TWI881208B - 鈮酸鋰溶液及其製造方法 - Google Patents

鈮酸鋰溶液及其製造方法 Download PDF

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Publication number
TWI881208B
TWI881208B TW111109377A TW111109377A TWI881208B TW I881208 B TWI881208 B TW I881208B TW 111109377 A TW111109377 A TW 111109377A TW 111109377 A TW111109377 A TW 111109377A TW I881208 B TWI881208 B TW I881208B
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Taiwan
Prior art keywords
lithium niobate
solution
niobium
lithium
positive electrode
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TW111109377A
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English (en)
Chinese (zh)
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TW202308944A (zh
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元野隆二
原周平
荒川泰輝
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日商三井金屬鑛業股份有限公司
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G33/00Compounds of niobium
    • C01G33/003Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G33/00Compounds of niobium
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • H01M10/0525Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/362Composites
    • H01M4/366Composites as layered products
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/62Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
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    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/026Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028Positive electrodes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Composite Materials (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
TW111109377A 2021-04-28 2022-03-15 鈮酸鋰溶液及其製造方法 TWI881208B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2021075470 2021-04-28
JP2021-075470 2021-04-28

Publications (2)

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TW202308944A TW202308944A (zh) 2023-03-01
TWI881208B true TWI881208B (zh) 2025-04-21

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US (1) US20240208839A1 (https=)
EP (1) EP4332064A4 (https=)
JP (2) JP7329705B2 (https=)
KR (1) KR102831339B1 (https=)
CN (1) CN117480122A (https=)
TW (1) TWI881208B (https=)
WO (1) WO2022230387A1 (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116581277A (zh) * 2023-06-30 2023-08-11 湖州耀宁固态能源科技有限公司 正极活性材料及其制备方法以及包含它的全固态锂电池
WO2025053115A1 (ja) * 2023-09-08 2025-03-13 三井金属鉱業株式会社 金属酸化合物分散液およびその製造方法
CN121666365A (zh) * 2023-09-08 2026-03-13 三井金属株式会社 铌酸化合物分散液及其制造方法
CN117276522B (zh) * 2023-11-22 2024-01-26 天津润光恒科技开发有限公司 纳米铌酸锂包覆的三元正极材料及其制备方法和应用
JP7774761B1 (ja) * 2025-06-26 2025-11-21 Jx金属株式会社 Nb錯体水溶液、全固体リチウムイオン電池用正極活物質の製造方法、全固体リチウムイオン電池用正極の製造方法及び全固体リチウムイオン電池の製造方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1597613A (zh) * 2004-08-06 2005-03-23 哈尔滨工业大学 柠檬酸凝胶方法低温制备铌酸锂纳米粉体
JP2018104242A (ja) * 2016-12-27 2018-07-05 多木化学株式会社 アルカリ金属安定型ニオブ酸ゾル
JP2020066570A (ja) * 2018-10-19 2020-04-30 Dowaエレクトロニクス株式会社 ニオブ酸リチウムの前駆体水溶液およびその製造方法
JP2020164401A (ja) * 2019-03-26 2020-10-08 Dowaエレクトロニクス株式会社 リチウムとニオブ錯体と亜硝酸とを含有する溶液およびその製造方法、並びに、リチウム二次電池用活物質の製造方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5441264B2 (ja) * 2009-03-12 2014-03-12 多木化学株式会社 ニオブ酸アンモニウムゾル及びその製造方法並びに薄膜形成用塗布液及び薄膜担持基材
JP6309808B2 (ja) * 2013-04-02 2018-04-11 Dowaホールディングス株式会社 リチウムと、ニオブ酸のペルオキソ錯体とを含有する溶液と、その製造方法
JP6205248B2 (ja) * 2013-11-21 2017-09-27 Dowaホールディングス株式会社 リチウムとニオブ錯体とを含有する溶液、およびその製造方法、並びにリチウムイオン電池
JP6882912B2 (ja) 2016-06-28 2021-06-02 Dowaエレクトロニクス株式会社 溶液およびその製造方法、ならびに二次電池用活物質の製造方法
JP6920045B2 (ja) * 2016-10-20 2021-08-18 Dowaエレクトロニクス株式会社 リチウム二次電池電極材料の製造方法、リチウム二次電池の製造方法
JP7054588B2 (ja) * 2017-02-10 2022-04-14 多木化学株式会社 ニオブ酸オルガノゾルおよびその製造方法
JP7010176B2 (ja) * 2018-08-29 2022-01-26 トヨタ自動車株式会社 ニオブ酸リチウム、及びそれの製造方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1597613A (zh) * 2004-08-06 2005-03-23 哈尔滨工业大学 柠檬酸凝胶方法低温制备铌酸锂纳米粉体
JP2018104242A (ja) * 2016-12-27 2018-07-05 多木化学株式会社 アルカリ金属安定型ニオブ酸ゾル
JP2020066570A (ja) * 2018-10-19 2020-04-30 Dowaエレクトロニクス株式会社 ニオブ酸リチウムの前駆体水溶液およびその製造方法
JP2020164401A (ja) * 2019-03-26 2020-10-08 Dowaエレクトロニクス株式会社 リチウムとニオブ錯体と亜硝酸とを含有する溶液およびその製造方法、並びに、リチウム二次電池用活物質の製造方法

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EP4332064A1 (en) 2024-03-06
JP7329705B2 (ja) 2023-08-18
US20240208839A1 (en) 2024-06-27
WO2022230387A1 (ja) 2022-11-03
EP4332064A4 (en) 2024-11-20
JP2023153202A (ja) 2023-10-17
CN117480122A (zh) 2024-01-30
TW202308944A (zh) 2023-03-01
JP7588188B2 (ja) 2024-11-21
KR20230174276A (ko) 2023-12-27
KR102831339B1 (ko) 2025-07-08
JPWO2022230387A1 (https=) 2022-11-03

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