WO2007022900A1 - Procede a haut rendement pour l'elaboration de thioalkylamines - Google Patents

Procede a haut rendement pour l'elaboration de thioalkylamines Download PDF

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Publication number
WO2007022900A1
WO2007022900A1 PCT/EP2006/008060 EP2006008060W WO2007022900A1 WO 2007022900 A1 WO2007022900 A1 WO 2007022900A1 EP 2006008060 W EP2006008060 W EP 2006008060W WO 2007022900 A1 WO2007022900 A1 WO 2007022900A1
Authority
WO
WIPO (PCT)
Prior art keywords
alkyl
halo
different
alkoxy
group
Prior art date
Application number
PCT/EP2006/008060
Other languages
English (en)
Inventor
Sergiy Pazenok
Original Assignee
Bayer Cropscience Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Cropscience Ag filed Critical Bayer Cropscience Ag
Priority to JP2008527349A priority Critical patent/JP2009505997A/ja
Priority to BRPI0615131-0A priority patent/BRPI0615131A2/pt
Priority to MX2008002330A priority patent/MX2008002330A/es
Priority to EP06776866A priority patent/EP1919860A1/fr
Publication of WO2007022900A1 publication Critical patent/WO2007022900A1/fr
Priority to IL189297A priority patent/IL189297A0/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/24—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfuric acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/23—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton
    • C07C323/24—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/25—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and nitrogen atoms, not being part of nitro or nitroso groups, bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated

Abstract

La présente invention concerne un procédé permettant l'élaboration de composés représentés par la formule (I). Dans un premier temps, on prend des alcools aminés représentés par la formule (II), et on les mélange à de l'acide sulfurique, ce qui donne le sel correspondant. Dans un deuxième temps, on les fait réagir dans une colonne séchante, ce qui donne les esters d'acide sulfurique représentés par la formule générale (III). Dans un troisième temps, on fait réagit ces esters avec des mercaptans ou sels de mercaptans dont le formule est 'RSM' (formule IV), en présence d'un diluant et d'une base. Dans ces formules, R1, R2, R3, R4, R5, R6, R, n et M sont tels que spécifiés dans la description.
PCT/EP2006/008060 2005-08-24 2006-08-16 Procede a haut rendement pour l'elaboration de thioalkylamines WO2007022900A1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
JP2008527349A JP2009505997A (ja) 2005-08-24 2006-08-16 高収率でのチオアルキルアミン類の調製
BRPI0615131-0A BRPI0615131A2 (pt) 2005-08-24 2006-08-16 preparação de tioalquilaminas com rendimentos elevados
MX2008002330A MX2008002330A (es) 2005-08-24 2006-08-16 Preparacion de tioalquilaminas con altos rendimientos.
EP06776866A EP1919860A1 (fr) 2005-08-24 2006-08-16 Procede a haut rendement pour l'elaboration de thioalkylamines
IL189297A IL189297A0 (en) 2005-08-24 2008-02-05 Preparation of thioalkylamines with high yields

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP05018347.4 2005-08-24
EP05018347 2005-08-24

Publications (1)

Publication Number Publication Date
WO2007022900A1 true WO2007022900A1 (fr) 2007-03-01

Family

ID=37110273

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/008060 WO2007022900A1 (fr) 2005-08-24 2006-08-16 Procede a haut rendement pour l'elaboration de thioalkylamines

Country Status (9)

Country Link
EP (1) EP1919860A1 (fr)
JP (1) JP2009505997A (fr)
KR (1) KR20080036645A (fr)
CN (1) CN101248040A (fr)
BR (1) BRPI0615131A2 (fr)
IL (1) IL189297A0 (fr)
MX (1) MX2008002330A (fr)
TW (1) TW200800868A (fr)
WO (1) WO2007022900A1 (fr)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011087837A2 (fr) 2009-12-22 2011-07-21 E. I. Du Pont De Nemours And Company 2-(aryloxy bicyclique)carboxamides fongicides
WO2012087372A1 (fr) 2010-12-22 2012-06-28 E. I. Du Pont De Nemours And Company 2-(aryloxy bicyclique)carboxamides fongicides
JP5550568B2 (ja) * 2009-01-27 2014-07-16 国立大学法人九州大学 ジチオカルバミン酸エステルの変換によるチオ化合物の製造方法
US9145354B2 (en) 2011-11-01 2015-09-29 Astex Therapeutics Limited Pharmaceutical compounds

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103664707A (zh) * 2013-12-14 2014-03-26 内蒙古河西航天科技发展有限公司 酸式硫酸-β-氨基酯及其合成方法和应用

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001023350A1 (fr) * 1999-09-28 2001-04-05 Nihon Nohyaku Co., Ltd. Derives de thioalkylamine et methode de preparation desdits derives
WO2003099777A1 (fr) * 2002-05-24 2003-12-04 Bayer Cropscience Ag Procede de preparation de derives de thioalkylamine

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001023350A1 (fr) * 1999-09-28 2001-04-05 Nihon Nohyaku Co., Ltd. Derives de thioalkylamine et methode de preparation desdits derives
EP1216988A1 (fr) * 1999-09-28 2002-06-26 Nihon Nohyaku Co., Ltd. Derives de thioalkylamine et methode de preparation desdits derives
WO2003099777A1 (fr) * 2002-05-24 2003-12-04 Bayer Cropscience Ag Procede de preparation de derives de thioalkylamine

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5550568B2 (ja) * 2009-01-27 2014-07-16 国立大学法人九州大学 ジチオカルバミン酸エステルの変換によるチオ化合物の製造方法
WO2011087837A2 (fr) 2009-12-22 2011-07-21 E. I. Du Pont De Nemours And Company 2-(aryloxy bicyclique)carboxamides fongicides
WO2012087372A1 (fr) 2010-12-22 2012-06-28 E. I. Du Pont De Nemours And Company 2-(aryloxy bicyclique)carboxamides fongicides
US9145354B2 (en) 2011-11-01 2015-09-29 Astex Therapeutics Limited Pharmaceutical compounds

Also Published As

Publication number Publication date
JP2009505997A (ja) 2009-02-12
CN101248040A (zh) 2008-08-20
TW200800868A (en) 2008-01-01
BRPI0615131A2 (pt) 2011-05-03
EP1919860A1 (fr) 2008-05-14
KR20080036645A (ko) 2008-04-28
IL189297A0 (en) 2008-06-05
MX2008002330A (es) 2008-03-18

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