WO2008153011A1 - 燃料電池システムとその起動方法 - Google Patents

燃料電池システムとその起動方法 Download PDF

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Publication number
WO2008153011A1
WO2008153011A1 PCT/JP2008/060578 JP2008060578W WO2008153011A1 WO 2008153011 A1 WO2008153011 A1 WO 2008153011A1 JP 2008060578 W JP2008060578 W JP 2008060578W WO 2008153011 A1 WO2008153011 A1 WO 2008153011A1
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WO
WIPO (PCT)
Prior art keywords
fuel
reforming
flow
catalyst layer
temperature
Prior art date
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PCT/JP2008/060578
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English (en)
French (fr)
Inventor
Susumu Hatada
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Nippon Oil Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Oil Corporation filed Critical Nippon Oil Corporation
Priority to CN2008800198710A priority Critical patent/CN101682063B/zh
Priority to US12/664,422 priority patent/US20100173208A1/en
Priority to KR1020107000672A priority patent/KR101465830B1/ko
Priority to EP08765368A priority patent/EP2173000A4/en
Priority to CA002689674A priority patent/CA2689674A1/en
Publication of WO2008153011A1 publication Critical patent/WO2008153011A1/ja

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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/04—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids
    • H01M8/04298—Processes for controlling fuel cells or fuel cell systems
    • H01M8/04313—Processes for controlling fuel cells or fuel cell systems characterised by the detection or assessment of variables; characterised by the detection or assessment of failure or abnormal function
    • H01M8/0432—Temperature; Ambient temperature
    • H01M8/04373—Temperature; Ambient temperature of auxiliary devices, e.g. reformers, compressors, burners
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/382—Multi-step processes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/04—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids
    • H01M8/04007—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids related to heat exchange
    • H01M8/04014—Heat exchange using gaseous fluids; Heat exchange by combustion of reactants
    • H01M8/04022—Heating by combustion
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/04—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids
    • H01M8/04223—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids during start-up or shut-down; Depolarisation or activation, e.g. purging; Means for short-circuiting defective fuel cells
    • H01M8/04225—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids during start-up or shut-down; Depolarisation or activation, e.g. purging; Means for short-circuiting defective fuel cells during start-up
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/04—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids
    • H01M8/04223—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids during start-up or shut-down; Depolarisation or activation, e.g. purging; Means for short-circuiting defective fuel cells
    • H01M8/04268—Heating of fuel cells during the start-up of the fuel cells
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/04—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids
    • H01M8/04298—Processes for controlling fuel cells or fuel cell systems
    • H01M8/043—Processes for controlling fuel cells or fuel cell systems applied during specific periods
    • H01M8/04302—Processes for controlling fuel cells or fuel cell systems applied during specific periods applied during start-up
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/04—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids
    • H01M8/04298—Processes for controlling fuel cells or fuel cell systems
    • H01M8/04313—Processes for controlling fuel cells or fuel cell systems characterised by the detection or assessment of variables; characterised by the detection or assessment of failure or abnormal function
    • H01M8/0438—Pressure; Ambient pressure; Flow
    • H01M8/04425—Pressure; Ambient pressure; Flow at auxiliary devices, e.g. reformers, compressors, burners
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/04—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids
    • H01M8/04298—Processes for controlling fuel cells or fuel cell systems
    • H01M8/04694—Processes for controlling fuel cells or fuel cell systems characterised by variables to be controlled
    • H01M8/04701—Temperature
    • H01M8/04738—Temperature of auxiliary devices, e.g. reformer, compressor, burner
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/04—Auxiliary arrangements, e.g. for control of pressure or for circulation of fluids
    • H01M8/04298—Processes for controlling fuel cells or fuel cell systems
    • H01M8/04694—Processes for controlling fuel cells or fuel cell systems characterised by variables to be controlled
    • H01M8/04746—Pressure; Flow
    • H01M8/04776—Pressure; Flow at auxiliary devices, e.g. reformer, compressor, burner
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/06—Combination of fuel cells with means for production of reactants or for treatment of residues
    • H01M8/0606—Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants
    • H01M8/0612—Combination of fuel cells with means for production of reactants or for treatment of residues with means for production of gaseous reactants from carbon-containing material
    • H01M8/0618—Reforming processes, e.g. autothermal, partial oxidation or steam reforming
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/24—Grouping of fuel cells, e.g. stacking of fuel cells
    • H01M8/241—Grouping of fuel cells, e.g. stacking of fuel cells with solid or matrix-supported electrolytes
    • H01M8/2425—High-temperature cells with solid electrolytes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0244—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being an autothermal reforming step, e.g. secondary reforming processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06—Integration with other chemical processes
    • C01B2203/066—Integration with other chemical processes with fuel cells
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/08—Methods of heating or cooling
    • C01B2203/0805—Methods of heating the process for making hydrogen or synthesis gas
    • C01B2203/085—Methods of heating the process for making hydrogen or synthesis gas by electric heating
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12—Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1288—Evaporation of one or more of the different feed components
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/16—Controlling the process
    • C01B2203/1604—Starting up the process
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/16—Controlling the process
    • C01B2203/1614—Controlling the temperature
    • C01B2203/1619—Measuring the temperature
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/10—Fuel cells with solid electrolytes
    • H01M8/12—Fuel cells with solid electrolytes operating at high temperature, e.g. with stabilised ZrO2 electrolyte
    • H01M2008/1293—Fuel cells with solid oxide electrolytes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/50—Fuel cells
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Sustainable Energy (AREA)
  • Sustainable Development (AREA)
  • Manufacturing & Machinery (AREA)
  • Electrochemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Fuel Cell (AREA)
  • Hydrogen, Water And Hydrids (AREA)

Abstract

　燃料電池システムを起動する方法において早期から確実に改質を行いアノード酸化劣化をより確実に防止する。炭化水素系燃料を改質して水素含有ガスを製造する改質触媒層を有する改質器と前記ガスを用いて発電を行う高温型燃料電池とを有する燃料電池システムの起動方法であって、ａ）起動完了時の燃料流量より少ない流量の燃料を改質可能な触媒層の温度条件と起動完了時の流量の燃料を改質可能な触媒層の温度条件とを予め知り、ｂ）触媒層温度を測定しつつ触媒層を昇温し、ｃ）触媒層の測定温度を前記温度条件のうちの少なくとも一つと比較して前記測定を行った時点で改質可能な燃料流量を判定し、ｄ）判定された流量が燃料流量の現在値を超えた場合に判定された流量の燃料を触媒層に供給して改質し改質ガスを燃料電池アノードに供給し、燃料の触媒層への供給量が起動完了時の流量になるまで工程ｃ及びｄを繰り返す。この方法に好適な燃料電池システム。
PCT/JP2008/060578 2007-06-13 2008-06-10 燃料電池システムとその起動方法 WO2008153011A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
CN2008800198710A CN101682063B (zh) 2007-06-13 2008-06-10 燃料电池系统和其起动方法
US12/664,422 US20100173208A1 (en) 2007-06-13 2008-06-10 Fuel cell system and method for starting up the same
KR1020107000672A KR101465830B1 (ko) 2007-06-13 2008-06-10 연료 전지 시스템과 그 기동 방법
EP08765368A EP2173000A4 (en) 2007-06-13 2008-06-10 FUEL CELL SYSTEM AND METHOD OF ACTIVATION THEREOF
CA002689674A CA2689674A1 (en) 2007-06-13 2008-06-10 Fuel cell system and method for starting up the same

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-156438 2007-06-13
JP2007156438A JP5164441B2 (ja) 2007-06-13 2007-06-13 燃料電池システムの起動方法

Publications (1)

Publication Number Publication Date
WO2008153011A1 true WO2008153011A1 (ja) 2008-12-18

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PCT/JP2008/060578 WO2008153011A1 (ja) 2007-06-13 2008-06-10 燃料電池システムとその起動方法

Country Status (8)

Country Link
US (1) US20100173208A1 (ja)
EP (1) EP2173000A4 (ja)
JP (1) JP5164441B2 (ja)
KR (1) KR101465830B1 (ja)
CN (1) CN101682063B (ja)
CA (1) CA2689674A1 (ja)
TW (1) TWI437757B (ja)
WO (1) WO2008153011A1 (ja)

Cited By (3)

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Publication number Priority date Publication date Assignee Title
EP2199255A1 (en) * 2007-08-29 2010-06-23 Nippon Oil Corporation Fuel cell system and method for starting the fuel cell system
JP2010205647A (ja) * 2009-03-05 2010-09-16 Nissan Motor Co Ltd 燃料電池システム
JP4868268B1 (ja) * 2011-01-05 2012-02-01 Ｔｏｔｏ株式会社 固体酸化物型燃料電池

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JP5078696B2 (ja) 2008-03-27 2012-11-21 Ｊｘ日鉱日石エネルギー株式会社 燃料電池システムの負荷追従運転方法
US8409760B2 (en) * 2009-01-20 2013-04-02 Adaptive Materials, Inc. Method for controlling a water based fuel reformer
US8936888B2 (en) * 2009-01-30 2015-01-20 Adaptive Materials, Inc. Fuel cell system with flame protection member
CA2758153A1 (en) * 2009-04-08 2010-10-14 Susumu Hatada Shutdown method for shutting down indirect internal reforming solid oxide fuel cell
JP5500504B2 (ja) * 2009-05-28 2014-05-21 Ｔｏｔｏ株式会社 固体電解質型燃料電池
JP4748465B2 (ja) * 2009-05-28 2011-08-17 Ｔｏｔｏ株式会社 燃料電池装置
JP4761259B2 (ja) * 2009-05-28 2011-08-31 Ｔｏｔｏ株式会社 固体電解質型燃料電池
JP5433323B2 (ja) * 2009-07-02 2014-03-05 Ｊｘ日鉱日石エネルギー株式会社 燃料電池システムの負荷追従運転方法
JP5281998B2 (ja) * 2009-09-24 2013-09-04 Ｊｘ日鉱日石エネルギー株式会社 燃料電池システムの負荷追従運転方法
WO2011024899A1 (ja) * 2009-08-27 2011-03-03 Ｊｘ日鉱日石エネルギー株式会社 燃料電池システムの負荷追従運転方法
JP5281991B2 (ja) * 2009-08-27 2013-09-04 Ｊｘ日鉱日石エネルギー株式会社 燃料電池システムの負荷追従運転方法
JP5281997B2 (ja) * 2009-09-24 2013-09-04 Ｊｘ日鉱日石エネルギー株式会社 燃料電池システムの負荷追従運転方法
JP5281996B2 (ja) * 2009-09-24 2013-09-04 Ｊｘ日鉱日石エネルギー株式会社 燃料電池システムの負荷追従運転方法
US20110189578A1 (en) * 2010-02-01 2011-08-04 Adaptive Materials, Inc. Fuel cell system including a resilient manifold interconnecting member
US8796888B2 (en) 2010-07-07 2014-08-05 Adaptive Materials, Inc. Wearable power management system
TWI573288B (zh) * 2010-10-18 2017-03-01 鴻海精密工業股份有限公司 發光二極體及其製作方法
US9162203B1 (en) * 2011-03-16 2015-10-20 Kabushiki Kaisha Toyota Chuo Kenkyusho Hydrogen generator
JP5731357B2 (ja) * 2011-11-09 2015-06-10 Ｊｘ日鉱日石エネルギー株式会社 固体酸化物形燃料電池システム及びその起動制御方法
WO2013069633A1 (ja) * 2011-11-09 2013-05-16 Ｊｘ日鉱日石エネルギー株式会社 固体酸化物形燃料電池システム及びその起動制御方法

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JP2002201002A (ja) * 2000-12-27 2002-07-16 Toyota Motor Corp 改質器の起動制御
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JP2005158466A (ja) * 2003-11-25 2005-06-16 Matsushita Electric Works Ltd 燃料電池発電システム
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JP2006190605A (ja) 2005-01-07 2006-07-20 Nippon Oil Corp 固体電解質形燃料電池システムの起動方法

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2199255A1 (en) * 2007-08-29 2010-06-23 Nippon Oil Corporation Fuel cell system and method for starting the fuel cell system
EP2199255A4 (en) * 2007-08-29 2013-09-11 Nippon Oil Corp FUEL CELL SYSTEM AND METHOD FOR STARTING UP THE FUEL CELL SYSTEM
US8574775B2 (en) 2007-08-29 2013-11-05 Nippon Oil Corporation Fuel cell system and method for starting up the same
JP2010205647A (ja) * 2009-03-05 2010-09-16 Nissan Motor Co Ltd 燃料電池システム
JP4868268B1 (ja) * 2011-01-05 2012-02-01 Ｔｏｔｏ株式会社 固体酸化物型燃料電池

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US20100173208A1 (en) 2010-07-08
KR20100034746A (ko) 2010-04-01
EP2173000A1 (en) 2010-04-07
TWI437757B (zh) 2014-05-11
JP5164441B2 (ja) 2013-03-21
KR101465830B1 (ko) 2014-11-26
CN101682063B (zh) 2013-07-31
EP2173000A4 (en) 2012-02-22

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