2 (fr) 2012-05-24
CN103249814A (zh) 2013-08-14
BR112013012087A2 (pt) 2016-08-16
EP2640810A4 (fr) 2014-09-17
AU2011328930A1 (en) 2013-05-30
CA2818273A1 (fr) 2012-05-24
EP2640810B1 (fr) 2016-03-02
SG190775A1 (en) 2013-07-31

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