KR102831339B1 - 니오브산리튬 용액 및 그 제조 방법 - Google Patents

니오브산리튬 용액 및 그 제조 방법 Download PDF

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KR102831339B1
KR102831339B1 KR1020237040898A KR20237040898A KR102831339B1 KR 102831339 B1 KR102831339 B1 KR 102831339B1 KR 1020237040898 A KR1020237040898 A KR 1020237040898A KR 20237040898 A KR20237040898 A KR 20237040898A KR 102831339 B1 KR102831339 B1 KR 102831339B1
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lithium niobate
solution
niobium
lithium
positive electrode
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KR20230174276A (ko
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류지 모토노
슈헤이 하라
다이키 아라카와
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미쓰이금속광업주식회사
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G33/00—Compounds of niobium
    • C01G33/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G33/00—Compounds of niobium
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/362—Composites
    • H01M4/366—Composites as layered products
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Composite Materials (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
KR1020237040898A 2021-04-28 2022-03-10 니오브산리튬 용액 및 그 제조 방법 Active KR102831339B1 (ko)

Applications Claiming Priority (3)

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JPJP-P-2021-075470 2021-04-28
JP2021075470 2021-04-28
PCT/JP2022/010677 WO2022230387A1 (ja) 2021-04-28 2022-03-10 ニオブ酸リチウム溶液およびその製造方法

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KR20230174276A KR20230174276A (ko) 2023-12-27
KR102831339B1 true KR102831339B1 (ko) 2025-07-08

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US (1) US20240208839A1 (https=)
EP (1) EP4332064A4 (https=)
JP (2) JP7329705B2 (https=)
KR (1) KR102831339B1 (https=)
CN (1) CN117480122A (https=)
TW (1) TWI881208B (https=)
WO (1) WO2022230387A1 (https=)

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CN116581277A (zh) * 2023-06-30 2023-08-11 湖州耀宁固态能源科技有限公司 正极活性材料及其制备方法以及包含它的全固态锂电池
WO2025053115A1 (ja) * 2023-09-08 2025-03-13 三井金属鉱業株式会社 金属酸化合物分散液およびその製造方法
CN121666365A (zh) * 2023-09-08 2026-03-13 三井金属株式会社 铌酸化合物分散液及其制造方法
CN117276522B (zh) * 2023-11-22 2024-01-26 天津润光恒科技开发有限公司 纳米铌酸锂包覆的三元正极材料及其制备方法和应用
JP7774761B1 (ja) * 2025-06-26 2025-11-21 Ｊｘ金属株式会社 Ｎｂ錯体水溶液、全固体リチウムイオン電池用正極活物質の製造方法、全固体リチウムイオン電池用正極の製造方法及び全固体リチウムイオン電池の製造方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2018002581A (ja) 2016-06-28 2018-01-11 Ｄｏｗａエレクトロニクス株式会社 溶液およびその製造方法、ならびに二次電池用活物質の製造方法
JP2020066570A (ja) * 2018-10-19 2020-04-30 Ｄｏｗａエレクトロニクス株式会社 ニオブ酸リチウムの前駆体水溶液およびその製造方法
JP2020164401A (ja) 2019-03-26 2020-10-08 Ｄｏｗａエレクトロニクス株式会社 リチウムとニオブ錯体と亜硝酸とを含有する溶液およびその製造方法、並びに、リチウム二次電池用活物質の製造方法

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CN1257131C (zh) * 2004-08-06 2006-05-24 哈尔滨工业大学 利用柠檬酸凝胶方法低温制备铌酸锂纳米粉体的方法
JP5441264B2 (ja) * 2009-03-12 2014-03-12 多木化学株式会社 ニオブ酸アンモニウムゾル及びその製造方法並びに薄膜形成用塗布液及び薄膜担持基材
JP6309808B2 (ja) * 2013-04-02 2018-04-11 Ｄｏｗａホールディングス株式会社 リチウムと、ニオブ酸のペルオキソ錯体とを含有する溶液と、その製造方法
JP6205248B2 (ja) * 2013-11-21 2017-09-27 Ｄｏｗａホールディングス株式会社 リチウムとニオブ錯体とを含有する溶液、およびその製造方法、並びにリチウムイオン電池
JP6920045B2 (ja) * 2016-10-20 2021-08-18 Ｄｏｗａエレクトロニクス株式会社 リチウム二次電池電極材料の製造方法、リチウム二次電池の製造方法
JP6774158B2 (ja) * 2016-12-27 2020-10-21 多木化学株式会社 アルカリ金属安定型ニオブ酸ゾル
JP7054588B2 (ja) * 2017-02-10 2022-04-14 多木化学株式会社 ニオブ酸オルガノゾルおよびその製造方法
JP7010176B2 (ja) * 2018-08-29 2022-01-26 トヨタ自動車株式会社 ニオブ酸リチウム、及びそれの製造方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2018002581A (ja) 2016-06-28 2018-01-11 Ｄｏｗａエレクトロニクス株式会社 溶液およびその製造方法、ならびに二次電池用活物質の製造方法
JP2020066570A (ja) * 2018-10-19 2020-04-30 Ｄｏｗａエレクトロニクス株式会社 ニオブ酸リチウムの前駆体水溶液およびその製造方法
JP2020164401A (ja) 2019-03-26 2020-10-08 Ｄｏｗａエレクトロニクス株式会社 リチウムとニオブ錯体と亜硝酸とを含有する溶液およびその製造方法、並びに、リチウム二次電池用活物質の製造方法

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EP4332064A1 (en) 2024-03-06
JP7329705B2 (ja) 2023-08-18
US20240208839A1 (en) 2024-06-27
WO2022230387A1 (ja) 2022-11-03
EP4332064A4 (en) 2024-11-20
JP2023153202A (ja) 2023-10-17
CN117480122A (zh) 2024-01-30
TW202308944A (zh) 2023-03-01
JP7588188B2 (ja) 2024-11-21
KR20230174276A (ko) 2023-12-27
TWI881208B (zh) 2025-04-21
JPWO2022230387A1 (https=) 2022-11-03

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