WO2011053037A3 - 금나노입자의 제조방법 - Google Patents

금나노입자의 제조방법 Download PDF

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Publication number
WO2011053037A3
WO2011053037A3 PCT/KR2010/007516 KR2010007516W WO2011053037A3 WO 2011053037 A3 WO2011053037 A3 WO 2011053037A3 KR 2010007516 W KR2010007516 W KR 2010007516W WO 2011053037 A3 WO2011053037 A3 WO 2011053037A3
Authority
WO
WIPO (PCT)
Prior art keywords
gold nanoparticles
solution
chloroauric acid
mixture
prepare
Prior art date
Application number
PCT/KR2010/007516
Other languages
English (en)
French (fr)
Other versions
WO2011053037A2 (ko
Inventor
이재범
이재욱
Original Assignee
부산대학교 산학협력단
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 부산대학교 산학협력단 filed Critical 부산대학교 산학협력단
Priority to KR1020127014924A priority Critical patent/KR101344051B1/ko
Publication of WO2011053037A2 publication Critical patent/WO2011053037A2/ko
Publication of WO2011053037A3 publication Critical patent/WO2011053037A3/ko

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G7/00—Compounds of gold
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/84—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer

Abstract

본 발명은 금나노입자의 제조방법에 관한 것으로, 보다 구체적으로는 염화금산(HAuCl4)을 증류수에 녹여 염화금산 용액을 제조하는 제 1단계; 제 1 파이토 화합물 용액에 제 2 파이토 화합물을 혼합하여 혼합용액을 제조하는 제 2단계; 상기 혼합용액을 상기 제1단계의 염화금산 용액에 첨가한 후 교반하여 금나노입자를 형성하는 제 3단계;를 포함하는 것을 특징으로 한다. 또한, 본 발명은 상기 형성된 금나노입자를 고분자 용액에 첨가한 후 초음파 분해를 수행하여 고분자를 금나노입자에 코팅하는 단계를 추가로 포함할 수 있다.
PCT/KR2010/007516 2009-10-30 2010-10-29 금나노입자의 제조방법 WO2011053037A2 (ko)

Priority Applications (1)

Application Number Priority Date Filing Date Title
KR1020127014924A KR101344051B1 (ko) 2009-10-30 2010-10-29 금나노입자의 제조방법

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR10-2009-0104313 2009-10-30
KR20090104313 2009-10-30

Publications (2)

Publication Number Publication Date
WO2011053037A2 WO2011053037A2 (ko) 2011-05-05
WO2011053037A3 true WO2011053037A3 (ko) 2011-10-13

Family

ID=43922862

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2010/007516 WO2011053037A2 (ko) 2009-10-30 2010-10-29 금나노입자의 제조방법

Country Status (2)

Country Link
KR (1) KR101344051B1 (ko)
WO (1) WO2011053037A2 (ko)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101333209B1 (ko) * 2011-06-17 2013-11-26 부산대학교 산학협력단 파이토케미컬로 표면처리된 금나노입자를 유효성분으로 함유하는 피부노화방지용 화장료 조성물
KR20140078977A (ko) 2012-12-18 2014-06-26 서울바이오시스 주식회사 고효율 발광 다이오드
CN104084597B (zh) * 2014-07-08 2015-05-20 青岛大学 含有金纳米粒子的分形树枝图案聚集体的制备方法
CN104209534B (zh) * 2014-07-30 2016-08-24 重庆凌峰橡塑制品有限公司 一种羟基氧化铁纳米棒-金纳米颗粒杂化结构的制备方法
KR101673686B1 (ko) 2014-11-03 2016-11-07 금오공과대학교 산학협력단 금 나노입자의 제조방법
KR101646617B1 (ko) * 2015-02-17 2016-08-09 부산대학교 산학협력단 파이토케미컬 유래 유기산을 포함하는 은나노입자 제조방법
CN109663931B (zh) * 2019-02-26 2022-02-22 云南师范大学 一种基于三七皂苷合成纳米金颗粒的方法
CN112387980A (zh) * 2019-08-19 2021-02-23 近镒生技股份有限公司 纳米金粒子、包含其的药物载体、其制备方法及其用途
KR102346758B1 (ko) 2019-12-03 2021-12-31 서강대학교산학협력단 금 나노입자 합성을 위한 미세 액적 기반 미세유체칩 및 이의 용도
CN115192706B (zh) * 2022-05-19 2023-05-26 中国医学科学院肿瘤医院 一种新型金纳米粒子的制备方法及其在治疗肿瘤中的应用

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20070042340A (ko) * 2005-10-18 2007-04-23 삼성전기주식회사 금속 나노 입자의 제조방법
JP2008106315A (ja) * 2006-10-26 2008-05-08 National Institute Of Advanced Industrial & Technology 金属ナノ粒子及びその製造方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20070042340A (ko) * 2005-10-18 2007-04-23 삼성전기주식회사 금속 나노 입자의 제조방법
JP2008106315A (ja) * 2006-10-26 2008-05-08 National Institute Of Advanced Industrial & Technology 金属ナノ粒子及びその製造方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
HOUSNI, ABDELGHANI ET AL.: "Monodisperse protein stabilized gold nanoparticles via a simple photochemical process.", J. PHYS. CHEM. C., vol. 112, 2008, pages 12282 - 12290 *
WANG, WENXING ET AL.: "One-step synthesis of biocompatible gold nanoparticles using gallic acid in the presence of poly-(N-vinyl-2-pyrrolidone).", COLLOIDS AND SURFACES A: PHYSICOCHEM. ENG. ASPECTS., vol. 301, 2007, pages 73 - 79 *

Also Published As

Publication number Publication date
WO2011053037A2 (ko) 2011-05-05
KR101344051B1 (ko) 2013-12-24
KR20120091345A (ko) 2012-08-17

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