WO2006125888A3 - Procede de preparation de composes organosiliciques en milieu biphasique - Google Patents

Procede de preparation de composes organosiliciques en milieu biphasique Download PDF

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Publication number
WO2006125888A3
WO2006125888A3 PCT/FR2006/001108 FR2006001108W WO2006125888A3 WO 2006125888 A3 WO2006125888 A3 WO 2006125888A3 FR 2006001108 W FR2006001108 W FR 2006001108W WO 2006125888 A3 WO2006125888 A3 WO 2006125888A3
Authority
WO
WIPO (PCT)
Prior art keywords
oxidizing
preparing
phase medium
compounds
organosilicium
Prior art date
Application number
PCT/FR2006/001108
Other languages
English (en)
Other versions
WO2006125888A2 (fr
Inventor
Sebastien Sterin
Original Assignee
Rhodia Chimie Sa
Sebastien Sterin
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhodia Chimie Sa, Sebastien Sterin filed Critical Rhodia Chimie Sa
Priority to BRPI0610465-7A priority Critical patent/BRPI0610465A2/pt
Priority to CA002609311A priority patent/CA2609311A1/fr
Priority to JP2008512862A priority patent/JP4750847B2/ja
Priority to EP06755494A priority patent/EP1888601A2/fr
Priority to CN200680018381XA priority patent/CN101184766B/zh
Priority to US11/921,010 priority patent/US20090215999A1/en
Publication of WO2006125888A2 publication Critical patent/WO2006125888A2/fr
Publication of WO2006125888A3 publication Critical patent/WO2006125888A3/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic System
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic System
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C07F7/1804—Compounds having Si-O-C linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic System
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)

Abstract

Le domaine de l'invention est celui de la synthèse de composés organosiliciques fonctionnalisés comprenant au moins un groupe azo activé, de formule (I) : [(G0)3SiO1/2]m [(G0)2SiO2/2]n [G0SiO3/2]o [SiO4/2]p [(G2)a(G1)a'(Z-CO-HN=NH-CO-A)SiO(3-a-a')/2]. Ce procédé consiste à mettre en œuvre au moins un précurseur (II) hydrazino (-HN-NH-) du composé (I), à oxyder le précurseur (II) en groupement azo propre au composé (I), à l'aide d'un système oxydant comprenant au moins un oxydant (Ox) et au moins une base (B), ce procédé étant caractérisé en ce que l'oxydation est réalisée en milieu biphasique aqueux/organique et en ce que l'on fait en sorte que le pH de la phase aqueuse soit compris entre 3 et 11, de préférence entre 5 et 9. L'invention concerne également les composés (I) stables à la chaleur susceptibles d'être obtenus par ce procédé.
PCT/FR2006/001108 2005-05-26 2006-05-17 Procede de preparation de composes organosiliciques en milieu biphasique WO2006125888A2 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
BRPI0610465-7A BRPI0610465A2 (pt) 2005-05-26 2006-05-17 processo de preparação de compostos organossilìcicos e compostos organossilìcicos suscetìveis de ser obtidos pelo processo
CA002609311A CA2609311A1 (fr) 2005-05-26 2006-05-17 Procede de preparation de composes organosiliciques en milieu biphasique
JP2008512862A JP4750847B2 (ja) 2005-05-26 2006-05-17 ２相媒体中での有機ケイ素化合物の製造方法
EP06755494A EP1888601A2 (fr) 2005-05-26 2006-05-17 Procede de preparation de composes organosiliciques en milieu biphasique
CN200680018381XA CN101184766B (zh) 2005-05-26 2006-05-17 在两相介质中制备有机硅化合物的方法
US11/921,010 US20090215999A1 (en) 2005-05-26 2006-05-17 Preparation Of Organosilicon Compounds In Two-Phase Medium

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0505285 2005-05-26
FR0505285A FR2886296B1 (fr) 2005-05-26 2005-05-26 Procede de preparation de composes organosiliciques en milieu biphasique

Publications (2)

Publication Number Publication Date
WO2006125888A2 WO2006125888A2 (fr) 2006-11-30
WO2006125888A3 true WO2006125888A3 (fr) 2007-01-25

Family

ID=35530783

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2006/001108 WO2006125888A2 (fr) 2005-05-26 2006-05-17 Procede de preparation de composes organosiliciques en milieu biphasique

Country Status (9)

Country Link
US (1) US20090215999A1 (fr)
EP (1) EP1888601A2 (fr)
JP (1) JP4750847B2 (fr)
KR (1) KR100978769B1 (fr)
CN (1) CN101184766B (fr)
BR (1) BRPI0610465A2 (fr)
CA (1) CA2609311A1 (fr)
FR (1) FR2886296B1 (fr)
WO (1) WO2006125888A2 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2886295B1 (fr) * 2005-05-26 2007-07-20 Rhodia Chimie Sa Composes organosiliciques et procede de preparation associe
FR2929614A1 (fr) * 2008-04-04 2009-10-09 Rhodia Operations Sas Procede perfectionne de preparation composes organosiliciques en milieu biphasique
DE102008002183A1 (de) * 2008-06-03 2009-12-10 Evonik Degussa Gmbh Verfahren zur Aufarbeitung salzhaltiger Rückstände aus der Herstellung von aminofunktionellen Organosilanen

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4118367A (en) * 1976-02-06 1978-10-03 The Malaysian Rubber Producers Research Association Reinforced rubber

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3931143A (en) 1967-02-15 1976-01-06 Pennwalt Corporation Unsymmetrical aliphatic monoazo compounds
US4118637A (en) * 1975-05-20 1978-10-03 Unep3 Energy Systems Inc. Integrated energy system
JPH0693134A (ja) * 1992-07-31 1994-04-05 Sumitomo Chem Co Ltd 優れたグリップ性能と転動抵抗を有するゴム組成物およびその製造方法
JPH06298719A (ja) * 1993-04-20 1994-10-25 Otsuka Chem Co Ltd カルバモイルアゾカルボン酸エステル誘導体及びその製造法
US5380828A (en) * 1993-10-05 1995-01-10 Ciba-Geigy Corporation Azodicarboxylic acid derivatives containing hindered amine moieties as polymer stabilizers
FR2826652B1 (fr) 2001-06-28 2005-09-09 Atofina Procede de preparation de composes type azoique.
JP2004339208A (ja) * 2003-04-24 2004-12-02 Ishihara Sangyo Kaisha Ltd フェニルヒドラジン誘導体又はその塩、それらの製造方法、並びにそれらを有効成分として含有する殺菌剤

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4118367A (en) * 1976-02-06 1978-10-03 The Malaysian Rubber Producers Research Association Reinforced rubber

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
DAWES, K.; ROWLEY, R.J.: "Chemical modification of natural rubber-a new silane coupling agent", PLASTICS AND RUBBER: MATERIALS AND APPLICATIONS, vol. 3, no. 1, 1978, pages 23 - 26, XP009060017 *
DAWES, K.; ROWLEY, R.J.: "chemical Modifications of Natural Rubber-A New Silane Coupling Agent", RUBBERCON '77, 1977, pages 18.1 - 18.11, XP009060018 *
MITCHELL, H.; LEBLANC, Y.: "Amination of Arenes with Electron-Deficient Azodicarboxylates", J.ORG.CHEM., vol. 59, 1994, pages 682 - 687, XP002363174 *

Also Published As

Publication number Publication date
CA2609311A1 (fr) 2006-11-30
CN101184766A (zh) 2008-05-21
FR2886296B1 (fr) 2007-07-20
EP1888601A2 (fr) 2008-02-20
CN101184766B (zh) 2012-02-15
WO2006125888A2 (fr) 2006-11-30
FR2886296A1 (fr) 2006-12-01
JP2008542245A (ja) 2008-11-27
BRPI0610465A2 (pt) 2012-10-23
US20090215999A1 (en) 2009-08-27
KR100978769B1 (ko) 2010-08-30
KR20080007384A (ko) 2008-01-18
JP4750847B2 (ja) 2011-08-17

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