WO2005082167A1 - Composition minérale et procédé d’utilisation de celle-ci - Google Patents

Composition minérale et procédé d’utilisation de celle-ci Download PDF

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Publication number
WO2005082167A1
WO2005082167A1 PCT/JP2005/003547 JP2005003547W WO2005082167A1 WO 2005082167 A1 WO2005082167 A1 WO 2005082167A1 JP 2005003547 W JP2005003547 W JP 2005003547W WO 2005082167 A1 WO2005082167 A1 WO 2005082167A1
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Prior art keywords
mineral
calcium
containing composition
diet
meal
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PCT/JP2005/003547
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English (en)
Inventor
Toshihiro Ito
Takanori Kawai
Shizuka Kogiso
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Taiyo Kagaku Co., Ltd.
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Publication of WO2005082167A1 publication Critical patent/WO2005082167A1/fr

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Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
    • A23L33/21—Addition of substantially indigestible substances, e.g. dietary fibres
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A23L27/33—Artificial sweetening agents containing sugars or derivatives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
    • A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
    • A23L29/238—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin from seeds, e.g. locust bean gum or guar gum
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/16—Inorganic salts, minerals or trace elements

Definitions

  • the present invention relates to a mineral-containing composition and a method of use thereof.
  • the disclosed composition is, however, formulated for the use of dispersing to processed foodstuff during the production, and does not take into consideration the use of dispersing at food service institutions and general households; therefore, thereby making it difficult to be used as it is in the food service institutions and the general households.
  • An object of the present invention is to provide a mineral-containing composition which little affects to the color and taste of foods, i ⁇ capable of being used in the food service institutions and the general households, and further capable of taking minerals in a given amount.
  • the present invention relates to: The present invention relates:
  • a mineral-containing composition comprising a water-soluble dietary fiber and a mineral
  • the diet is a soup, a beverage, a rice-based diet and/or a side dish;
  • the present invention provides a mineral-containing composition little affecting color and taste of foods and having excellent water-dispersibility, allowing easy use by adding to a diet which being fed by the food service institutions or taken at the general households, and further allowing an intake of a given amount of a mineral.
  • the mineral-containing composition of the present invention resides in that the mineral-containing composition comprises a water-soluble dietary fiber and a mineral. Since the mineral-containing composition has the above feature, the dispersibility in water is improved as compared with conventional mineral- containing compositions, thereby providing a mineral-containing composition which can be easily added to the diet upon food intake in the food service institutions or the general households.
  • the mineral-containing composition can be used in the food service institutions and the general households, the conventional problem of causing a difference in the amounts of mineral taken by individuals.
  • the mineral usable in the present invention includes calcium, phosphorus, sulfur, potassium, sodium, chlorine, magnesium, iron, zinc, silicon, manganese, copper, boron, molybdenum, selenium, iodine, chromium, cobalt, nickel, vanadium, arsenic, and the like.
  • calcium, magnesium and iron are preferable from the viewpoints of nutrition science, and iron is more preferable.
  • These minerals may be used alone or in a mixture of two or more kinds.
  • the mineral used in the present invention may be used in the form as it is, or preferably in the form of an inorganic or organic salt (simply referred to herein as a mineral salt in some cases).
  • the mineral salt is not particularly limited, and a mineral salt little affecting to taste is preferable.
  • the mineral salt little affecting to taste includes a soluble mineral salt such as a calcium lactate.
  • a mineral salt corresponding to the salts regulated by the test method of general notice 29 in the Seventh Edition of Japan's Specifications and Standards for Food Additives in which the mineral salt is defined as "very slightly soluble" (the amount of water required to solve 1 g of a solute is 1000 ml or more and less than 10000 ml) or "practically insoluble” (the amount of water required to solve 1 g of a solute is 10000 ml or more); more preferable is a mineral salt pertinent to "practically insoluble.”
  • the preferable mineral salt include calcium salts such as calcium pyrophosphate, calcium phosphate, and calcium carbonate, including a material containing eggshell calcium, seashell calcium, seaweed calcium, dolomite, or natural calcium carbonate; magnesium salts such as magnesium hydroxide and magnesium phosphate; iron salts such as ferrous hydroxide, ferrous phosphate, ferric pyrophosphate,
  • preferable are calcium pyrophosphate, calcium phosphate, calcium carbonate, magnesium hydroxide, magnesium phosphate, ferrous phosphate, ferric pyrophosphate, and cuprous chloride; more preferable are calcium pyrophosphate, calcium phosphate, calcium carbonate, magnesium hydroxide, magnesium phosphate, ferrous phosphate and ferric pyrophosphate; still more preferable are calcium carbonate and ferric pyrophosphate.
  • Those mineral salts may be used alone or in a mixture of two or more kinds.
  • the average particle size of the mineral salt used in the present invention is preferably 1 ⁇ m or less, more preferably 0.5 ⁇ m or less, from the viewpoints of absorbability and palatability.
  • the average particle size is determined by, for example, a laser diffraction particle size distribution analyzer.
  • the method for obtaining the mineral salt having the average particle size includes a physical powdering method employing a homomixer, a ball-mill, a jet mill or the like, or a method of neutral salt formation. Among them, the method of neutral salt formation is preferable because fine particles having even particle sizes can be easily obtained.
  • the method of neutral salt formation refers to a method for obtaining a salt by reacting an acid with a base.
  • the method of neutral salt formation known are a method employing neutralization reaction between a strong acid and a strong basic salt such as ferric chloride and tetrasodium pyrophosphate in the case of ferric pyrophosphate, a method employing neutralization reaction between a weak acid and a strong basic salt, for instance, a carbonate such as calcium carbonate and calcium hydroxide or the like.
  • the content of the mineral in the mineral-containing composition of the present invention is not particularly limited, as long as the mineral is contained in a desired amount in the mineral-containing composition.
  • the content of the mineral in the mineral-containing composition is preferably from 0.1 to 100 mg/g, more preferably from 1 to 50 mg/g.
  • the water-soluble dietary fiber used for the present invention includes, for example, pectin, sodium alginate, a part of hemicellulose, glucomannan, galactomannan, and partial decomposition products thereof. Among them, the decomposition product of the galactomannan is preferable.
  • the galactomannan in the present invention means a polysaccharide in which a sugar chain comprising mannose as a main component thereof is bound to a side chain comprising a galactose as a main component thereof.
  • Specific examples of the galactomannan include guar gum, locust bean gum, tara gum, and the like, preferably guar gum or locust bean gum.
  • the decomposition product of the galactomannan in the present invention can be obtained by mixing one or more kinds of the galactomannan mentioned above, followed by decomposition. Alternatively, the decomposition product can be obtained by decomposing them, followed by mixing the decomposed.
  • the method for decomposing the galactomannan is not particularly limited. The method includes an enzymolysis method, an acidolysis method and the like; preferably is an enzymolysis method due to capability of obtaining a product having a given quality.
  • An enzyme used for the enzymolysis method may be a commercial product or a natural product as long as being capable to hydrolyze the sugar chain including a mannose as the major component; preferably ⁇ -galactomannanase derived from Aspergillus strains or Rhizopus strains, more preferably ⁇ -galactomannanase derived from Aspergillus strains.
  • One or more kinds of the enzymes may be used for the decomposition.
  • the viscosity of a 1% by weight solution of the decomposed galactomannan product obtained in the manner described above is preferably 10 mPa's or less at 25°C.
  • the weight-average molecular weight of the decomposed galactomannan product is preferably from 2000 to 100000.
  • the above-mentioned viscosity can be measured by a B-type viscometer for a 1% by weight aqueous solution of the decomposed galactomannan product.
  • the weight-average molecular weight can be measured by a method of calculating from the molecular distribution determined by high-performance liquid chromatography (column: YMC-Pack Diol-120, manufactured by YMC) using a polyethylene glycol (molecular weight : 2000, 20000, 100000 and the like) as markers.
  • YMC-Pack Diol-120 manufactured by YMC
  • polyethylene glycol molecular weight : 2000, 20000, 100000 and the like
  • the above-mentioned water-soluble dietary fiber there may be used a commercial product, for example, such as SUNFIBER (decomposed galactomannan product) manufactured by Taiyo Kagaku Co., Ltd.
  • the content of the water-soluble dietary fiber in the mineral-containing composition of the present invention is preferably from 0.1 to 5% by weight, more preferably from 0.3 to 1% by weight, from the viewpoints of improving dispersibility, suppressing increase of viscosity and securing excellent palatability.
  • the mineral used in the present invention is preferably coated with an emulsifying agent from the viewpoints of absorbability to body and processing applicability to foodstuff.
  • the state of coating with the emulsifying agent means a state of emulsification with an emulsifying agent, and the state can be confirmed whether or not the mineral is stably dispersed in water.
  • the emulsifying agent used for the emulsification is not particularly limited, as long as the emulsifying agent is able to coat the mineral.
  • the emulsifying agent includes a glycerol fatty acid ester, a propylene glycol fatty acid ester, a sorbitan fatty acid ester, a pentaerythritol fatty acid ester, a sorbitol fatty acid ester, a polyglycerol fatty acid ester, a sucrose fatty acid ester, a fatty acid ester of an organic acid, lecithin, an enzymatically decomposed lecithin, and the like.
  • an enzymatically decomposed lecithin a polyglycerol fatty acid ester and a sucrose fatty acid ester.
  • These emulsifying agents can be used alone or in a mixture of two or more kinds.
  • the enzymatically decomposed lecithin in the present specification refers to those obtained by subjecting lecithin to hydrolysis with phospholipase or the like.
  • the lecithin includes a plant-derived lecithin such as soybean or an animal- derived lecithin such as an egg yolk.
  • the phospholipase may be a phospholipase having phospholipase A and/or D activity, regardless of whether the origin may be derived from animals such as a pig pancreas, plants such as a cabbage or bacteria such as fungi; preferably phospholipase A which hydrolyzes a primary or secondary position of the fatty acid ester bonding, more preferably phospholipase A2 which hydrolyzes secondary position of the diacyl glycerophospholipid.
  • the enzymatically decomposed lecithin may use a commercial product, for example, such as SUNLECIT ⁇ IN L manufactured by Taiyo Kagaku Co., Ltd.
  • the polyglycerol fatty acid ester in the present invention means an ester formed between a polyglycerol and a fatty acid.
  • the average degree of polymerization of the polyglycerol, the kind of the fatty acid and an esterification ratio, which constitute the polyglycerol fatty acid ester are not particularly limited.
  • the average degree of polymerization of the polyglycerol is preferably 3 or more, more preferably from 3 to 11.
  • the fatty acid preferably has a hydroxyl group in a saturated or unsaturated, straight or branched chain having 6 to 22 carbon atoms, more preferably 8 to 18 carbon atoms, even more preferably 12 to 14 carbon atoms.
  • the sucrose fatty acid ester of the present invention refers to an ester formed between a sucrose and a fatty acid.
  • the fatty acid constituting the sucrose fatty acid ester is not particularly limited.
  • the fatty acid preferably has an HLB of 10 or more, more preferably 12 or more, wherein the HLB is calculated from a molecular weight ratio of a hydrophilic group and a lipophilic group.
  • the fatty acid has a hydroxyl group in a saturated or unsaturated, straight or branched chain having 8 to 22 carbon atoms, more preferably 10 to 20 carbon atoms, even more preferably 14 to 18 carbon atoms.
  • sucrose fatty acid ester there may be used a commercial product, for example, such as SUNSOFT SE-14, SUNSOFT SE-16, or SUNSOFT SE-16P manufactured by Taiyo Kagaku Co., Ltd.
  • the method of coating the mineral with the emulsifying agent includes, for example, a method comprising subjecting the mineral to a neutral salt formation method as disclosed in WO 98/14072 in a solution prepared by dissolving an emulsifying agent to give precipitates, and subjecting the precipitates to a liquid-solid separation; a method comprising mixing a mineral with a solution prepared by dissolving an emulsifying agent in a solvent capable of dissolving the emulsifying agent such as water, thereafter properly mixing the resulting mixture with an excipient such as dextrin and the like, and removing the solvent by spray-drying, freeze-drying or the like; a method comprising melting an emulsifying agent with heating, and then mixing the melted solution with a mineral, and thereafter cooling the resulting mixture to solidify.
  • the method of coating a mineral includes a method comprising mixing a mineral with the emulsifying agent, and uniformly powdering the resulting mixture.
  • the mineral coated with the emulsifying agent there may be used commercially available products such as SUNACTIVE Fe-12, SUNAC ⁇ VE Fe-P80 manufactured by Taiyo Kagaku Co., Ltd., and the like.
  • the content of the emulsifying agent in the composition of the present invention is preferably from 0.01 to 20 parts by weight, more preferably from 0.1 to 15 parts by weight, based on 100 parts by weight of the mineral, from the viewpoints of absorbability to a living body and flavor.
  • the mineral-containing composition of the present invention further comprises trehalose for further improvement of dispersibility.
  • the content of trehalose in the mineral-containing composition of the present invention is preferably 30% by weight or more, more preferably 40% by weight or more, from the viewpoint of improvement in dispersibility.
  • the upper limit of the content is not particularly limited, as long as the effects of the present invention are not inhibited.
  • the upper limit of the content is preferably 80% by weight or less, more preferably 60% by weight or less.
  • other optional components such as excipients and nutrient components can be added within the range so as not to inhibit the effects of the present invention.
  • the other components include monosaccharides and disaccharides such as fructose, lactose, glucose, saccharose, maltose, galactose, and xylose; oligosaccharides such as xylooligosaccharide, fructooligosaccharide, galactooligosacchande, lactulose, palatinose, soybean oligosaccharide, raffinose, isomaltooligosaccharide; starch, dextrin and decomposed products thereof; a polysaccharide thickener; sugar alcohols such as sorbitol, xylitol, erythritol, maltitol, and lactitol; vitamins such as vitamin A, vitamin B 1?
  • These optional components may be used alone or in a mixture of two or more kinds.
  • the mineral-containing composition of the present invention may be prepared by mixing each of the components mentioned above in given amounts.
  • the composition may be prepared by, for example, using one or more granulation devices selected from a fluidized-bed granulator, a tumbling- bed granulator, a spray-drying granulator, an extrusion granulator, a disintegrating-type granulator, a compression granulator, a mixing granulator, a vertical-type granulator, and the like.
  • granulation devices selected from a fluidized-bed granulator, a tumbling- bed granulator, a spray-drying granulator, an extrusion granulator, a disintegrating-type granulator, a compression granulator, a mixing granulator, a vertical-type granulator, and the like.
  • those prepared by employing the fluidized-bed granulator are preferable, from the viewpoint of dispersibility.
  • the mineral-containing composition of the present invention is prepared by the fluidized-bed granulator, it is preferable that the water-soluble dietary fiber described above is added to a sprayed solution during the granulation from the viewpoint of improving dispersibility.
  • the form of the mineral-containing composition of the present invention after the preparation is not particularly limited.
  • the form includes solution, powder, granule, tablet and the like, preferably granule from the viewpoint of improving dispersibility.
  • the particle size of the granule is not particularly limited. It is preferable that 70% or more of the granule has a particle size of preferably from 10 to 1000 ⁇ m, more preferably 50 to 500 ⁇ m, from the viewpoint of improving dispersibility.
  • the mineral-containing composition of the present invention obtained in the manner as described above can be used as a food additive.
  • the diet includes soups, beverages, rice-based diets and side dishes.
  • Specific examples of the soups include miso soup, butajiru, kenchinjiru, osuimono, Western soup, Chinese noodles (rame ⁇ ), wheat noodles ( ⁇ do ⁇ ), buckwheat noodles (soba), stew, and the like.
  • the beverages include teas such as green tea, oolong tea, black tea, and herbal tea, concentrated fruit juices, concentrated reduced juices, straight juices, fruits mixed juice, pulp-containing fruit juices, fruit-juice containing beverages, fruit and vegetable mixed juices, vegetable juices, carbonated beverages, cold beverages, milk beverages, Japanese sake, beers, wines, cocktails, syochu, whiskies, and the like.
  • teas such as green tea, oolong tea, black tea, and herbal tea
  • concentrated fruit juices concentrated reduced juices, straight juices, fruits mixed juice, pulp-containing fruit juices, fruit-juice containing beverages, fruit and vegetable mixed juices, vegetable juices, carbonated beverages, cold beverages, milk beverages, Japanese sake, beers, wines, cocktails, syochu, whiskies, and the like.
  • rice-based diets include white rice, onigiri, rice porridge, sushi rice, chirashi-sushi, rice boiled with barley, kamameshi, takikomi rice, gomoku rice, festive red rice, donhurio, stir-fried rice, pilaf, rice with curry roux, dried curry, paella, stir-fried chicken and rice, and the like.
  • the side dishes as used herein mean dishes other than the main dishes, and the side dishes may be served as a main course or side course in a diet. Among them, the soups are preferable because the composition of the present invention can be easily used.
  • the additive to a diet as used herein means an additive added to the diet described above.
  • the method of addition includes addition during cooking, addition after being cooked, addition upon the intake of the diet, and the like. Among them, the method of addition upon the intake of the diet is preferable since the addition is easily performed and adjustable to a required amount depending upon individuals. It is preferable that the mineral-containing composition of the present invention is used for addition to a food ration of mass feeding and/or a household cooking, more preferably for addition to food ration provided at hospitals, elder care facilities, schools, sport facilities, facilities of the Self Defense Force and the like.
  • the mineral-containing composition of the present invention is preferably provided, for example, with a small portion packaged in a small pack, bottle or the like, in consideration of user-friendliness in the food service institutions and the general households.
  • the mineral-containing composition of the present invention is provided with a bottle with a cap having a small hole. Since the composition is provided in such a form, the composition can be sprinkled and/or dispersed to each dish as handy as table salt, thereby remarkably improving usefulness in the food service institutions and the general households. Furthermore, since the composition can be added to each dish considering the amount of deficient minerals of an individual, the conventional problem that there is a difference in the amounts of intake of the mineral by individuals.
  • the present invention further provides method of supplementing a mineral, comprising the step of calculating an amount of the mineral deficient in an individual from an amount of the diet taken by the individual, and supplementing the mineral corresponding to the deficient portion, wherein the mineral-containing composition as defined above is added to a diet.
  • the amount of the mineral deficient can be calculated, for example, by subtracting an amount of mineral contained in a diet of an individual from the essential amount of intake disclosed in the sixth edition of "The nutrition necessary for Japanese (dietary reference intakes)" (edited by the Institute of Health and Nutrition Information, published by DAI-ICHI SHUPPAN
  • the amount of the deficient mineral calculated as described above is supplemented by adding the mineral-containing composition of the present invention to a diet of an individual during cooking, after being cooked or upon intake of the diet, preferably upon intake of the diet.
  • the mineral-containing composition of the present invention can be applied not only for supplementing deficiency of minerals, but also for supplementing minerals for the purpose of amelioration of symptoms, such as iron supplement to patients suffering from anemia, or calcium supplement to patients suffering from bone fracture.
  • the amount of the mineral supplemented is calculated by adding the necessary amount suitable for symptoms of an individual to the essential intake amount described above.
  • the calculated amount of mineral to be supplemented is supplemented by adding the mineral-containing composition of the present invention to a diet of an individual during cooking, after being cooked or upon intake of a diet, preferably upon intake of a diet, in the same manner as described above.
  • Example 1 Preparation of Mineral(Iron)-Containing Granule
  • An iron solution prepared by dissolving 130 g of ferric chloride hexahydrate and 3 g of enzymatically decomposed lecithin ("SUNLECITHIN L,” manufactured by Taiyo Kagaku Co., Ltd.) in 600 g of ion-exchanged water was gradually added while stirring to a pyrophosphate solution prepared by dissolving 200 g of tetrasodium pyrophosphate decahydrate and 17 g of pentaglycerol monomyristate ("SUNSOFT A-141E,” manufactured by Taiyo Kagaku Co., Ltd.) in 5 kg of ion-exchanged water.
  • SUNSOFT A-141E pentaglycerol monomyristate
  • the pH of the mixed solution was adjusted to 3.0.
  • the reaction mixture was subjected to solid-liquid separation by centrifugation (3000 G, 5 minutes) to give an iron salt coated with the emulsifying agent.
  • 800 ml of ion-exchanged water was added to the iron salt, and the mixture was dispersed, to give 860 ml of a solution of the iron salt coated with the emulsifying agent.
  • the average particle size of the iron salt in the resulting solution was determined by a laser diffraction particle size distribution analyzer ("HELOS & RODOS," manufactured by SYMPATEC). As a result, the average particle size was 0.5 ⁇ m.
  • Dextrin was added to the resulting solution, and the mixture was spray- dried, to give a ferric pyrophosphate powder coated with the emulsifying agent, containing 8% by weight of iron.
  • Example 2 Preparation of Mineral (Calcium)-Containing Granule
  • Preparation of Calcium Carbonate Powder Coated with Emulsifying Agent A calcium solution prepared by dissolving 200 g of calcium chloride dihydrate and 30 g of enzymatically decomposed lecithin ("SUNLECITHIN L,” manufactured by Taiyo Kagaku Co., Ltd.) in 1.2 kg of ion-exchanged water, was gradually added while stirring to a carbonate solution prepared by dissolving 110 g of sodium carbonate and 140 g of a polyglycerol fatty acid ester ("SUNSOFT A-12E,” manufactured by Taiyo Kagaku Co., Ltd.) in 2.6 kg of ion-exchanged water.
  • SUNSOFT A-12E a polyglycerol fatty acid ester
  • the pH of the mixture was adjusted to 9.0.
  • the solution was subjected to liquid-solid separation by centrifugation (3000 G, 5 minutes) to give a calcium salt coated with the emulsifying agent.
  • 800 ml of ion-exchanged water was added to the calcium salt, and the mixture was dispersed, to give 860 ml of a solution of the calcium salt coated with the emulsifying agent.
  • the average particle size of the calcium salt in the resulting solution was determined by a laser diffraction particle size distribution analyzer ("HELOS & RODOS.” manufactured by SYMPATEC). As a result, the average particle size was 0.6 ⁇ m.
  • Dextrin was added to the resulting solution, and the mixture was spray- dried to give a calcium carbonate powder coated with the emulsifying agent, containing 25% by weight of calcium.
  • the mixture was granulated while spraying a solution prepared by dissolving 0.5 g of decomposed galactomannan product ("SUNFIBRE,” manufactured by Taiyo Kagaku Co., Ltd.) in 10 ml of water, to give a mineral(calcium)-containing granule B of the present invention in which the calcium content 1 g of the composition was 100 mg.
  • the particle size distribution of the resulting granule was determined. As a result, 80% of the granules fall within the range of from 50 to 500 ⁇ m.
  • Example 3 Preparation of Mineral (Calcium)-Containing Granule
  • Preparation of Eggshell Calcium Powder Coated with Emulsifying Agent There were mixed together 90 g of middle-chain fatty acid triglyceride ( ("SUNSOFT MCT-6,” manufactured by Taiyo Kagaku Co., Ltd.) and 10 g of polyglycerol condensed ricinoleate (“SUNSOFT 818H,” manufactured by Taiyo Kagaku Co., Ltd.). Next, 100 g of eggshell calcium (“EGGSHELL CALCIUM TS-800,” manufactured by Taiyo Kagaku Co., Ltd., average particle size: about 5 ⁇ m) was added thereto to give an oily suspension.
  • EGGSHELL CALCIUM TS-800 manufactured by Taiyo Kagaku Co., Ltd., average particle size: about 5 ⁇ m
  • the suspension was dispersed with "READY MILL” (manufactured by AIMEX), to give a dispersion of the eggshell calcium.
  • the average particle size of the eggshell calcium in the resulting suspension was determined by a laser diffraction particle size distribution analyzer ("HELOS & RODOS,” manufactured by SYMPATEC). As a result, the average particle size was 0.7 ⁇ m.
  • HELOS & RODOS laser diffraction particle size distribution analyzer
  • SYMPATEC laser diffraction particle size distribution analyzer
  • the average particle size was 0.7 ⁇ m.
  • There were mixed together 130 g of the resulting dispersion 18.6 g of polyglycerol stearate ("SUNSOFT PS-68,” manufactured by Taiyo Kagaku Co., Ltd.), 1.8 g of citric acid monostearic acid ester ("SUNSOFT NO. 621B,” manufactured by Taiyo Kagaku Co., Ltd.), 2.6 g of polyglycerol
  • the mixture was granulated while spraying a solution prepared by dissolving 0.5 g of decomposed galactomannan product ("SUNFIBRE,” manufactured by Taiyo Kagaku Co., Ltd.) in 10 ml of water, to give a mineral(calcium)-containing granule C of the present invention in which of the calcium content in 1 g of the composition was 50 mg.
  • the particle size distribution of the resulting granule was determined. As a result, 80% of the granules fall within the range of from 50 to 500 ⁇ m.
  • Example 4 Preparation of Mineral (MagnesiumVContaining Granule (1) Preparation of Magnesium Phosphate Powder Coated with Emulsifying Agent A phosphoric acid solution was prepared by dissolving 270 g of 85 % phosphoric acid and 20 g of enzymatically decomposed lecithin ("SUNLECITHIN L,” manufactured by Taiyo Kagaku Co., Ltd.) in 5 kg of ion- exchanged water.
  • SUNLECITHIN L enzymatically decomposed lecithin
  • a solution was prepared by dispersing 200 g of magnesium hydroxide in 15 kg of ion-exchanged water, adding 150 g of a polyglycerol fatty acid ester ("SUNSOFT A-14C,” manufactured by Taiyo Kagaku Co., Ltd.) to dissolve. To the resulting solution was gradually added the prepared phosphoric acid solution while stirring, to give a mixture. The pH of the mixture was adjusted to 5.0. After the termination of salt formation of magnesium hydroxide by neutralization reaction, 80 g of gum arabic ("NEOSOFT AB,” manufactured by Taiyo Kagaku Co., Ltd.) was added to the solution.
  • SUNSOFT A-14C polyglycerol fatty acid ester
  • the mixture was subjected to a solid-liquid separation by centrifugation (3000 G, 10 minutes) to give a magnesium salt coated with the emulsifying agent.
  • 800 ml of ion-exchanged water was added to the magnesium salt, and the mixture was dispersed, to give 860 ml of a solution of the magnesium salt coated with the emulsifying agent.
  • the average particle size of the magnesium salt in the resulting solution was determined by a laser diffraction particle size distribution analyzer ("HELOS & RODOS," manufactured by SYMPATEC). As a result, the average particle size was 0.3 ⁇ m.
  • the mixture was granulated while spraying a solution prepared by dissolving 0.5 g of decomposed galactomannan product (SUNFIBRE,” manufactured by Taiyo Kagaku Co., Ltd.) in 10 ml of water, to give a mineral (magnesium)-containing granule D of the present invention in which the magnesium content in 1 g of the composition was 50 mg.
  • the particle size distribution of the resulting granule was determined. As a result, 80% of the granule fall within the range of from 50 to 500 ⁇ m.
  • Test Example 1 Evaluation of Dispersibility The amount 5 g each of the mineral-containing granules obtained in each of Examples 1 to 4 and the Comparative Example 1 was added to 100 mL of water at an ambient temperature while stirring at 360 rpm. The dispersibility was evaluated by determining the time period until which the granules were completely dispersed (time period for complete dispersion). The results are shown in the Table 1.
  • Example 2 Flavor Test 1 To miso soup served as a food rationing in a hospital was added 0.7 g of the mineral-containing granule A obtained in Example 1 and 1.0 g of the mineral-containing granule B obtained in Example 2, to give a mineral- supplemented miso soup. Thereafter, the flavor thereof was compared to that of miso soup without addition of the mineral-containing granules. As a result, it was confirmed that there is no significant difference in flavor therebetween.
  • Test Example 3 Flavor Test 2 200 g of polished rice was washed, and a proper amount of water was added thereto. Further, thereto were added 0.5 g of the mineral-containing granule A obtained in Example 1, 1 g of the mineral-containing granule C obtained in Example 3 and 0.5 g of the mineral-containing granule D obtained in Example 4, and the rice was cooked, to give a mineral-supplemented rice. The flavor of the mineral-supplemented rice was compared to rice without the addition of the mineral-containing granule. As a result, it was confirmed that there is no significant difference in flavor therebetween.
  • Example 5 Use of Granule in Food Ration in Hospital In a food rationing in a hospital, the contents of iron and calcium in the food ration were calculated considering daily menu. As a result, as shown in the Table 2, the iron contents were 2 mg in the breakfast meal, 2 mg in the lunchtime meal and 3 mg in the evening meal, and the calcium contents were 140 mg in the breakfast meal, 120 mg in the lunchtime meal and 160 mg in the evening meal. Table 2 Daily Menu Breakfast Lunchtime Evening Total for Meal Meal Meal One Day Iron Content 2 mg 2 mg 3 mg 7 mg Calcium 140 mg 120 mg 160 mg 420 mg Content
  • the amount of iron and calcium to be supplemented to each meal was 1 mg of iron for each of the meals, and 60 mg of calcium in the breakfast meal, 80 mg in the lunchtime meal and 40 mg in the evening meal.
  • the method of supplement as shown in the Table 4, to the miso soup served in each meal, 0.5 g each of the mineral(iron)-containing granule A obtained in Example 1 was added to the miso soup, and the mineral(calcium)- containing granule B obtained in Example 2 was added in an amount of 0.6 g in the breakfast meal, 0.8 g in the lunchtime meal and 0.4 g in the evening meal.
  • the amounts of iron and calcium required in a female (32 years old) were 12 mg of iron per day and 600 mg of calcium per day, the deficiencies per day were 5 mg in iron and 180 mg in calcium. Therefore, as shown in the Table 4, the amounts of iron and calcium to be supplemented to each meal were 1.2 mg of iron to the breakfast meal and 1.4 mg each to the lunchtime meal and the evening meal, and 60 mg of calcium to the breakfast meal, 80 mg to the lunchtime meal and 40 mg to the evening meal.
  • the amounts of iron and calcium to be supplemented to each meal were 1.2 mg of iron to the breakfast meal and 1.4 mg each to the lunchtime meal and the evening meal; and 100 mg each of calcium to the breakfast meal and the lunchtime meal and 80 mg to the evening meal.
  • to the miso soup served in each meal was added 0.6 g of the mineral(iron)-containing granule A obtained in Example 1 in the breakfast meal, 0.7 g each in the lunchtime meal and the evening meal, and 1.0 g each of the mineral(calcium)-containing granule B obtained in Example 2 in the breakfast meal and the lunchtime meal and 0.8 g in the evening meal.
  • the mineral-containing composition of the present invention can be easily used as a mineral supplement used in food rationing facilities and in general households.

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Mycology (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

Une composition minérale comprenant une fibre alimentaire hydrosoluble et un minéral ; utilisation de la composition minérale sous forme d’additif à un régime alimentaire ; et un procédé d’enrichissement d’un minéral, comprenant l’étape consistant à calculer une quantité du minéral déficient chez un individu en fonction d’une quantité extraite d’un régime alimentaire par l’individu, et fournir le minéral dans une quantité correspondante à une quantité déficiente, où la composition minérale est ajoutée à un régime alimentaire. La composition minérale de la présente invention peut être facilement utilisée en tant que complément minéral utilisé dans les centres de diététique et dans les domiciles en général.
PCT/JP2005/003547 2004-02-27 2005-02-24 Composition minérale et procédé d’utilisation de celle-ci WO2005082167A1 (fr)

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WO2014009805A1 (fr) * 2012-07-31 2014-01-16 Alesco S.R.L. Compositions liquides comprenant du fer destinées à être utilisées dans le traitement de troubles ou de maladies liés à une carence en fer
ITMI20131483A1 (it) * 2013-09-09 2015-03-10 Alesco Srl Composizioni in forma solida a base di minerali e formulazioni orosolubili contenenti le stesse.
CN110353272A (zh) * 2019-07-11 2019-10-22 南通大学 一种钙营养强化剂的制备方法
IT201800006288A1 (it) * 2018-06-13 2019-12-13 Composizioni comprendenti minerali sucrosomiali contenenti sali minerali per uso nelle condizioni di deficienza di tali minerali

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EP3498265A1 (fr) * 2012-07-31 2019-06-19 Alesco S.r.l. Composition solide comprenant du fer destinée à être utilisée dans des maladies liées à une déficience en fer
WO2014009805A1 (fr) * 2012-07-31 2014-01-16 Alesco S.R.L. Compositions liquides comprenant du fer destinées à être utilisées dans le traitement de troubles ou de maladies liés à une carence en fer
ITMI20121350A1 (it) * 2012-07-31 2014-02-01 Alesco Srl Composizione solido a base di ferro per uso nelle condizioni di deficienza di ferro.
ITMI20121351A1 (it) * 2012-07-31 2014-02-01 Alesco Srl Composizione liquida a base di ferro per uso nelle condizioni di deficienza di ferro.
US10765752B2 (en) 2012-07-31 2020-09-08 Alesco S.R.L. Solid composition comprising iron for use in iron deficient conditions
CN111265546A (zh) * 2012-07-31 2020-06-12 阿勒思科公司 用于缺铁病况的含铁固体组合物
CN104602674A (zh) * 2012-07-31 2015-05-06 阿勒思科公司 用于缺铁病况的含铁固体组合物
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WO2014009806A1 (fr) * 2012-07-31 2014-01-16 Alesco S.R.L. Composition solide comprenant du fer destinée à être utilisée dans des conditions de carence en fer
EA027684B1 (ru) * 2012-07-31 2017-08-31 Алеско С.Р.Л. Твердая композиция, содержащая железо, для применения при железодефицитных состояниях
US10183077B2 (en) 2012-07-31 2019-01-22 Alesco S.R.L. Solid composition comprising iron for use in iron deficient conditions
US20160287633A1 (en) * 2013-09-09 2016-10-06 Alesco S.R.L. Solid compostitions based on minerals and orally disintegrating formulations containing the same
WO2015033216A1 (fr) * 2013-09-09 2015-03-12 Alesco S.R.L. Compositions solides comprenant des minéraux, et formulations à désintégration orale les contenant
ITMI20131483A1 (it) * 2013-09-09 2015-03-10 Alesco Srl Composizioni in forma solida a base di minerali e formulazioni orosolubili contenenti le stesse.
US11813290B2 (en) 2013-09-09 2023-11-14 Alesco S.R.L. Solid compositions based on minerals and orally disintegrating formulations containing the same
IT201800006288A1 (it) * 2018-06-13 2019-12-13 Composizioni comprendenti minerali sucrosomiali contenenti sali minerali per uso nelle condizioni di deficienza di tali minerali
WO2019239372A1 (fr) * 2018-06-13 2019-12-19 Pharmanutra S.P.A. Composition comprenant des minéraux de sucrosomial contenant des sels minéraux destinée à être utilisée dans des états de carence en de tels minéraux
CN110353272A (zh) * 2019-07-11 2019-10-22 南通大学 一种钙营养强化剂的制备方法

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