UA48952C2 - Спосіб одержання оцтової кислоти - Google Patents
Спосіб одержання оцтової кислотиInfo
- Publication number
- UA48952C2 UA48952C2 UA97041697A UA97041697A UA48952C2 UA 48952 C2 UA48952 C2 UA 48952C2 UA 97041697 A UA97041697 A UA 97041697A UA 97041697 A UA97041697 A UA 97041697A UA 48952 C2 UA48952 C2 UA 48952C2
- Authority
- UA
- Ukraine
- Prior art keywords
- dimethyl ether
- acetic acid
- production
- product flow
- carbon oxide
- Prior art date
Links
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 title abstract 9
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 9
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 abstract 8
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 3
- 229910002090 carbon oxide Inorganic materials 0.000 abstract 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract 2
- 229910002091 carbon monoxide Inorganic materials 0.000 abstract 2
- 230000003197 catalytic effect Effects 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 230000006315 carbonylation Effects 0.000 abstract 1
- 238000005810 carbonylation reaction Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000007792 gaseous phase Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 230000003993 interaction Effects 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 238000003786 synthesis reaction Methods 0.000 abstract 1
- 230000009466 transformation Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/01—Preparation of ethers
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
- C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Запропоновано спосіб одержання оцтової кислоти, що містить в собі стадії каталітичного перетворення синтез-газу, багатого на водень та окис вуглецю, у потік продукту, що містить метанол, простий діметиловий ефір і воду, каталітичної взаємодії метанолу і простого діметилового ефіру в потоці продукту з моноокисом вуглецю та витягу з продукту, який отримано таким чином, потоку, що складається, в основному, з оцтової кислоти. Потік продукту піддають охолодженню з наступним поділом на рідку фазу, що містить метанол, простий діметиловий ефір і воду, що піддають реакції з окисом вуглецю, та газоподібну фазу, що містить окис вуглецю і залишкові кількості простого діметилового ефіру, що виводять із процесу, причому на стадії карбонилювання додають моноокис вуглецю.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DK040796A DK40796A (da) | 1996-04-10 | 1996-04-10 | Fremgangsmåde til fremstilling af eddikesyre |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA48952C2 true UA48952C2 (uk) | 2002-09-16 |
Family
ID=8093178
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UA97041697A UA48952C2 (uk) | 1996-04-10 | 1997-04-09 | Спосіб одержання оцтової кислоти |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US5728871A (uk) |
| EP (1) | EP0801050B1 (uk) |
| JP (1) | JPH1053554A (uk) |
| KR (1) | KR970069966A (uk) |
| CN (1) | CN1078581C (uk) |
| AT (1) | ATE202331T1 (uk) |
| DE (1) | DE69705254T2 (uk) |
| DK (1) | DK40796A (uk) |
| ES (1) | ES2160274T3 (uk) |
| RU (1) | RU2193551C2 (uk) |
| TW (1) | TW413674B (uk) |
| UA (1) | UA48952C2 (uk) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DK136196A (da) * | 1996-11-29 | 1998-05-30 | Haldor Topsoe As | Fremgangsmåde til fremstilling af eddikesyre |
| EP0978501B9 (en) * | 1998-08-06 | 2004-10-06 | Haldor Topsoe A/S | Acetic acid reactive distillation process based on dme/methanol carbonylation |
| US6781014B1 (en) | 1999-11-01 | 2004-08-24 | Acetex (Cyprus) Limited | Methanol plant retrofit for manufacture of acetic acid |
| US6232352B1 (en) | 1999-11-01 | 2001-05-15 | Acetex Limited | Methanol plant retrofit for acetic acid manufacture |
| US6274096B1 (en) | 1999-11-01 | 2001-08-14 | Acetex (Cyprus) Limited | Methanol plant retrofit |
| US6747067B2 (en) * | 2000-03-06 | 2004-06-08 | Woodland Chemical Systems, Inc. | Process for converting cellulosic material into liquids |
| US6531630B2 (en) | 2000-12-29 | 2003-03-11 | Kenneth Ebenes Vidalin | Bimodal acetic acid manufacture |
| US6596781B1 (en) | 2002-05-02 | 2003-07-22 | Chevron U.S.A. Inc. | Integrated process for preparing Fischer-Tropsch products and acetic acid from synthesis gas |
| EA007455B1 (ru) * | 2002-05-20 | 2006-10-27 | Асетэкс (Кипр) Лимитед | Интегрированный способ производства уксусной кислоты и метанола |
| US6846951B1 (en) | 2003-10-09 | 2005-01-25 | Acetex (Cyprus) Limited | Integrated process for acetic acid and methanol |
| US7465823B2 (en) * | 2004-03-17 | 2008-12-16 | Celanese International Corporation | Utilization of acetic acid reaction heat in other process plants |
| MY146697A (en) | 2004-07-09 | 2012-09-14 | Acetex Cyprus Ltd | Preparation of syngas for acetic acid synthesis by partial oxidation of methanol feedstock |
| CA2496839A1 (en) | 2004-07-19 | 2006-01-19 | Woodland Chemical Systems Inc. | Process for producing ethanol from synthesis gas rich in carbon monoxide |
| US7465822B2 (en) | 2005-05-05 | 2008-12-16 | Bp Chemicals Ltd. | Process for carbonylation of alkyl ethers |
| US20060252959A1 (en) * | 2005-05-05 | 2006-11-09 | The Regents Of The University Of California | Process for carbonylation of alkyl ethers |
| EA013194B1 (ru) * | 2006-04-05 | 2010-02-26 | Вудлэнд Байофьюэлс Инк. | Способ получения этанола |
| US7507855B2 (en) * | 2006-12-15 | 2009-03-24 | The Regents Of The University Of California | Process for carbonylation of aliphatic alcohols and/or ester derivatives thereof |
| KR20150099811A (ko) * | 2012-12-21 | 2015-09-01 | 비피 케미칼즈 리미티드 | 합성 가스 및 디메틸에테르로부터 메틸 아세테이트 및 메탄올을 제조하기 위한 통합 프로세스 |
| EP2935173A1 (en) | 2012-12-21 | 2015-10-28 | BP Chemicals Limited | Integrated process for the production of methanol and methyl acetate |
| JP6161724B2 (ja) | 2012-12-21 | 2017-07-12 | ビーピー ケミカルズ リミテッドＢｐ Ｃｈｅｍｉｃａｌｓ Ｌｉｍｉｔｅｄ | メタノールおよび酢酸メチルを生産するための統合方法 |
| WO2018004994A1 (en) | 2016-07-01 | 2018-01-04 | Res Usa, Llc | Fluidized bed membrane reactor |
| WO2018004992A1 (en) | 2016-07-01 | 2018-01-04 | Res Usa, Llc | Conversion of methane to dimethyl ether |
| US10189763B2 (en) | 2016-07-01 | 2019-01-29 | Res Usa, Llc | Reduction of greenhouse gas emission |
| CN109574839B (zh) * | 2017-09-29 | 2021-08-31 | 中国科学院大连化学物理研究所 | 一种合成气直接生产乙酸甲酯和/或乙酸的方法 |
| EP3689848A4 (en) * | 2017-09-29 | 2021-05-12 | Dalian Institute Of Chemical Physics, Chinese Academy of Sciences | PROCESS FOR THE DIRECT PRODUCTION OF METHYL ACETATE AND / OR ACETIC ACID FROM SYNTHETIC GAS |
| CN109908947B (zh) * | 2019-03-14 | 2021-03-30 | 厦门大学 | 一种合成气高选择性转化制乙酸的催化剂及其应用 |
| US20220298095A1 (en) * | 2021-03-19 | 2022-09-22 | Saudi Arabian Oil Company | Production of Acetic Acid through Cryogenic Separation of Syngas |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3769329A (en) * | 1970-03-12 | 1973-10-30 | Monsanto Co | Production of carboxylic acids and esters |
| US4081253A (en) * | 1976-12-10 | 1978-03-28 | Texaco Development Corporation | Production of purified synthesis gas and carbon monoxide |
| US4110359A (en) * | 1976-12-10 | 1978-08-29 | Texaco Development Corporation | Production of cleaned and purified synthesis gas and carbon monoxide |
| CA1299195C (en) * | 1986-06-16 | 1992-04-21 | G. Paull Torrence | Addition of hydrogen to carbon monoxide feed gas in producing acetic acid by carbonylation of methanol |
| DK158221C (da) * | 1987-06-30 | 1990-09-10 | Haldor Topsoe As | Fremgangsmaade til fremstilling af eddikesyre, metylacetat, eddikesyreanhydrid eller blandinger deraf |
-
1996
- 1996-04-10 DK DK040796A patent/DK40796A/da unknown
-
1997
- 1997-03-21 TW TW086103570A patent/TW413674B/zh not_active IP Right Cessation
- 1997-03-21 ES ES97104856T patent/ES2160274T3/es not_active Expired - Lifetime
- 1997-03-21 AT AT97104856T patent/ATE202331T1/de not_active IP Right Cessation
- 1997-03-21 DE DE69705254T patent/DE69705254T2/de not_active Expired - Lifetime
- 1997-03-21 EP EP97104856A patent/EP0801050B1/en not_active Expired - Lifetime
- 1997-04-04 US US08/832,880 patent/US5728871A/en not_active Expired - Lifetime
- 1997-04-09 JP JP9091069A patent/JPH1053554A/ja active Pending
- 1997-04-09 UA UA97041697A patent/UA48952C2/uk unknown
- 1997-04-09 RU RU97105573/04A patent/RU2193551C2/ru active
- 1997-04-10 KR KR1019970013142A patent/KR970069966A/ko not_active Application Discontinuation
- 1997-04-10 CN CN97110543A patent/CN1078581C/zh not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE69705254D1 (de) | 2001-07-26 |
| EP0801050A1 (en) | 1997-10-15 |
| TW413674B (en) | 2000-12-01 |
| KR970069966A (ko) | 1997-11-07 |
| EP0801050B1 (en) | 2001-06-20 |
| DE69705254T2 (de) | 2001-10-11 |
| ATE202331T1 (de) | 2001-07-15 |
| DK40796A (da) | 1997-10-11 |
| CN1171391A (zh) | 1998-01-28 |
| JPH1053554A (ja) | 1998-02-24 |
| CN1078581C (zh) | 2002-01-30 |
| RU2193551C2 (ru) | 2002-11-27 |
| US5728871A (en) | 1998-03-17 |
| ES2160274T3 (es) | 2001-11-01 |
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