WO2009077161A3 - Verfahren zur herstellung von fettsäurealkylestern - Google Patents

Verfahren zur herstellung von fettsäurealkylestern Download PDF

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Publication number
WO2009077161A3
WO2009077161A3 PCT/EP2008/010690 EP2008010690W WO2009077161A3 WO 2009077161 A3 WO2009077161 A3 WO 2009077161A3 EP 2008010690 W EP2008010690 W EP 2008010690W WO 2009077161 A3 WO2009077161 A3 WO 2009077161A3
Authority
WO
WIPO (PCT)
Prior art keywords
fatty acid
alkyl esters
acid alkyl
producing fatty
producing
Prior art date
Application number
PCT/EP2008/010690
Other languages
English (en)
French (fr)
Other versions
WO2009077161A2 (de
Inventor
Wulf Dietrich
Stefan Grasser
Dieter Heinz
Jürgen KARTHAUS
Leslaw Mleczko
Heinrich Morhenn
Rafael Warsitz
Ren WU
Original Assignee
Bayer Technology Services Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE102007061872A external-priority patent/DE102007061872A1/de
Priority claimed from DE102008036295A external-priority patent/DE102008036295A1/de
Application filed by Bayer Technology Services Gmbh filed Critical Bayer Technology Services Gmbh
Priority to AU2008337840A priority Critical patent/AU2008337840A1/en
Priority to US12/743,621 priority patent/US20100298586A1/en
Priority to CA2709575A priority patent/CA2709575A1/en
Priority to BRPI0821347-0A priority patent/BRPI0821347A2/pt
Priority to MX2010005939A priority patent/MX2010005939A/es
Priority to EP08860839A priority patent/EP2225353A2/de
Priority to CN2008801217051A priority patent/CN101903509A/zh
Publication of WO2009077161A2 publication Critical patent/WO2009077161A2/de
Publication of WO2009077161A3 publication Critical patent/WO2009077161A3/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/10—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of rare earths
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B01J35/647—2-50 nm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/66—Pore distribution
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

Die vorliegende Erfindung betrifft ein mehrstufiges Verfahren zur Herstellung von Fettsäurealkylestern.
PCT/EP2008/010690 2007-12-19 2008-12-16 Verfahren zur herstellung von fettsäurealkylestern WO2009077161A2 (de)

Priority Applications (7)

Application Number Priority Date Filing Date Title
AU2008337840A AU2008337840A1 (en) 2007-12-19 2008-12-16 Method for producing fatty acid alkyl esters
US12/743,621 US20100298586A1 (en) 2007-12-19 2008-12-16 Method for producing fatty acid alkyl esters
CA2709575A CA2709575A1 (en) 2007-12-19 2008-12-16 Method for producing fatty acid alkyl esters
BRPI0821347-0A BRPI0821347A2 (pt) 2007-12-19 2008-12-16 Processo para a produção de ésteres alquílicos de ácidos graxos
MX2010005939A MX2010005939A (es) 2007-12-19 2008-12-16 Procedimiento para la preparacion de esteres alquilicos de acidos grasos.
EP08860839A EP2225353A2 (de) 2007-12-19 2008-12-16 Verfahren zur herstellung von fettsäurealkylestern
CN2008801217051A CN101903509A (zh) 2007-12-19 2008-12-16 用于制备脂肪酸烷基酯的方法

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE102007061872A DE102007061872A1 (de) 2007-12-19 2007-12-19 Verfahren zur Herstellung von Fettsäurealkylestern
DE102007061872.9 2007-12-19
DE102008036295.6 2008-08-04
DE102008036295A DE102008036295A1 (de) 2008-08-04 2008-08-04 Katalysatorzusammensetzung zur Umesterung

Publications (2)

Publication Number Publication Date
WO2009077161A2 WO2009077161A2 (de) 2009-06-25
WO2009077161A3 true WO2009077161A3 (de) 2009-09-24

Family

ID=40565227

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2008/010690 WO2009077161A2 (de) 2007-12-19 2008-12-16 Verfahren zur herstellung von fettsäurealkylestern

Country Status (17)

Country Link
US (1) US20100298586A1 (de)
EP (1) EP2225353A2 (de)
CN (1) CN101903509A (de)
AR (1) AR071265A1 (de)
AU (1) AU2008337840A1 (de)
BR (1) BRPI0821347A2 (de)
CA (1) CA2709575A1 (de)
CL (1) CL2008003689A1 (de)
CO (1) CO6280548A2 (de)
EC (1) ECSP10010215A (de)
MX (1) MX2010005939A (de)
PE (1) PE20091660A1 (de)
PH (1) PH12010501172A1 (de)
RU (1) RU2010129470A (de)
TW (1) TW200942513A (de)
UY (1) UY31523A1 (de)
WO (1) WO2009077161A2 (de)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8070836B2 (en) * 2007-10-16 2011-12-06 Wayne State University Combined homogeneous and heterogeneous catalytic transesterification process for biodiesel production
DE102008036295A1 (de) * 2008-08-04 2010-02-11 Bayer Technology Services Gmbh Katalysatorzusammensetzung zur Umesterung
US20110224451A1 (en) * 2008-06-11 2011-09-15 Rajiv Kumar Chaturvedi Process for production of biodiesel
DE102009006777A1 (de) * 2009-01-30 2010-08-05 Wolfgang F. Prof. Dr. Hölderich Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen
US20110054200A1 (en) * 2009-09-01 2011-03-03 Catilin, Inc. Systems and Processes for Biodiesel Production
DE102009060881A1 (de) * 2009-12-30 2011-07-07 Emery Oleochemicals GmbH, 40589 Wärmetauscher in Verfahren und Vorrichtung zur Herstellung eines Esters
EP2446965A1 (de) * 2010-11-02 2012-05-02 Evonik Degussa GmbH Verfahren zur Herstellung von unterstützten Katalysatoren und Verwendung des Katalysators zur Veresterung von freien Fettsäuren in pflanzlichem Öl
EP2522712A1 (de) * 2011-05-13 2012-11-14 Cognis IP Management GmbH Verfahren zur Herstellung von Fettsäureniedrigalkylestern auf Basis von nicht-raffinierten Fetten und Ölen
TWI572352B (zh) * 2012-03-01 2017-03-01 波麥堤克藥學Ｓｍｔ有限公司 用於製備具中鏈長度之脂肪酸的三酸甘油酯之方法
CN103553923B (zh) * 2013-10-23 2016-06-01 南京工业大学 一种合成碳酸二月桂酯的生产方法
CN103922930B (zh) * 2014-05-06 2015-06-10 江苏瑞晨化学有限公司 一种多酸插层水滑石催化剂制备醋酸正丙酯的方法
MY191588A (en) * 2017-06-06 2022-06-30 Univ Putra Malaysia Method of producing fatty acid methyl ester
CN109608331B (zh) * 2018-12-13 2022-12-20 东营市海科新源化工有限责任公司 固体超强酸催化剂及其制备方法、异壬酸异壬酯的制备方法
CN109438243B (zh) * 2018-12-15 2021-06-01 浦拉司科技（上海）有限责任公司 一种电子级没食子酸辛酯的制备方法

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB634411A (en) * 1946-07-16 1950-03-22 Unilever Ltd Method of treating low-grade fatty stock to form alkyl esters therefrom
WO2002006205A1 (fr) * 2000-07-19 2002-01-24 Laboratoires Expanscience Procede de preparation d'un ester de corps gras et son utilisation dans les domaines pharmaceutique, cosmetique ou alimentaire
US6440057B1 (en) * 1997-11-24 2002-08-27 Energea Umwelttechnologie Gmbh Method for producing fatty acid methyl ester and equipment for realizing the same
DE10164274A1 (de) * 2001-12-27 2003-07-17 Energietechnik Leipzig Gmbh Verfahren und Vorrichtung zur kontinuierlichen Extraktion freier Fettsäuren und spezieller Inhaltsstoffe aus nativen Ölen und zur Umesterung nativer Öle
EP1616853A1 (de) * 2004-07-12 2006-01-18 Institut Français du Pétrole Verfahren zur Herstellung von Fettsäurealkylestern und Glycerin von hoher Reinheit
WO2006050925A1 (en) * 2004-11-11 2006-05-18 Aser S.R.L. Process for producing esters from vegetable oils or animal fats using heterogeneous catalysts
WO2006089429A1 (en) * 2005-02-28 2006-08-31 University Of Ottawa Apparatus and method for bio-fuel production
WO2006133437A1 (en) * 2005-06-09 2006-12-14 Biosphere Environmental Energy Llc Systems and methods for esterification and transesterification of fats and oils
WO2007083213A2 (en) * 2006-01-19 2007-07-26 Merloni Progetti S.P.A. Process for the preparation of biodiesel

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0454719B1 (de) * 1989-01-17 1996-06-05 Davy Process Technology Limited Kontinuierliches Verfahren zur Herstellung von Carbonsäureestern
FR2752242B1 (fr) * 1996-08-08 1998-10-16 Inst Francais Du Petrole Procede de fabrication d'esters a partir d'huiles vegetales ou animales et d'alcools
ATE481166T1 (de) * 2001-03-30 2010-10-15 Revo Internat Inc Verfahren zur herstellung von fettsäurealkylester unter verwendung eines verbundmetalloxidkatalysators
JP4997681B2 (ja) * 2001-09-28 2012-08-08 住友化学株式会社 脂肪酸エステルの製造方法および製造装置
ES2229948B1 (es) * 2003-10-14 2006-07-01 Universidad Politecnica De Valencia Preparacion de monoesteres de acidos grasos.
US7563915B2 (en) * 2006-05-30 2009-07-21 The Penn State Research Foundation Green biodiesel
WO2008013551A1 (en) * 2006-07-23 2008-01-31 Iowa State University Research Foundation, Inc. New composite-based catalysts for biodiesel production

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB634411A (en) * 1946-07-16 1950-03-22 Unilever Ltd Method of treating low-grade fatty stock to form alkyl esters therefrom
US6440057B1 (en) * 1997-11-24 2002-08-27 Energea Umwelttechnologie Gmbh Method for producing fatty acid methyl ester and equipment for realizing the same
WO2002006205A1 (fr) * 2000-07-19 2002-01-24 Laboratoires Expanscience Procede de preparation d'un ester de corps gras et son utilisation dans les domaines pharmaceutique, cosmetique ou alimentaire
DE10164274A1 (de) * 2001-12-27 2003-07-17 Energietechnik Leipzig Gmbh Verfahren und Vorrichtung zur kontinuierlichen Extraktion freier Fettsäuren und spezieller Inhaltsstoffe aus nativen Ölen und zur Umesterung nativer Öle
EP1616853A1 (de) * 2004-07-12 2006-01-18 Institut Français du Pétrole Verfahren zur Herstellung von Fettsäurealkylestern und Glycerin von hoher Reinheit
WO2006050925A1 (en) * 2004-11-11 2006-05-18 Aser S.R.L. Process for producing esters from vegetable oils or animal fats using heterogeneous catalysts
WO2006089429A1 (en) * 2005-02-28 2006-08-31 University Of Ottawa Apparatus and method for bio-fuel production
WO2006133437A1 (en) * 2005-06-09 2006-12-14 Biosphere Environmental Energy Llc Systems and methods for esterification and transesterification of fats and oils
WO2007083213A2 (en) * 2006-01-19 2007-07-26 Merloni Progetti S.P.A. Process for the preparation of biodiesel

Also Published As

Publication number Publication date
BRPI0821347A2 (pt) 2015-06-16
EP2225353A2 (de) 2010-09-08
UY31523A1 (es) 2009-08-03
CA2709575A1 (en) 2009-06-25
PE20091660A1 (es) 2009-11-15
MX2010005939A (es) 2010-08-02
ECSP10010215A (es) 2010-07-30
AR071265A1 (es) 2010-06-09
CN101903509A (zh) 2010-12-01
CL2008003689A1 (es) 2009-10-23
RU2010129470A (ru) 2012-01-27
US20100298586A1 (en) 2010-11-25
CO6280548A2 (es) 2011-05-20
TW200942513A (en) 2009-10-16
AU2008337840A1 (en) 2009-06-25
WO2009077161A2 (de) 2009-06-25
PH12010501172A1 (en) 2009-06-25

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