WO1998001544A1 - Procede de production de granules enzymatiques - Google Patents

Procede de production de granules enzymatiques Download PDF

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Publication number
WO1998001544A1
WO1998001544A1 PCT/JP1997/002395 JP9702395W WO9801544A1 WO 1998001544 A1 WO1998001544 A1 WO 1998001544A1 JP 9702395 W JP9702395 W JP 9702395W WO 9801544 A1 WO9801544 A1 WO 9801544A1
Authority
WO
WIPO (PCT)
Prior art keywords
enzyme
weight
water
extruded product
detergent
Prior art date
Application number
PCT/JP1997/002395
Other languages
English (en)
Japanese (ja)
Inventor
Takeshi Ishikawa
Shigeru Kuroda
Jun Kozuka
Shitsuw Shikata
Masafumi Nomura
Original Assignee
Kao Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kao Corporation filed Critical Kao Corporation
Publication of WO1998001544A1 publication Critical patent/WO1998001544A1/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38672—Granulated or coated enzymes
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N9/00—Enzymes; Proenzymes; Compositions thereof; Processes for preparing, activating, inhibiting, separating or purifying enzymes
    • C12N9/98—Preparation of granular or free-flowing enzyme compositions

Definitions

  • agitating tumbling granulator examples include Henshi X Lumixer (Mitsui Miike Kakoki Co., Ltd.), High Speed Mixer (Fukae Kogyo Co., Ltd.), Vertical Granule Yuriichi (Fuji Sangyo Co., Ltd.) ), Gakuo (Mitsui Mining Co., Ltd.)
  • these crystalline gayates may be blended into base detergent particles or may be dry-blended as separate particles.
  • Sequestering agents other than crystalline alkali metal silicates Sequestering agents other than Al force Li metal silicate in detergent compositions, C a I on capturing ability is preferably more than 200 CaC0 3 mgZg.
  • an aluminosilicate having an ion exchange capacity of 200 Ca CO 3 mgZg or more represented by the following formula (4) can also be used.
  • Example 10 Example 11 Example 12 Example 13 Example 14 Example 15 Example 15 Extruded product Example 3
  • Example 3 Example 3
  • Example 5 Pulverization Sub-type, Le speed mill Granulation Granulation Granulation Sphericalization Malmerizer-Granulation Granulation Granulation Coating Granulation Granulation Granulization In-flight None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None None

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Genetics & Genomics (AREA)
  • Zoology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Biomedical Technology (AREA)
  • Biotechnology (AREA)
  • Molecular Biology (AREA)
  • Microbiology (AREA)
  • Medicinal Chemistry (AREA)
  • Biochemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Detergent Compositions (AREA)
  • Enzymes And Modification Thereof (AREA)

Abstract

L'invention concerne un procédé de production de granulés enzymatiques qui consiste à: a) mélanger une composition de formation de granulés sensiblement anhydre comprenant des enzymes et 10 à 40 % en poids d'un liant thermoplastique hydrosoluble ayant un point de fusion ou de ramolissement de 35 à 80 °C, et b) réaliser un moulage par extrusion du mélange obtenu à l'étape a) à une température du point de fusion ou de ramolissement du liant ou à une température supérieure, d'une composition détersive comprenant les granulés enzymatiques obtenus par ledit procédé et d'un détergent. Le procédé peut donner des granulés enzymatiques de granulométrie réduite par ralentissement de l'activité enzymatique. Les granulés enzymatiques ainsi produits ont une faible distribution granulométrique et sont donc difficiles à classer, même lorsqu'ils sont mélangés à un détergent. Par ailleurs, le procédé donne une grande marge de manoeuvre dans la préparation et offre l'avantage que les matériaux adhèrent peu à la paroi interne de la machine qu'on utilise pour la production.
PCT/JP1997/002395 1996-07-10 1997-07-09 Procede de production de granules enzymatiques WO1998001544A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP20115896A JPH1023888A (ja) 1996-07-10 1996-07-10 酵素造粒物の製造方法
JP8/201158 1996-07-10

Publications (1)

Publication Number Publication Date
WO1998001544A1 true WO1998001544A1 (fr) 1998-01-15

Family

ID=16436347

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP1997/002395 WO1998001544A1 (fr) 1996-07-10 1997-07-09 Procede de production de granules enzymatiques

Country Status (2)

Country Link
JP (1) JPH1023888A (fr)
WO (1) WO1998001544A1 (fr)

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000022104A1 (fr) * 1998-10-09 2000-04-20 Kao Corporation Particules d'enzyme
WO2000047060A1 (fr) * 1999-02-10 2000-08-17 Dsm N.V. Granules contenant des enzymes alimentaires
WO2001083727A3 (fr) * 2000-05-04 2002-07-11 Dsm Nv Procede permettant de produire des granules enzymatiques
US7501269B2 (en) 2002-01-15 2009-03-10 Basf Aktiengesellschaft Granulates containing feed-enzymes
US7556802B1 (en) 1999-06-25 2009-07-07 Basf Se Polymer-coated, granulated enzyme-containing feed additives and method for the production thereof
US9259393B2 (en) 2000-11-15 2016-02-16 Aptalis Pharma S.R.L. Microspheres of pancreatic enzymes with high stability and production method thereof
US9976171B2 (en) 2011-08-08 2018-05-22 Allergan Pharmaceuticals International Limited Method for dissolution testing of solid compositions containing digestive enzymes
US10087493B2 (en) 2008-03-07 2018-10-02 Aptalis Pharma Canada Ulc Method for detecting infectious parvovirus in pharmaceutical preparations
US10184121B2 (en) 2013-06-28 2019-01-22 Allergan Pharmaceuticals International Limited Methods for removing viral contaminants from pancreatic extracts
US10206882B2 (en) 2007-02-20 2019-02-19 Allergan Pharmaceuticals International Limited Stable digestive enzyme compositions
US10538720B2 (en) 2016-03-08 2020-01-21 The Procter & Gamble Company Particles including enzyme
US10993996B2 (en) 2013-08-09 2021-05-04 Allergan Pharmaceuticals International Limited Digestive enzyme composition suitable for enteral administration
WO2022072193A1 (fr) 2020-09-30 2022-04-07 Danisco Us Inc Granulés enrobés produits par un procédé de réticulation in situ
US11364205B2 (en) 2010-10-01 2022-06-21 Societe Des Produits Nestle S.A. Stable low digestive enzyme content formulation

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE69913146T2 (de) * 1998-06-30 2004-09-16 Novozymes A/S Neues, verbessertes, enzymhaltiges Granulat
JP5751890B2 (ja) * 2011-03-31 2015-07-22 花王株式会社 自動食器洗浄機用洗浄剤組成物

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1987004184A1 (fr) * 1985-12-27 1987-07-16 Showa Denko Kabushiki Kaisha Procede de granulation d'enzyme
JPH0841491A (ja) * 1994-08-02 1996-02-13 Kao Corp 洗剤用酵素造粒物の製造方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1987004184A1 (fr) * 1985-12-27 1987-07-16 Showa Denko Kabushiki Kaisha Procede de granulation d'enzyme
JPH0841491A (ja) * 1994-08-02 1996-02-13 Kao Corp 洗剤用酵素造粒物の製造方法

Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6410287B1 (en) 1998-10-09 2002-06-25 Kao Corporation Enzyme particles
US6544763B2 (en) 1998-10-09 2003-04-08 Kao Corporation Enzyme particles
WO2000022104A1 (fr) * 1998-10-09 2000-04-20 Kao Corporation Particules d'enzyme
WO2000047060A1 (fr) * 1999-02-10 2000-08-17 Dsm N.V. Granules contenant des enzymes alimentaires
US7186533B2 (en) 1999-02-10 2007-03-06 Basf Aktiengesellschaft Granulates containing feed-enzymes
US7556802B1 (en) 1999-06-25 2009-07-07 Basf Se Polymer-coated, granulated enzyme-containing feed additives and method for the production thereof
WO2001083727A3 (fr) * 2000-05-04 2002-07-11 Dsm Nv Procede permettant de produire des granules enzymatiques
US9259393B2 (en) 2000-11-15 2016-02-16 Aptalis Pharma S.R.L. Microspheres of pancreatic enzymes with high stability and production method thereof
US9884025B2 (en) 2000-11-15 2018-02-06 Aptalis Pharma S.R.L. Microspheres of pancreatic enzymes with high stability and production method thereof
US7501269B2 (en) 2002-01-15 2009-03-10 Basf Aktiengesellschaft Granulates containing feed-enzymes
US10206882B2 (en) 2007-02-20 2019-02-19 Allergan Pharmaceuticals International Limited Stable digestive enzyme compositions
US10087493B2 (en) 2008-03-07 2018-10-02 Aptalis Pharma Canada Ulc Method for detecting infectious parvovirus in pharmaceutical preparations
US11364205B2 (en) 2010-10-01 2022-06-21 Societe Des Produits Nestle S.A. Stable low digestive enzyme content formulation
US9976171B2 (en) 2011-08-08 2018-05-22 Allergan Pharmaceuticals International Limited Method for dissolution testing of solid compositions containing digestive enzymes
US10184121B2 (en) 2013-06-28 2019-01-22 Allergan Pharmaceuticals International Limited Methods for removing viral contaminants from pancreatic extracts
US10993996B2 (en) 2013-08-09 2021-05-04 Allergan Pharmaceuticals International Limited Digestive enzyme composition suitable for enteral administration
US10538720B2 (en) 2016-03-08 2020-01-21 The Procter & Gamble Company Particles including enzyme
WO2022072193A1 (fr) 2020-09-30 2022-04-07 Danisco Us Inc Granulés enrobés produits par un procédé de réticulation in situ

Also Published As

Publication number Publication date
JPH1023888A (ja) 1998-01-27

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