TWI455904B - 單相水凝黏合劑、其製造方法及以其製成之建築材料 - Google Patents

單相水凝黏合劑、其製造方法及以其製成之建築材料 Download PDF

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TWI455904B
TWI455904B TW097128234A TW97128234A TWI455904B TW I455904 B TWI455904 B TW I455904B TW 097128234 A TW097128234 A TW 097128234A TW 97128234 A TW97128234 A TW 97128234A TW I455904 B TWI455904 B TW I455904B
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Taiwan
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weight
starting material
phase
water content
calcium
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TW097128234A
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TW200922901A (en
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Peter Stemmermann
Guenter Beuchle
Krassimir Garbev
Uwe Schweike
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Karlsruher Inst Technologie
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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B7/00—Hydraulic cements
    • C04B7/345—Hydraulic cements not provided for in one of the groups C04B7/02 - C04B7/34
    • C04B7/3453—Belite cements, e.g. self-disintegrating cements based on dicalciumsilicate
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/20—Silicates
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/18—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing mixtures of the silica-lime type
    • C04B28/186—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing mixtures of the silica-lime type containing formed Ca-silicates before the final hardening step
    • C04B28/188—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing mixtures of the silica-lime type containing formed Ca-silicates before the final hardening step the Ca-silicates being present in the starting mixture
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00034—Physico-chemical characteristics of the mixtures
    • C04B2111/00215—Mortar or concrete mixtures defined by their oxide composition
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00—Technologies relating to the processing of minerals
    • Y02P40/10—Production of cement, e.g. improving or optimising the production methods; Cement grinding

Claims (15)

  1. 鈣、氧及氫原子之單相水凝黏合劑，該等原子係於包含具有平均結合度高於Q1.5 之矽酸鹽組成單元及矽烷醇基之排列中，其中並無任何或部分鈣原子係由與氧六重配位或更高配位之金屬原子M[6]x+ 所取代及/或並無或部分矽原子係由與氧四面體配位之金屬原子M[4]y+ 所取代，[CaO+(x/2)．(M[6]x+ Ox/2 )]：[SiO2 +M[4]y+ Oy/2 ]之莫耳比具有0.2至2.0之值，及該黏合劑具有3.5重量%至20重量%之水含量。
  2. 如申請專利範圍第1項之單相水凝黏合劑，該[CaO+(x/2)]．(M[6]x+ Ox/2 )]：[SiO2 +M[4]y+ Oy/2 ]之莫耳比具有0.3至小於1.0之數值。
  3. 如申請專利範圍第1或2項之單相水凝黏合劑，其中部分鈣原子係由Na、K、Li、Mg、Sr、Ba、Mn、Fe[+II]或Al[+III]原子所取代。
  4. 如申請專利範圍第1或2項之單相水凝黏合劑，其中部分矽原子係經Al、Ge、B、P、Fe、Be或Ti原子取代。
  5. 如申請專利範圍第1或2項之單相水凝黏合劑，其於添加水後反應成為水合物，其中大於50重量%水合物為具有莫耳比[CaO+(x/2)]．(M[6]x+ Ox/2 )]：[SiO2 +M[4]y+ Oy/2 ]小於1.5之矽酸鈣水合物。
  6. 一種混合物，其係含有如申請專利範圍第1至5項中任一項之單相水凝黏合劑。
  7. 如申請專利範圍第6項之混合物，含有至少10重量%之該單相水凝黏合劑。
  8. 一種製造如申請專利範圍第1至5項中任一項之單相水凝黏合劑之方法，係經由-反應研磨含有呈結構水、結晶水或氫氧基形式及具有Q0 至Q2 之結合度的矽酸鹽組成單元之形式存在的鈣、矽、氧及氫原子之第一起始物料，與具有Q3 至Q4 之矽酸鹽組成單元結合度之呈固體矽酸鹽原料形式之第二起始物料，以及-只要水含量為高於20重量%或以上，乾燥該單相水凝黏合劑至3.5重量%至20重量%之水含量。
  9. 一種製造如申請專利範圍第1至5項中任一項之單相水凝黏合劑之方法，其係經由-反應研磨一種材料，該材料於反應研磨期間形成含有呈結構水、結晶水或氫氧基形式及具有Q0 至Q2 之結合度的矽酸鹽組成單元之形式存在的鈣、矽、氧及氫原子之第一起始物料，與具有Q3 至Q4 之矽酸鹽組成單元結合度之呈固體矽酸鹽原料形式之第二起始物料，以及-只要水含量為高於20重量%或以上，乾燥該單相水凝黏合劑至3.5重量%至20重量%之水含量。
  10. 一種製造如申請專利範圍第6或7項之混合物之方法， 其係經由以下所製造：-反應研磨原料該原料含有申請專利範圍第8項中所述之第一起始物料或申請專利範圍第9項中所述於反應研磨期間形成第一起始物料之材料，且含有申請專利範圍第8或9項中所述之第二起始物料以及額外材料，以及-只要該單相水凝黏合劑之水含量為高於20重量%，乾燥該混合物直至其中所含的單相水凝黏合劑具有3.5重量%至20重量%之水含量。
  11. 如申請專利範圍第8至10項中任一項之方法，其中使用石英或石英砂作為第二起始物料。
  12. 如申請專利範圍第8或10項中任一項之方法，其中該第一起始物料及該第二起始物料係共同存在於一種材料中。
  13. 如申請專利範圍第10項之方法，其中不再用作為建築材料的水泥岩或可含有集料或砂的砂漿係經直接研磨。
  14. 一種建築材料，其係經由使用水凝固如申請專利範圍第1至5項中任一項之單相水凝黏合劑，或如申請專利範圍第6或7項之混合物及隨後硬化而製造。
  15. 如申請專利範圍第14項之建築材料，其含有鹼性敏感添加劑。
TW097128234A 2007-07-27 2008-07-25 單相水凝黏合劑、其製造方法及以其製成之建築材料 TWI455904B (zh)

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DE102007035258A DE102007035258B3 (de) 2007-07-27 2007-07-27 Einphasiges hydraulisches Bindemittel, Verfahren zu seiner Herstellung und mit diesem Bindemittel hergestellter Baustoff

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TWI455904B true TWI455904B (zh) 2014-10-11

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US (1) US8226764B2 (zh)
EP (1) EP2183195B1 (zh)
JP (1) JP5586462B2 (zh)
KR (2) KR20160003321A (zh)
CN (1) CN101821214B (zh)
AU (1) AU2008281033B2 (zh)
BR (1) BRPI0814176A2 (zh)
CA (1) CA2693224C (zh)
DE (1) DE102007035258B3 (zh)
EA (1) EA023619B1 (zh)
ES (1) ES2610207T3 (zh)
HU (1) HUE030870T2 (zh)
PL (1) PL2183195T3 (zh)
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WO (1) WO2009015771A1 (zh)
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DE102007035259B3 (de) * 2007-07-27 2008-11-13 Forschungszentrum Karlsruhe Gmbh Einphasiges hydraulisches Bindemittel, Verfahren zu seiner Herstellung und mit diesem Bindemittel hergestellter Baustoff
AU2012267929B2 (en) * 2011-06-09 2016-05-12 Rutgers, The State University Of New Jersey Synthetic formulations and methods of manufacturing and using thereof
EP2676943B2 (de) 2012-06-20 2021-01-20 HeidelbergCement AG Verfahren zur Herstellung eines Belitzements mit hoher Reaktivitaet und geringem Calcium/Silicat-Verhaeltnis
EP2801557B9 (de) 2013-05-11 2016-01-20 HeidelbergCement AG Verfahren zur Herstellung eines Magnesiumsilikat-Belit-Calciumaluminatzements
GB2530485B (en) 2014-09-15 2017-02-22 Schlumberger Holdings Mid-infrared carbon dioxide sensor
GB2530095B (en) 2014-09-15 2017-07-12 Schlumberger Holdings Mid-infrared sensor
US10414690B2 (en) 2015-01-19 2019-09-17 Cimpor Portugal, Sgps, Sa. Amorphous low-calcium content silicate hydraulic binders and methods for their manufacturing
EP3247685B1 (en) 2015-01-19 2020-08-19 Cimpor Portugal, SGPS, SA Methods for their manufacturing dendritic belite based hydraulic binders
US11499084B2 (en) 2018-12-03 2022-11-15 Halliburton Energy Services, Inc. Expansion agents for cement compositions
WO2020117190A1 (en) 2018-12-03 2020-06-11 Halliburton Energy Services, Inc. Strength retrogression mitigation materials for cement compositions
WO2020117191A1 (en) 2018-12-03 2020-06-11 Halliburton Energy Services, Inc. Composite material for slurry yield enhancement
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EA023619B1 (ru) 2016-06-30
EP2183195A1 (de) 2010-05-12
DE102007035258B3 (de) 2008-11-20
EA201070192A1 (ru) 2010-06-30
KR20160003321A (ko) 2016-01-08
HUE030870T2 (en) 2017-06-28
US20100206199A1 (en) 2010-08-19
CN101821214B (zh) 2014-09-17
KR20100040704A (ko) 2010-04-20
US8226764B2 (en) 2012-07-24
EP2183195B1 (de) 2016-10-26
AU2008281033A1 (en) 2009-02-05
CA2693224A1 (en) 2009-02-05
ES2610207T3 (es) 2017-04-26
ZA200908353B (en) 2010-07-28
BRPI0814176A2 (pt) 2015-01-20
CN101821214A (zh) 2010-09-01
AU2008281033B2 (en) 2013-11-14
PL2183195T3 (pl) 2017-04-28
TW200922901A (en) 2009-06-01
JP5586462B2 (ja) 2014-09-10
KR101621022B1 (ko) 2016-05-13
CA2693224C (en) 2015-06-30
WO2009015771A1 (de) 2009-02-05
JP2010534608A (ja) 2010-11-11

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