WO2009028514A1 - ペンタフルオロスルファニルベンゼン化合物の製造方法、及び新規なペンタフルオロスルファニルベンゼン化合物 - Google Patents

ペンタフルオロスルファニルベンゼン化合物の製造方法、及び新規なペンタフルオロスルファニルベンゼン化合物 Download PDF

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WO2009028514A1
WO2009028514A1 PCT/JP2008/065218 JP2008065218W WO2009028514A1 WO 2009028514 A1 WO2009028514 A1 WO 2009028514A1 JP 2008065218 W JP2008065218 W JP 2008065218W WO 2009028514 A1 WO2009028514 A1 WO 2009028514A1
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pentafluorosulfanylbenzene compound
group
formula
novel
producing
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PCT/JP2008/065218
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English (en)
French (fr)
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Shigeyoshi Nishino
Hidetaka Shima
Yoji Omata
Hiroyuki Oda
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Ube Industries, Ltd.
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Priority to JP2009530133A priority Critical patent/JP5418226B2/ja
Publication of WO2009028514A1 publication Critical patent/WO2009028514A1/ja

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    • C—CHEMISTRY; METALLURGY
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    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/10—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings
    • C09K19/20—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a chain containing carbon and oxygen atoms as chain links, e.g. esters or ethers
    • C09K19/2007—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a chain containing carbon and oxygen atoms as chain links, e.g. esters or ethers the chain containing -COO- or -OCO- groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C381/00—Compounds containing carbon and sulfur and having functional groups not covered by groups C07C301/00 - C07C337/00
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    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/10—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings
    • C09K19/14—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a carbon chain
    • C09K19/16—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a carbon chain the chain containing carbon-to-carbon double bonds, e.g. stilbenes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/10—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings
    • C09K19/20—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a chain containing carbon and oxygen atoms as chain links, e.g. esters or ethers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/10—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings
    • C09K19/22—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing at least two benzene rings linked by a chain containing carbon and nitrogen atoms as chain links, e.g. Schiff bases
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    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/30—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing saturated or unsaturated non-aromatic rings, e.g. cyclohexane rings
    • C09K19/3001—Cyclohexane rings
    • C09K19/3048—Cyclohexane rings in which at least two rings are linked by a carbon chain containing carbon to carbon double bonds
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    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/30—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing saturated or unsaturated non-aromatic rings, e.g. cyclohexane rings
    • C09K19/3001—Cyclohexane rings
    • C09K19/3059—Cyclohexane rings in which at least two rings are linked by a carbon chain containing carbon to carbon triple bonds
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    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/30—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing saturated or unsaturated non-aromatic rings, e.g. cyclohexane rings
    • C09K19/3001—Cyclohexane rings
    • C09K19/3066—Cyclohexane rings in which the rings are linked by a chain containing carbon and oxygen atoms, e.g. esters or ethers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/06—Non-steroidal liquid crystal compounds
    • C09K19/08—Non-steroidal liquid crystal compounds containing at least two non-condensed rings
    • C09K19/30—Non-steroidal liquid crystal compounds containing at least two non-condensed rings containing saturated or unsaturated non-aromatic rings, e.g. cyclohexane rings
    • C09K19/3001—Cyclohexane rings
    • C09K19/3066—Cyclohexane rings in which the rings are linked by a chain containing carbon and oxygen atoms, e.g. esters or ethers
    • C09K19/3068—Cyclohexane rings in which the rings are linked by a chain containing carbon and oxygen atoms, e.g. esters or ethers chain containing -COO- or -OCO- groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Liquid Crystal Substances (AREA)

Abstract

　式（１）で表されるペンタフルオロスルファニルベンゼン化合物と、Ｒ1ＯＨ、Ｒ1ＣＯＯＨ、Ｒ1ＨＣ＝ＣＨ2、Ｒ1Ｘ、Ｒ1Ｃ≡ＣＨ等（Ｒ1はアルキル基、シクロアルキル基、アラルキル基、アリール基等を示す）から選ばれる１種以上とを反応させる、式（３）で表されるペンタフルオロスルファニルベンゼン化合物の工業的に有利な製造方法、及び新規なペンタフルオロスルファニルベンゼン化合物である。 （式中、Ａは、ハロゲン原子、－ＯＨ、－ＣＯＯＨ、－ＨＣ＝ＣＨ2、－ＣＨ2Ｘ（Ｘは脱離性基）、－ＢＹ2（Ｙはヒドロキシ基等）等を示す。） （式中、Ｚは、－Ｏ－、－ＯＣＨ2－、－ＣＨ2Ｏ－、－ＣＯＯ－、－ＯＣＯ－、－ＨＣ＝ＣＨ－、－Ｃ≡Ｃ－等の連結基を示し、ｎは０又は１である。）
PCT/JP2008/065218 2007-08-28 2008-08-26 ペンタフルオロスルファニルベンゼン化合物の製造方法、及び新規なペンタフルオロスルファニルベンゼン化合物 WO2009028514A1 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2009530133A JP5418226B2 (ja) 2007-08-28 2008-08-26 ペンタフルオロスルファニルベンゼン化合物の製造方法、及び新規なペンタフルオロスルファニルベンゼン化合物

Applications Claiming Priority (14)

Application Number Priority Date Filing Date Title
JP2007-221052 2007-08-28
JP2007221052 2007-08-28
JP2007233614 2007-09-10
JP2007-233614 2007-09-10
JP2007-263359 2007-10-09
JP2007263359 2007-10-09
JP2007-298237 2007-11-16
JP2007298237 2007-11-16
JP2007-328307 2007-12-20
JP2007328307 2007-12-20
JP2007331361 2007-12-25
JP2007-331361 2007-12-25
JP2008-073331 2008-03-21
JP2008073331 2008-03-21

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010024142A (ja) * 2008-07-15 2010-02-04 Ube Ind Ltd （アリーロイル又はヘテロアリーロイル）メチルペンタフルオロスルファニルベンゼン化合物の製造方法
CZ303004B6 (cs) * 2010-10-07 2012-02-15 Ústav organické chemie a biochemie Akademie ved CR v.v.i. Zpusob prípravy substituovaných 3- a 4-(pentafluorsulfanyl)benzenu
CN106414402A (zh) * 2013-11-01 2017-02-15 宇部兴产株式会社 丙烯酰(氧基或氨基)五氟硫烷基苯化合物、其药学可接受的盐及其前药
JP2017214311A (ja) * 2016-05-31 2017-12-07 三菱ケミカル株式会社 カップリング化合物の製造方法
CN111454186A (zh) * 2019-01-18 2020-07-28 山东省联合农药工业有限公司 一种含五氟硫基的芳基甲酰苯胺类化合物及其制备方法与用途
JP2021066737A (ja) * 2021-01-19 2021-04-30 三菱ケミカル株式会社 カップリング化合物の製造方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03501247A (ja) * 1987-06-27 1991-03-22 メルク・パテント・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング アリール‐五フツ化硫黄化合物
DE19748109A1 (de) * 1997-10-31 1999-05-06 Merck Patent Gmbh Schwefelpentafluorid-Derivate und flüssigkristallines Medium
DE10151491A1 (de) * 2000-11-03 2002-05-08 Merck Patent Gmbh Flüssigkristallines Medium mit niedriger Rotationsviskosität
JP2002212163A (ja) * 2001-01-24 2002-07-31 Seimi Chem Co Ltd 五フッ化硫黄化合物及び該化合物を含有する液晶組成物
WO2005095388A1 (en) * 2004-03-05 2005-10-13 F. Hoffmann-La Roche Ag Pentafluorosulfanyl compounds, their manufacture and use as pharmaceutical agents

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS58177939A (ja) * 1982-04-13 1983-10-18 Chisso Corp ４−α，α，α−トリフルオロメチル安息香酸トランス−４−（トランス−４′−アルキルシクロヘキシル）シクロヘキシルエステル
JP4668431B2 (ja) * 2001-02-08 2011-04-13 Ａｇｃセイミケミカル株式会社 光学活性化合物、それを含有する液晶組成物および液晶素子
CN1148434C (zh) * 2001-04-26 2004-05-05 李文惠 一种液晶化合物的制备方法
DE10222192A1 (de) * 2002-05-18 2003-11-27 Aventis Pharma Gmbh Pentafluorsulfuranyl-benzoylguanidine, Verfahren zu ihrer Herstellung, ihre Verwendung als Medikament oder Diagnostikum sowie sie enthaltendes Medikament
DE10338554A1 (de) * 2003-08-22 2005-03-31 Aventis Pharma Deutschland Gmbh Pentafluorosulfanylphenyl-substituierte Benzoylguanidine, Verfahren zu ihrer Herstellung, ihre Verwendung als Medikament oder Diagnostikum sowie sie enthaltendes Medikament
GB2415193A (en) * 2004-06-19 2005-12-21 F2 Chemicals Ltd Fluorinated arylboronic acids
DE102004043937A1 (de) * 2004-09-11 2006-03-30 Sanofi-Aventis Deutschland Gmbh Ortho-substituierte Pentafluorsulfuranyl-Benzole, Verfahren zu ihrer Herstellung sowie ihre Verwendung als Synthese-Zwischenstufen

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03501247A (ja) * 1987-06-27 1991-03-22 メルク・パテント・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング アリール‐五フツ化硫黄化合物
DE19748109A1 (de) * 1997-10-31 1999-05-06 Merck Patent Gmbh Schwefelpentafluorid-Derivate und flüssigkristallines Medium
DE10151491A1 (de) * 2000-11-03 2002-05-08 Merck Patent Gmbh Flüssigkristallines Medium mit niedriger Rotationsviskosität
JP2002212163A (ja) * 2001-01-24 2002-07-31 Seimi Chem Co Ltd 五フッ化硫黄化合物及び該化合物を含有する液晶組成物
WO2005095388A1 (en) * 2004-03-05 2005-10-13 F. Hoffmann-La Roche Ag Pentafluorosulfanyl compounds, their manufacture and use as pharmaceutical agents

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010024142A (ja) * 2008-07-15 2010-02-04 Ube Ind Ltd （アリーロイル又はヘテロアリーロイル）メチルペンタフルオロスルファニルベンゼン化合物の製造方法
CZ303004B6 (cs) * 2010-10-07 2012-02-15 Ústav organické chemie a biochemie Akademie ved CR v.v.i. Zpusob prípravy substituovaných 3- a 4-(pentafluorsulfanyl)benzenu
WO2012045290A1 (en) * 2010-10-07 2012-04-12 ÚSTAV ORGANICKÉ CHEMIE A BIOCHEMIE AKADEMIE VĚD ČESKÉ REPUBLIKY, v.v.i. Process for the preparation of 3- and 4-(pentafluorosulfanyl)benzenes
CN106414402A (zh) * 2013-11-01 2017-02-15 宇部兴产株式会社 丙烯酰(氧基或氨基)五氟硫烷基苯化合物、其药学可接受的盐及其前药
JPWO2015064764A1 (ja) * 2013-11-01 2017-03-09 宇部興産株式会社 アリーロイル（オキシ又はアミノ）ペンタフルオロスルファニルベンゼン化合物、薬学的に許容されるその塩、及びそのプロドラッグ
EP3064489A4 (en) * 2013-11-01 2017-06-21 Ube Industries, Ltd. Aryloyl(oxy or amino)pentafluorosulfanylbenzene compound, pharmaceutically acceptable salt thereof, and prodrugs thereof
JP2017214311A (ja) * 2016-05-31 2017-12-07 三菱ケミカル株式会社 カップリング化合物の製造方法
JP7209454B2 (ja) 2016-05-31 2023-01-20 三菱ケミカル株式会社 カップリング化合物の製造方法
CN111454186A (zh) * 2019-01-18 2020-07-28 山东省联合农药工业有限公司 一种含五氟硫基的芳基甲酰苯胺类化合物及其制备方法与用途
CN111454186B (zh) * 2019-01-18 2022-11-08 山东省联合农药工业有限公司 一种含五氟硫基的芳基甲酰苯胺类化合物及其制备方法与用途
JP2021066737A (ja) * 2021-01-19 2021-04-30 三菱ケミカル株式会社 カップリング化合物の製造方法
JP7081698B2 (ja) 2021-01-19 2022-06-07 三菱ケミカル株式会社 カップリング化合物の製造方法

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JP5418226B2 (ja) 2014-02-19
TW200927888A (en) 2009-07-01

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