US20060157172A1 - Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product therefrom - Google Patents
Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product therefrom Download PDFInfo
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- US20060157172A1 US20060157172A1 US11/334,813 US33481306A US2006157172A1 US 20060157172 A1 US20060157172 A1 US 20060157172A1 US 33481306 A US33481306 A US 33481306A US 2006157172 A1 US2006157172 A1 US 2006157172A1
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/04—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
- C22F1/053—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with zinc as the next major constituent
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/06—Making non-ferrous alloys with the use of special agents for refining or deoxidising
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C21/00—Alloys based on aluminium
- C22C21/10—Alloys based on aluminium with zinc as the next major constituent
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/002—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working by rapid cooling or quenching; cooling agents used therefor
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
Definitions
- the invention relates to an aluminum alloy that is not sensitive to quenching, and which is used for the production of high-strength forged pieces low in inherent tension, and high-strength extruded and rolled products. Furthermore, the invention relates to a method for the production of a semi-finished product from such an aluminum alloy.
- High-strength aluminum alloys are needed for the aeronautics and space industry, in particular, bearing hull, wing, and chassis parts which demonstrate high strength both under static stress and under dynamic stress.
- the required strength properties can be achieved, in the case of the aforementioned semi-finished products, by using alloys from the 7000 group (7xxx alloys), in accordance with the classification of aluminum alloys prepared by the Aluminum Association (AA).
- Die-forged pieces for parts that are subject to great stress in the aeronautics and space industry for example, parts made from the alloys AA 7075, AA 7175, AA 7475 and, particularly preferably, from the alloys AA 7049 and AA 7050, in America, and made from the alloys AA 7010, AA 7049A, and AA 7050A in Europe.
- a high-strength aluminum alloy of the aforementioned type is known from WO 02/052053 A1, or U.S. Pat. No. 6,972,110 issued on Dec. 6, 2005 to Chakrabarti et al., the disclosure of which is hereby incorporated herein by reference. That reference discloses an alloy having an increased zinc content as compared with earlier alloys of the same type, coupled with a reduced copper and magnesium content.
- the copper and magnesium content in the case of this previously known alloy amounts to less than 3.5%, in total.
- the copper content itself is indicated as being 1.2-2.2 wt.-%, preferably 1.6-2.2 wt.-%.
- this previously known alloy necessarily contains one or more elements from the group zirconium, scandium, and hafnium, with maximum proportions of 0.4 wt.-% zirconium, 0,4 wt.-% scandium, and 0.3 wt.-% hafnium.
- the semi-finished products should be subjected to a special heat treatment to produce the semi-finished products from one of the aforementioned alloys.
- These products can be in the form of forged pieces, wherein with this heat treatment, the extruded profiles, or the rolled sheets are treated to have the desired strength.
- This treatment includes quenching from solution heat temperature, in most cases combined with subsequent cold forming at medium thickness values of more than 50 mm.
- the cold forming serves to reduce the tensions induced during quenching.
- the step of cold forming can occur by means of cold upsetting or also by means of stretching the semi-finished product, typically by 1-3%.
- the semi-finished products produced should be as low in inherent tension as possible, to minimize any undesirable drawing during further processing.
- the semi-finished products and also the finished parts produced from them should be low in inherent tension, to give the designer the possibility of utilizing the entire material potential.
- the method steps to be used for the production of parts for aeronautics and space technology from the alloys AA 7050 as well as AA 7010, and also the maximum thickness of the semi-finished products used for the production of the parts are standardized and/or prescribed.
- the maximal permissible thickness is 200 mm and presupposes that after quenching, the semi-finished product is necessarily subjected to a cold forming step, for the reasons indicated above. With extruded and rolled products, cold forming can be achieved in a fairly simple manner, because of the geometry, which is generally simple, via stretching in the longitudinal direction.
- the invention relates to a high-strength aluminum alloy that is not sensitive to quenching, having the same or better strength properties as the alloys AA 7010 and AA 7050 which, at the same time, has lower inherent tensions due to quenching after cold forming, and from which semi-finished products having a medium thickness can be produced having great strength and fracture resistance, without the need for a cold forming step to reduce inherent tensions induced by quenching.
- the invention further relates to a method for the production of a semi-finished product having the desired properties from this alloy.
- a high-strength aluminum alloy that is not sensitive to quenching comprises an alloy consisting of: 7.0-10.5 wt. % zinc, 1.0-2.5 wt. % magnesium, 0.1-1.15 wt. % copper, 0.06-0.25 wt. % zirconium, 0.02-0.15 wt. % titanium, at most 0.5 wt. % manganese, at most 0.6 wt. % silver, at most 0.10 wt. % silicon, at most 0.10 wt. % iron, at most 0.04 wt.
- % chrome and at least one element selected from the group consisting of: hafnium, scandium, strontium and/or vanadium with a summary content of at most 1.0 wt. %.
- the alloy can also contain contaminants at proportions of at most 0.05 wt. % per element and a total proportion of at most 0.15 wt. %, wherein the remaining component includes aluminum.
- the sum of the alloy elements zinc and magnesium and copper is at least 9 wt. %.
- the invention can also relate to a process for treating the above alloy. That process can include a series of steps including hot forming a plurality of homogenized bars via forging, extrusion and/or rolling in the temperature range of 350-440° C. Next there can be a step of solution heat treating of a hot-formed semi-finished product at temperatures that are sufficiently high to bring the alloy elements necessary for hardening into solution uniformly distributed in the structure, preferably at 465-500° C. Next, there can be the step of quenching of the solution heat treated semi-finished products in water, in a water/glycol mixture, or in a salt mixture at temperatures between 100° C. and 170° C.
- Step of cold forming of the quenched semi-finished product to reduce the inherent tensions that occurred during quenching in the quenching medium.
- step of artificial aging of the quenched semi-finished product in at least one stage, whereby the heating rates, holding times, and temperatures are adjusted for optimization of the properties.
- Semi-finished products having a medium thickness have temper hardening thickness values of 50-180 mm.
- Semi-finished products having a greater thickness have a temper hardening thickness of >180 mm.
- semi-finished products produced from the alloy can be mildly cooled, for example in a glycol/water mixture, without any noteworthy negative influence on the very good material properties, after subsequent warm settling. For this reason, the step of cold forming is not necessary for medium thickness values, since the inherent stresses induced with the mild cooling are non-critically low. Therefore it is possible to produce semi-finished products in the medium thickness range with this alloy, in a simple and inexpensive manner, namely without a cold-forming step that would otherwise be necessary.
- the advantageous properties of the alloy as described above can also be utilized to simplify the production process of a part for the production of which a semi-finished product having a greater starting thickness is required, and which part has a medium thickness after being processed.
- a semi-finished product having a greater thickness for example a forged one, is pre-processed by cutting, after the step of hot forming.
- the pre-processing is designed so that the semi-finished product, which will then be quenched within the course of hot forming, undergoes a reduction in thickness.
- This reduction in thickness is necessary for the production of the finished part, in any case, wherein the pre-processed semi-finished product can be subjected to heat treatment with mild quenching (glycol/water mixture), without performing a cold forming step that is otherwise necessary for greater thickness values.
- mild quenching glycol/water mixture
- semi-finished products having a medium thickness can therefore be quenched in mild manner, by means of glycol/water mixtures.
- semi-finished products having a greater thickness such mild quenching is not practical because of the minimum cooling speed that is required. Accordingly, semi-finished products having a greater thickness are quenched in water. As a result of this, these semi-finished products are subsequently subjected to cold forming, for example upsetting or stretching by 1-5%.
- the aforementioned properties of the semi-finished product produced from this alloy are unexpected, since contrary to the default values that result from the state of the art, the copper content is clearly lower than was the case for previously known high-strength aluminum alloys.
- the copper content is only 0.8-1.1 wt. %.
- the copper content is only about 50% of the preferred copper content of the aluminum alloys known from WO 02/052053 A1 or U.S. Pat. No. 6,972,110. It is surprising that very high strength values are achieved despite this. It is assumed that these properties are based on the balanced composition of the alloy components, which also includes the relative high zinc content values and the magnesium content that is adapted to this.
- the sum of the elements magnesium, copper, and zinc are at least 9 wt. %. It has been shown that the desired strength properties can only be achieved if the elements magnesium, copper, and zinc in total are more than 9 wt. %. This characteristic of the alloy is a measure of the fact that the products have the desired strength properties. This rule also determines the heat treatability of the semi-finished products produced with the alloy.
- the content will be limited to 0.2-0.7 wt. %, particularly to 0.20-0.40 wt. %.
- the manganese content of the alloy was limited to a maximum 0.5 wt. %.
- the ability to through-harden an Al—Zn—Cu—Mg alloy decreases with an increasing manganese content. For this reason, the manganese content is limited.
- zirconium The reduced effect of the manganese with regard to controlling the structure is balanced out by means of adding zirconium. According to a preferred exemplary embodiment, the latter amounts to 0.14-0.20 wt. %.
- Zirconium also precipitates from the structure during homogenization of the extruded bars, in the form of zirconium aluminides. These aluminides are generally configured to be more micro-dispersed than the manganese aluminides. For this reason, they are particularly helpful with regard to controlling recrystallization.
- the zirconium aluminides that are formed are not made more coarse by the heat treatment that is provided, and are stable in the selected temperature ranges, in contrast to manganese aluminides. For this reason, zirconium is a necessary component of the alloy.
- the titanium contained in the alloy primarily serves for making the grain fine during extrusion molding.
- a value of 0.03-0.1 wt. % titanium is preferred, particularly 0.03-0.06 wt. % titanium added to the alloy.
- the desired properties are achieved if the alloy components are used in the proportions of the range indicated.
- Semi-finished products having the required properties can no longer be produced with an alloy in which one or more alloy components have a proportion that lies outside the range indicated.
- the semi-finished products are produced from this alloy with the following steps:
- Solution heat treating of the hot-formed semi-finished product at temperatures that are sufficiently high to bring the alloy elements necessary for hardening into solution uniformly distributed in the structure, preferably at 465-500° C.; Quenching of the solution heat treated semi-finished products in water, at a temperature between room temperature and 100° C., or in a water/glycol mixture, or in a salt mixture at temperatures between 100° C. and 170° C.; and
- the artificial aging of the quenched semi-finished product occurs in two stages.
- the semi-finished product is heated to a temperature of more than 100° C. and held at this temperature for more than eight hours, and in the second stage, it is heated to more than 130° C. and heated for more than five hours.
- These two stages can be performed directly following one another.
- the semi-finished product treated with the first stage can also cool off, and the second stage of artificial aging can be performed at a later point in time, without having to accept any disadvantages with regard to the desired properties of the semi-finished product.
- FIG. 1 is a graph representing the strength behavior of various AA 7xxx alloys as a function of the average cooling speed during quenching from solution heat treatment temperature
- FIG. 2 is a flow chart for a process for producing the alloy.
- the two alloys Z1, Z2 have the following composition: Si Fe Cu Mn Mg Cr Zn Ti Zr Ti + Zr Alloy Z1 0.05 0.05 0.95 0.39 1.70 0.002 8.35 0.035 0.12 0.155 Alloy Z2 0.04 0.07 0.90 0.004 1.65 0.001 8.50 0.025 0.12 0.145
- the alloys Z1, Z2 were cast to produce extrusion blocks having a diameter of 370 mm, on an industrial scale.
- the extrusion blocks were homogenized to balance out the micro-segregation resulting from solidification.
- the blocks were homogenized in two stages, in a temperature range of 465° C.-485° C., and cooled.
- the homogenized blocks were pre-heated to 370° C. and formed multiple times to produce free-form forged pieces having a thickness of 250 mm and to a width of 500 mm.
- the free-form forged pieces of alloy Z1 and Z2 were solution heat treated at 485° C. for at least 4 hours, quenched in water at room temperature, and subsequently artificially aged between 100° C. and 160° C., wherein the artificial aging was carried out in two stages.
- the semi-finished product was heated to more than 100° C. and held at this temperature for more than eight hours.
- the second stage which was carried out immediately after the first stage, took place at a temperature of more than 130° C. for more than five hours.
- the results show that the R p02 and R m values are almost identical for all three stress directions, and lie above 490 MPa for the stretching limit (R p02 ) and above 520 MPa for tensile strength.
- the A 5 values are highest for the L direction, and reach at least 4% breaking elongation (A 5 ) for the two transverse directions.
- the K IC values are listed as follows: Alloy Test Direction Position K IC (MPa ⁇ m) R p0.2 (MPa) Z1 L-T Edge 30.5 529 L-T Core 32.9 504 T-L Edge 23.1 516 T-L Core 20.4 502 Z2 L-T Edge 30.3 514 L-T Core 35.9 520 T-L Edge 23.6 514 T-L Core 21.8 508
- the stress crack corrosion resistance was determined on round samples for the LT and the ST position, according to ASTM G47 (alternating immersion test). The results are listed below for the alloy Z1: Electrical Stress Direction Stress Mpa Duration (Days) Conductivity LT 320 >30 34.7 ST 320 >30 34.7
- forged pieces having the same parameters were produced from the alloy Z1.
- the forged pieces were cold-upset in the short transverse direction (ST) after solution heat treatment and quenching, to reduce the inherent stresses resulting from quenching.
- ST short transverse direction
- the strength properties were determined at room temperature, in the sample positions “long” (L), “long-transverse” (LT), and “short-transverse” (ST).
- the results show that the R p02 and R m values for all three stress directions are less, and that the lowest value was found for the short-transverse direction (ST).
- the A 5 values are highest for the L direction, and reach-at least 6% breaking elongation (A 5 ) for the two-transverse directions.
- the decrease in strength can be reduced by shortening the second hardening stage.
- the K IC values are listed in the following table: Alloy Test Direction Position K IC (MPa ⁇ m) R p0.2 (MPa) Z1 L-T Edge 30.5 529 L-T Core 32.9 504 T-L Edge 23.1 516 T-L Core 20.4 502 Z1 + Cold L-T Edge 38.9 485 Upsetting L-T Core 42.2 448 T-L Edge 23.9 474 T-L Core 21.9 468
- free-form forged pieces having a thickness of 150 mm and a width of 500 mm were produced from alloy Z1 and, after solution heat treatment, were quenched in water or a water/glycol mixture with approximately 20% and approximately 40%, respectively, and warm settled as described above.
- One forged piece was additionally cold upset after being quenched in water.
- the influence of the various cooling media was determined on drawn samples that were taken from the forged pieces in the directions “long” (L), “long-transverse” (LT), and “short-transverse” (ST).
- the average strength properties of the alloy for a thickness of 150 mm for various cooling treatments are shown as follows: Quenching R p0.2 R m A 5 Medium Stress Direction (MPa) (MPa) (%) Water(RT) L 551 573 10.3 LT 515 544 7.5 ST 505 549 8.0 Water (RT) + L 491 537 12.8 Cold upsetting LT 465 520 8.7 ST 430 513 8.5 Water/Glycol L 545 566 12.5 (16-20%) LT 520 547 7.2 ST 512 548 8.3 Water/Glycol L 503 529 12.2 (38-40%) LT 493 525 5.0 ST 487 526 5.6
- the K IC values are contained in the following table: Quenching Medium Test Direction K IC (MPa ⁇ m) R p.02 Water (RT) L-T 36.8 551 T-L 23.8 515 Water (RT) + Cold L-T 39.1 491 Upsetting T-L 24.1 465 Water/glycol L-T 28.2 545 (16-20%) T-L 20.7 520 Water/glycol L-T 35.4 503 (38-40%) T-L 18.5 493
- the alloy Z1 was also cast in another example, analogous to the first example, and blocks for extrusion were produced.
- the homogenized blocks were pre-heated to over 370° C. and pressed into extrusion profiles having a rectangular cross-section, with a thickness of 40 mm and a width of 100 mm.
- the profiles were solution heat treated for at least 4 hours at 485° C., quenched in water at room temperature, and subsequently artificially aged between 100° C. and 160° C., in two stages (first stage: >100° C., >8 h; second stage: >130° C., >5 h).
- the results show that the R p02 and R m values are highest in the L direction, at values of 600 MPa and 609 MPa, respectively, and lowest in the ST direction, at values of 505 MPa and 561 MPa, respectively.
- the A 5 values are highest for the L direction, and reach at least 7% breaking elongation (A 5 ) for the two transverse directions.
- FIG. 1 shows a diagram representing the strength behavior of various AA 7xxx alloys as a function of the average cooling speed during quenching from solution heat treatment temperature. It is clearly evident in this representation that the loss in strength when using the claimed aluminum alloy is significantly less, even at low cooling speeds, than in the case of the comparison alloys AA 7075, AA 7010, and AA 7050.
- the strength values of the products/semi-finished products produced with the claimed alloy are significantly improved, in particular with regard to stress crack corrosion resistance, as compared with products of previously known alloys, which represents a result that was not foreseeable in the form that occurred.
- the results shown are also interesting in that the strength values described can be particularly presented with artificial aging that is carried out in only two stages.
- FIG. 2 shows a flow chart for a process for producing the alloy.
- step 1 comprises providing the alloy which is disclosed in the above examples.
- step 2 the alloy is hot formed as described above, and in step 3 , the alloy is solution heat treated as described above.
- step 4 the alloy is quenched, while in step 5 , the alloy is optionally cold formed, while in step 6 , the alloy is artificially aged as described above.
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Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
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US12/859,757 US20110008202A1 (en) | 2005-01-19 | 2010-08-19 | Alluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US13/136,301 US20120202086A1 (en) | 2005-01-19 | 2011-07-28 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US14/101,036 US20140099230A1 (en) | 2005-01-19 | 2013-12-09 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US14/861,853 US10301710B2 (en) | 2005-01-19 | 2015-09-22 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
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DE102005002390 | 2005-01-19 | ||
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US12/859,757 Continuation US20110008202A1 (en) | 2005-01-19 | 2010-08-19 | Alluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
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US11/334,813 Abandoned US20060157172A1 (en) | 2005-01-19 | 2006-01-18 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product therefrom |
US12/859,757 Abandoned US20110008202A1 (en) | 2005-01-19 | 2010-08-19 | Alluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US13/136,301 Abandoned US20120202086A1 (en) | 2005-01-19 | 2011-07-28 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US14/101,036 Abandoned US20140099230A1 (en) | 2005-01-19 | 2013-12-09 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US14/861,853 Expired - Fee Related US10301710B2 (en) | 2005-01-19 | 2015-09-22 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
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US12/859,757 Abandoned US20110008202A1 (en) | 2005-01-19 | 2010-08-19 | Alluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US13/136,301 Abandoned US20120202086A1 (en) | 2005-01-19 | 2011-07-28 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US14/101,036 Abandoned US20140099230A1 (en) | 2005-01-19 | 2013-12-09 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
US14/861,853 Expired - Fee Related US10301710B2 (en) | 2005-01-19 | 2015-09-22 | Aluminum alloy that is not sensitive to quenching, as well as method for the production of a semi-finished product |
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ES2292075T3 (es) | 2008-03-01 |
ES2292075T5 (es) | 2010-12-17 |
US20110008202A1 (en) | 2011-01-13 |
US20160010195A1 (en) | 2016-01-14 |
DE502005001724D1 (de) | 2007-11-29 |
US20140099230A1 (en) | 2014-04-10 |
EP1683882B2 (de) | 2010-07-21 |
EP1683882B1 (de) | 2007-10-17 |
US10301710B2 (en) | 2019-05-28 |
EP1683882A1 (de) | 2006-07-26 |
US20120202086A1 (en) | 2012-08-09 |
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