WO2008078609A1 - α－スルホ脂肪酸アルキルエステル塩含有粉体の製造方法 - Google Patents

α－スルホ脂肪酸アルキルエステル塩含有粉体の製造方法 Download PDF

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Publication number
WO2008078609A1
WO2008078609A1 PCT/JP2007/074332 JP2007074332W WO2008078609A1 WO 2008078609 A1 WO2008078609 A1 WO 2008078609A1 JP 2007074332 W JP2007074332 W JP 2007074332W WO 2008078609 A1 WO2008078609 A1 WO 2008078609A1
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WO
WIPO (PCT)
Prior art keywords
condensation
fatty acid
alkyl ester
acid alkyl
ester salt
Prior art date
Application number
PCT/JP2007/074332
Other languages
English (en)
French (fr)
Inventor
Nobukazu Shogase
Kensuke Itakura
Masahiko Matsubara
Original Assignee
Lion Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lion Corporation filed Critical Lion Corporation
Priority to JP2008551044A priority Critical patent/JP5358190B2/ja
Publication of WO2008078609A1 publication Critical patent/WO2008078609A1/ja

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)

Abstract

濃縮工程での色調劣化がなく、臭気も抑制されたα－スルホ脂肪酸アルキルエステル塩含有粉体を提供する。α－スルホ脂肪酸アルキルエステル塩を含有する水性ペーストを濃縮乾燥機で加熱して、該濃縮乾燥機の出口における水分量が４質量％以下である濃縮品を調製する濃縮工程と、前記濃縮品を冷却固化装置で冷却して固化し、固形物を調製する冷却固化工程と、前記固形物を破砕造粒する造粒工程とを有するα－スルホ脂肪酸アルキルエステル塩含有粉体の製造方法であって、前記水性ペーストのｐＨを４．５～６．５に調整するとともに、前記濃縮工程では、前記濃縮乾燥機の出口における前記濃縮品の温度が９０～１４０°Cとなるように加熱する。
PCT/JP2007/074332 2006-12-25 2007-12-18 α－スルホ脂肪酸アルキルエステル塩含有粉体の製造方法 WO2008078609A1 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2008551044A JP5358190B2 (ja) 2006-12-25 2007-12-18 α−スルホ脂肪酸アルキルエステル塩含有粉体の製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2006346961 2006-12-25
JP2006-346961 2006-12-25

Publications (1)

Publication Number Publication Date
WO2008078609A1 true WO2008078609A1 (ja) 2008-07-03

Family

ID=39562402

Family Applications (1)

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PCT/JP2007/074332 WO2008078609A1 (ja) 2006-12-25 2007-12-18 α－スルホ脂肪酸アルキルエステル塩含有粉体の製造方法

Country Status (3)

Country Link
JP (1) JP5358190B2 (ja)
MY (1) MY162130A (ja)
WO (1) WO2008078609A1 (ja)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010116736A1 (ja) * 2009-04-10 2010-10-14 ライオン株式会社 α－スルホ脂肪酸アルキルエステルアルカノールアミン塩の製造方法
WO2010123060A1 (ja) * 2009-04-22 2010-10-28 ライオン株式会社 脂肪酸アルキルエステルスルホナート金属塩粉末混合物及びその製造方法
WO2015098415A1 (ja) * 2013-12-27 2015-07-02 花王株式会社 内部オレフィンスルホン酸塩の製造方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS577462A (en) * 1980-06-16 1982-01-14 Lion Corp Production of high-concentration solution of alpha-sulfofatty acid ester salt
JPH08170093A (ja) * 1994-12-16 1996-07-02 Lion Corp α−スルホ脂肪酸アルキルエステル塩粉粒体の製造方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10204479A (ja) * 1997-01-21 1998-08-04 Lion Corp 界面活性剤粉体および粒状洗剤組成物

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS577462A (en) * 1980-06-16 1982-01-14 Lion Corp Production of high-concentration solution of alpha-sulfofatty acid ester salt
JPH08170093A (ja) * 1994-12-16 1996-07-02 Lion Corp α−スルホ脂肪酸アルキルエステル塩粉粒体の製造方法

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010116736A1 (ja) * 2009-04-10 2010-10-14 ライオン株式会社 α－スルホ脂肪酸アルキルエステルアルカノールアミン塩の製造方法
JP5618988B2 (ja) * 2009-04-10 2014-11-05 ライオン株式会社 α−スルホ脂肪酸アルキルエステルアルカノールアミン塩の製造方法
WO2010123060A1 (ja) * 2009-04-22 2010-10-28 ライオン株式会社 脂肪酸アルキルエステルスルホナート金属塩粉末混合物及びその製造方法
JP5688772B2 (ja) * 2009-04-22 2015-03-25 ライオン株式会社 脂肪酸アルキルエステルスルホナート金属塩粉末混合物及びその製造方法
US9708252B2 (en) 2009-04-22 2017-07-18 Lion Corporation Fatty acid alkyl ester sulfonate metal salt powder mixture and method for producing the same
WO2015098415A1 (ja) * 2013-12-27 2015-07-02 花王株式会社 内部オレフィンスルホン酸塩の製造方法
JP2015143203A (ja) * 2013-12-27 2015-08-06 花王株式会社 内部オレフィンスルホン酸塩の製造方法
US9815779B2 (en) 2013-12-27 2017-11-14 Kao Corporation Method for producing internal olefin sulfonate

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Publication number Publication date
JPWO2008078609A1 (ja) 2010-04-22
MY162130A (en) 2017-05-31
JP5358190B2 (ja) 2013-12-04

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