UA98330C2 - Процесс получения катализатора на основе кобальта на подкладке для синтеза фишера-тропша - Google Patents

Процесс получения катализатора на основе кобальта на подкладке для синтеза фишера-тропша

Info

Publication number
UA98330C2
UA98330C2 UAA200912556A UAA200912556A UA98330C2 UA 98330 C2 UA98330 C2 UA 98330C2 UA A200912556 A UAA200912556 A UA A200912556A UA A200912556 A UAA200912556 A UA A200912556A UA 98330 C2 UA98330 C2 UA 98330C2
Authority
UA
Ukraine
Prior art keywords
precursor
producing
treated
tropsch synthesis
synthesis catalyst
Prior art date
Application number
UAA200912556A
Other languages
English (en)
Ukrainian (uk)
Inventor
Якобус Лукас Візажі
Ян Маттеус Ботха
Йоханнес Герхардус Коортзен
Майкл Стівен Датт
Алта Бохмер
де Лоосдрехт Ян ван
Абдул Мутхаліб Саіб
Original Assignee
Сасол Текнолоджи (Проприетари) Лимитед
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Сасол Текнолоджи (Проприетари) Лимитед filed Critical Сасол Текнолоджи (Проприетари) Лимитед
Publication of UA98330C2 publication Critical patent/UA98330C2/ru

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74Iron group metals
    • B01J23/75Cobalt
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/8913Cobalt and noble metals
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08Heat treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16Reducing
    • B01J37/18Reducing with gases containing free hydrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/12Silica and alumina
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02Impregnation, coating or precipitation
    • B01J37/0201Impregnation
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/70Catalyst aspects
    • C10G2300/703Activation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Thermal Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

Процесс получения катализатора на основе кобальта на подкладке для синтеза Фишера-Тропша, который включает: на первом этапе активации – обработку предшественника катализатора газом-восстановителем при первой скорости нагревания HR1, пока предшественник не достигнет температуры Т1, где 80 °C≤Т1≤180 °C, чтобы получить частично обработанный предшественник катализатора, на втором этапе активации – обработку частично обработанного предшественника катализатора газом-восстановителем при второй скорости нагревания HR2, где 0(HR2<HR1 на протяжении времени t1, где t1 составляет от 0, 1до 20 часов, чтобы получить частично восстановленный предшественник катализатора, и после этого – на третьем этапе активации – обработку частично восстановленного предшественника катализатора газом-восстановителем при третьей скорости нагревания HR3, де HR3>HR2, пока частично восстановленный предшественник катализатора не достигнет температуры Т2, и выдержку частично восстановленного предшественника катализатора при Т2 в течении времени t2, где t2 0<t2≤20 часов для получения активированного катализатора.
UAA200912556A 2007-05-04 2008-05-05 Процесс получения катализатора на основе кобальта на подкладке для синтеза фишера-тропша UA98330C2 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ZA200703621 2007-05-04
PCT/IB2008/051723 WO2008135939A2 (en) 2007-05-04 2008-05-05 Catalysts

Publications (1)

Publication Number Publication Date
UA98330C2 true UA98330C2 (ru) 2012-05-10

Family

ID=39874005

Family Applications (2)

Application Number Title Priority Date Filing Date
UAA200912556A UA98330C2 (ru) 2007-05-04 2008-05-05 Процесс получения катализатора на основе кобальта на подкладке для синтеза фишера-тропша
UAA200912562A UA98643C2 (ru) 2007-05-04 2008-05-05 Процесс получения катализатора на основе кобальта на подкладке для синтеза фишера-тропша

Family Applications After (1)

Application Number Title Priority Date Filing Date
UAA200912562A UA98643C2 (ru) 2007-05-04 2008-05-05 Процесс получения катализатора на основе кобальта на подкладке для синтеза фишера-тропша

Country Status (11)

Country Link
US (2) US8067333B2 (ru)
EP (2) EP2155836B1 (ru)
JP (2) JP5284346B2 (ru)
CN (2) CN101688124B (ru)
AU (2) AU2008247041B2 (ru)
BR (2) BRPI0810702A2 (ru)
CA (2) CA2685135C (ru)
RU (2) RU2458100C2 (ru)
UA (2) UA98330C2 (ru)
WO (3) WO2008135941A2 (ru)
ZA (2) ZA200907930B (ru)

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* Cited by examiner, † Cited by third party
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UA98644C2 (ru) 2007-05-11 2012-06-11 Сасол Текнолоджи (Проприетари) Лимитед Процесс регенерации отработанного катализатора на основе кобальта для синтеза фишера-тропша
EP2276563B1 (en) * 2008-04-15 2018-05-23 Sasol Technology (Proprietary) Limited Process for the preparation of a COBALT BASED FISCHER-TROPSCH CATALYST and Fischer Tropsch process
CN102310004B (zh) * 2010-07-07 2013-04-10 中国石油化工股份有限公司 一种钴基费托合成催化剂的还原方法
GB2482171B (en) * 2010-07-22 2018-04-11 Gtl F1 Ag Catalyst treatment
BR112013030533B1 (pt) 2011-04-28 2018-07-03 Sasol Technology (Proprietary) Limited Catalisadores
RU2591702C2 (ru) * 2011-05-06 2016-07-20 Сэсол Текнолоджи (Проприетери) Лимитед Катализаторы
AU2012252072B2 (en) * 2011-05-06 2017-07-06 Sasol Technology (Proprietary) Limited A process for preparing a cobalt - containing hydrocarbon synthesis catalyst precursor
CN103120953B (zh) * 2011-11-18 2014-11-26 中国石油化工股份有限公司 歧化与烷基转移催化剂的还原方法
FR2984347B1 (fr) * 2011-12-14 2015-03-20 IFP Energies Nouvelles Procede de fabrication d'hydrocarbures avec conditionnement du catalyseur
WO2013158955A1 (en) 2012-04-20 2013-10-24 Rensselaer Polytechnic Institute Sensory lighting system and method for characterizing an illumination space
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Also Published As

Publication number Publication date
WO2008135940A3 (en) 2009-03-12
CN101688124A (zh) 2010-03-31
UA98643C2 (ru) 2012-06-11
WO2008135939A2 (en) 2008-11-13
CA2685139A1 (en) 2008-11-13
US8067333B2 (en) 2011-11-29
EP2155836B1 (en) 2016-05-04
RU2009143199A (ru) 2011-06-10
WO2008135940A2 (en) 2008-11-13
EP2155837B1 (en) 2015-07-15
JP5284346B2 (ja) 2013-09-11
ZA200907932B (en) 2010-07-28
AU2008247041A1 (en) 2008-11-13
AU2008247041B2 (en) 2011-05-26
CN101688123A (zh) 2010-03-31
WO2008135941A3 (en) 2009-03-12
RU2456329C2 (ru) 2012-07-20
US20100144520A1 (en) 2010-06-10
JP5284347B2 (ja) 2013-09-11
AU2008247040A1 (en) 2008-11-13
CA2685135C (en) 2015-02-10
CN101688124B (zh) 2013-01-23
ZA200907930B (en) 2010-07-28
BRPI0810702A2 (pt) 2014-10-21
US8062992B2 (en) 2011-11-22
WO2008135939A3 (en) 2009-03-12
BRPI0810701A2 (pt) 2014-10-29
RU2009143198A (ru) 2011-06-10
EP2155836A2 (en) 2010-02-24
CA2685139C (en) 2014-10-07
CA2685135A1 (en) 2008-11-13
WO2008135941A2 (en) 2008-11-13
EP2155837A2 (en) 2010-02-24
JP2010525936A (ja) 2010-07-29
CN101688123B (zh) 2013-02-27
AU2008247040B2 (en) 2011-08-04
RU2458100C2 (ru) 2012-08-10
US20100152035A1 (en) 2010-06-17
JP2010525935A (ja) 2010-07-29

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