TWI551649B - 具高耐水解性和淺的自然顏色之衝擊性改質聚碳酸酯組成物 - Google Patents
具高耐水解性和淺的自然顏色之衝擊性改質聚碳酸酯組成物 Download PDFInfo
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- TWI551649B TWI551649B TW098113402A TW98113402A TWI551649B TW I551649 B TWI551649 B TW I551649B TW 098113402 A TW098113402 A TW 098113402A TW 98113402 A TW98113402 A TW 98113402A TW I551649 B TWI551649 B TW I551649B
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- butyl
- graft polymer
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- 239000000203 mixture Substances 0.000 title claims description 113
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- 125000004432 carbon atom Chemical group C* 0.000 claims description 13
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- 239000003999 initiator Substances 0.000 claims description 12
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- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims description 11
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- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 7
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- 125000000217 alkyl group Chemical group 0.000 claims description 6
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- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 4
- 125000000524 functional group Chemical group 0.000 claims description 4
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- AKNMPWVTPUHKCG-UHFFFAOYSA-N 2-cyclohexyl-6-[(3-cyclohexyl-2-hydroxy-5-methylphenyl)methyl]-4-methylphenol Chemical compound OC=1C(C2CCCCC2)=CC(C)=CC=1CC(C=1O)=CC(C)=CC=1C1CCCCC1 AKNMPWVTPUHKCG-UHFFFAOYSA-N 0.000 claims description 3
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- PRWJPWSKLXYEPD-UHFFFAOYSA-N 4-[4,4-bis(5-tert-butyl-4-hydroxy-2-methylphenyl)butan-2-yl]-2-tert-butyl-5-methylphenol Chemical compound C=1C(C(C)(C)C)=C(O)C=C(C)C=1C(C)CC(C=1C(=CC(O)=C(C=1)C(C)(C)C)C)C1=CC(C(C)(C)C)=C(O)C=C1C PRWJPWSKLXYEPD-UHFFFAOYSA-N 0.000 claims description 3
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- FQUNFJULCYSSOP-UHFFFAOYSA-N bisoctrizole Chemical compound N1=C2C=CC=CC2=NN1C1=CC(C(C)(C)CC(C)(C)C)=CC(CC=2C(=C(C=C(C=2)C(C)(C)CC(C)(C)C)N2N=C3C=CC=CC3=N2)O)=C1O FQUNFJULCYSSOP-UHFFFAOYSA-N 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- PWWSSIYVTQUJQQ-UHFFFAOYSA-N distearyl thiodipropionate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCCCCCCC PWWSSIYVTQUJQQ-UHFFFAOYSA-N 0.000 claims description 3
- 235000019305 distearyl thiodipropionate Nutrition 0.000 claims description 3
- 235000008434 ginseng Nutrition 0.000 claims description 3
- 230000009477 glass transition Effects 0.000 claims description 3
- MSKNHYKUZCSREG-UHFFFAOYSA-N (2,6-ditert-butylphenyl) dihydrogen phosphite Chemical compound CC(C)(C)C1=CC=CC(C(C)(C)C)=C1OP(O)O MSKNHYKUZCSREG-UHFFFAOYSA-N 0.000 claims description 2
- DKCPKDPYUFEZCP-UHFFFAOYSA-N 2,6-di-tert-butylphenol Chemical compound CC(C)(C)C1=CC=CC(C(C)(C)C)=C1O DKCPKDPYUFEZCP-UHFFFAOYSA-N 0.000 claims description 2
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- 125000003710 aryl alkyl group Chemical group 0.000 claims description 2
- 235000010290 biphenyl Nutrition 0.000 claims description 2
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- GPOGLVDBOFRHDV-UHFFFAOYSA-N (2-nonylphenyl) dihydrogen phosphite Chemical compound CCCCCCCCCC1=CC=CC=C1OP(O)O GPOGLVDBOFRHDV-UHFFFAOYSA-N 0.000 claims 1
- 238000010559 graft polymerization reaction Methods 0.000 claims 1
- 125000001971 neopentyl group Chemical group [H]C([*])([H])C(C([H])([H])[H])(C([H])([H])[H])C([H])([H])[H] 0.000 claims 1
- CSWFWSPPZMEYAY-UHFFFAOYSA-N octadecyl dihydrogen phosphite Chemical compound CCCCCCCCCCCCCCCCCCOP(O)O CSWFWSPPZMEYAY-UHFFFAOYSA-N 0.000 claims 1
- 230000003647 oxidation Effects 0.000 claims 1
- 238000007254 oxidation reaction Methods 0.000 claims 1
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 claims 1
- 239000000758 substrate Substances 0.000 claims 1
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 30
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- XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 description 29
- 239000004676 acrylonitrile butadiene styrene Substances 0.000 description 29
- 238000000034 method Methods 0.000 description 22
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 21
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- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 description 3
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- CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Substances [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 description 1
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- PPASLZSBLFJQEF-RXSVEWSESA-M sodium-L-ascorbate Chemical compound [Na+].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RXSVEWSESA-M 0.000 description 1
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- LXEJRKJRKIFVNY-UHFFFAOYSA-N terephthaloyl chloride Chemical compound ClC(=O)C1=CC=C(C(Cl)=O)C=C1 LXEJRKJRKIFVNY-UHFFFAOYSA-N 0.000 description 1
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- AXZWODMDQAVCJE-UHFFFAOYSA-L tin(II) chloride (anhydrous) Chemical compound [Cl-].[Cl-].[Sn+2] AXZWODMDQAVCJE-UHFFFAOYSA-L 0.000 description 1
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- CMWCOKOTCLFJOP-UHFFFAOYSA-N titanium(3+) Chemical class [Ti+3] CMWCOKOTCLFJOP-UHFFFAOYSA-N 0.000 description 1
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- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
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- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- LIPMRGQQBZJCTM-UHFFFAOYSA-N tris(2-propan-2-ylphenyl) phosphate Chemical compound CC(C)C1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C(C)C)OC1=CC=CC=C1C(C)C LIPMRGQQBZJCTM-UHFFFAOYSA-N 0.000 description 1
- XHGIFBQQEGRTPB-UHFFFAOYSA-N tris(prop-2-enyl) phosphate Chemical compound C=CCOP(=O)(OCC=C)OCC=C XHGIFBQQEGRTPB-UHFFFAOYSA-N 0.000 description 1
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- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L69/00—Compositions of polycarbonates; Compositions of derivatives of polycarbonates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/13—Phenols; Phenolates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L51/00—Compositions of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L69/00—Compositions of polycarbonates; Compositions of derivatives of polycarbonates
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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- C08K5/005—Stabilisers against oxidation, heat, light, ozone
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/51—Phosphorus bound to oxygen
- C08K5/52—Phosphorus bound to oxygen only
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
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- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2207/00—Properties characterising the ingredient of the composition
- C08L2207/04—Thermoplastic elastomer
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2666/00—Composition of polymers characterized by a further compound in the blend, being organic macromolecular compounds, natural resins, waxes or and bituminous materials, non-macromolecular organic substances, inorganic substances or characterized by their function in the composition
- C08L2666/02—Organic macromolecular compounds, natural resins, waxes or and bituminous materials
- C08L2666/24—Graft or block copolymers according to groups C08L51/00, C08L53/00 or C08L55/02; Derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L51/00—Compositions of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
- C08L51/04—Compositions of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers grafted on to rubbers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L55/00—Compositions of homopolymers or copolymers, obtained by polymerisation reactions only involving carbon-to-carbon unsaturated bonds, not provided for in groups C08L23/00 - C08L53/00
- C08L55/02—ABS [Acrylonitrile-Butadiene-Styrene] polymers
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- Chemical Kinetics & Catalysis (AREA)
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| FR2969158B1 (fr) | 2010-12-15 | 2013-01-18 | Arkema France | Procede pour modifiants chocs et composition thermoplastique modifiee choc ayant une resistance hydrolytique amelioree |
| EP2537895B1 (en) | 2011-06-20 | 2014-06-04 | Styrolution (Jersey) Limited | Impact modified polycarbonate compositions |
| EP2657258A1 (de) * | 2012-04-23 | 2013-10-30 | Bayer MaterialScience AG | Verfahren zur Herstellung von ABS-Zusammensetzungen mit verbesserter Oberfläche nach Wärme-Feucht-Lagerung |
| EP2657259A1 (de) * | 2012-04-23 | 2013-10-30 | Bayer MaterialScience AG | ABS-Zusammensetzungen mit verbesserter Oberfläche nach Wärme-Feucht-Lagerung |
| EP2687534A1 (de) * | 2012-07-20 | 2014-01-22 | LANXESS Deutschland GmbH | Halogenfreie Poly(alkylenphosphate) |
| JPWO2014141759A1 (ja) * | 2013-03-14 | 2017-02-16 | 三菱エンジニアリングプラスチックス株式会社 | 熱可塑性樹脂組成物 |
| US9260603B2 (en) * | 2013-03-15 | 2016-02-16 | Sabic Global Technologies B.V. | Polymer compositions, method of manufacture, and articles formed therefrom |
| CN103214801B (zh) * | 2013-04-16 | 2016-01-20 | 上海瀚氏模具成型有限公司 | 一种抗老化塑料汽车保险杠及其制备方法 |
| EP2848640A1 (de) * | 2013-09-13 | 2015-03-18 | LANXESS Deutschland GmbH | Phosphorsäureester-Zubereitungen mit verringerter Hygroskopie |
| CN103756279B (zh) * | 2013-12-31 | 2016-04-06 | 东莞市松燊塑料科技有限公司 | 一种无卤阻燃pc/pet合金及其制备方法 |
| WO2016184765A1 (de) | 2015-05-18 | 2016-11-24 | Ineos Styrolution Group Gmbh | Abs-formmasse mit guter eigenschaftskombination von verarbeitbarkeit und oberflächenqualität |
| WO2017065762A1 (en) | 2015-10-14 | 2017-04-20 | Covestro Llc | Phosphazene modified polycarbonate molded battery cooling device |
| EP3786226B1 (en) | 2019-08-27 | 2024-07-24 | Trinseo Europe GmbH | Stabilized compositions of polycarbonates and vinylidene substituted aromatic compounds |
| WO2024206154A1 (en) * | 2023-03-24 | 2024-10-03 | Covestro Llc | Thermal stabilization package for polycarbonate/acrylonitrile-butadiene-styrene blends |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19632701A1 (de) * | 1996-03-14 | 1997-09-18 | Bayer Ag | Stabilisierung von ABS-Pfropfpolymerisaten mit Dithiodipropionsäure |
| CN1717453A (zh) * | 2002-11-29 | 2006-01-04 | 拜尔材料科学股份公司 | 冲击改性共混物 |
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|---|---|---|---|---|
| US3130177A (en) * | 1961-03-24 | 1964-04-21 | Borg Warner | Blends of polycarbonates with polybutadiene, styrene, acrylonitrile graft copolymers |
| DE3542468A1 (de) * | 1985-11-30 | 1987-06-04 | Bayer Ag | Neue stabilisatorsysteme fuer polymere i |
| EP0702019A1 (en) * | 1994-09-16 | 1996-03-20 | General Electric Company | Liquid neo-diol phosphites as polymer stabilizers |
| US6545089B1 (en) * | 1997-09-04 | 2003-04-08 | General Electric Company | Impact modified carbonnate polymer composition having improved resistance to degradation and improved thermal stability |
| US6063844A (en) * | 1998-04-02 | 2000-05-16 | General Electric Company | Polycarbonate/rubber-modified graft copolymer resin blends having improved thermal stability |
| JP3616792B2 (ja) * | 1998-10-16 | 2005-02-02 | 出光興産株式会社 | 難燃性熱可塑性樹脂組成物および射出成形品 |
| DE19941491A1 (de) * | 1999-09-01 | 2001-03-15 | Bayer Ag | Thermoplastische Formmassen auf Basis bestimmter Pfropfkautschukkomponenten |
| DE10026858A1 (de) * | 2000-05-31 | 2001-12-06 | Basf Ag | Stabilisierte thermoplastische Formmassen |
| DE10255825A1 (de) * | 2002-11-29 | 2004-06-09 | Bayer Ag | Blends mit verbesserten Eigenschaften |
| US7309755B2 (en) * | 2005-08-24 | 2007-12-18 | General Electric Company | Method of producing polycarbonate articles by rotation molding and rotation molded articles made by the method |
| DE102005058847A1 (de) * | 2005-12-09 | 2007-06-14 | Bayer Materialscience Ag | Polycarbonat-Formmassen |
| WO2007085610A1 (en) * | 2006-01-25 | 2007-08-02 | Basf Se | Low individual colour thermoplastic molding composition |
| JP4848788B2 (ja) * | 2006-02-08 | 2011-12-28 | 三菱エンジニアリングプラスチックス株式会社 | 熱可塑性樹脂組成物および樹脂成形品 |
| JP5168812B2 (ja) * | 2006-04-13 | 2013-03-27 | 三菱エンジニアリングプラスチックス株式会社 | 熱可塑性樹脂組成物および樹脂成形品 |
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- 2015-06-01 US US14/726,729 patent/US20150259529A1/en not_active Abandoned
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19632701A1 (de) * | 1996-03-14 | 1997-09-18 | Bayer Ag | Stabilisierung von ABS-Pfropfpolymerisaten mit Dithiodipropionsäure |
| CN1717453A (zh) * | 2002-11-29 | 2006-01-04 | 拜尔材料科学股份公司 | 冲击改性共混物 |
Also Published As
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| RU2010147711A (ru) | 2012-05-27 |
| WO2009129962A1 (de) | 2009-10-29 |
| BRPI0911355A2 (pt) | 2018-02-20 |
| JP2011518904A (ja) | 2011-06-30 |
| CN102015891A (zh) | 2011-04-13 |
| CA2722228A1 (en) | 2009-10-29 |
| BRPI0911355B1 (pt) | 2019-07-30 |
| MX2010010645A (es) | 2010-10-20 |
| CN102015891B (zh) | 2015-04-29 |
| EP2285905A1 (de) | 2011-02-23 |
| US20090281216A1 (en) | 2009-11-12 |
| ES2390469T3 (es) | 2012-11-13 |
| KR20100135836A (ko) | 2010-12-27 |
| WO2009129962A4 (de) | 2010-01-21 |
| KR101661771B1 (ko) | 2016-09-30 |
| CA2722228C (en) | 2018-02-06 |
| TW201005033A (en) | 2010-02-01 |
| EP2285905B1 (de) | 2012-07-25 |
| US20150259529A1 (en) | 2015-09-17 |
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