SU673166A3 - Способ получени сульфоксидных или сульфоновых производных карбаматов - Google Patents
Способ получени сульфоксидных или сульфоновых производных карбаматовInfo
- Publication number
- SU673166A3 SU673166A3 SU731964954A SU1964954A SU673166A3 SU 673166 A3 SU673166 A3 SU 673166A3 SU 731964954 A SU731964954 A SU 731964954A SU 1964954 A SU1964954 A SU 1964954A SU 673166 A3 SU673166 A3 SU 673166A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- carbamates
- derivatives
- temperature
- producing
- general formula
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 4
- 150000004657 carbamic acid derivatives Chemical class 0.000 title description 3
- ATTZFSUZZUNHBP-UHFFFAOYSA-N Piperonyl sulfoxide Chemical compound CCCCCCCCS(=O)C(C)CC1=CC=C2OCOC2=C1 ATTZFSUZZUNHBP-UHFFFAOYSA-N 0.000 title 1
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 21
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- NHQDETIJWKXCTC-UHFFFAOYSA-N 3-chloroperbenzoic acid Chemical compound OOC(=O)C1=CC=CC(Cl)=C1 NHQDETIJWKXCTC-UHFFFAOYSA-N 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 150000003462 sulfoxides Chemical class 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- 230000002363 herbicidal effect Effects 0.000 description 3
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 3
- 235000019341 magnesium sulphate Nutrition 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- QHTQREMOGMZHJV-UHFFFAOYSA-N Thiobencarb Chemical compound CCN(CC)C(=O)SCC1=CC=C(Cl)C=C1 QHTQREMOGMZHJV-UHFFFAOYSA-N 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 125000004344 phenylpropyl group Chemical group 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- 125000001424 substituent group Chemical group 0.000 description 2
- -1 sulfone derivatives of carbamates Chemical class 0.000 description 2
- YNJSNEKCXVFDKW-UHFFFAOYSA-N 3-(5-amino-1h-indol-3-yl)-2-azaniumylpropanoate Chemical compound C1=C(N)C=C2C(CC(N)C(O)=O)=CNC2=C1 YNJSNEKCXVFDKW-UHFFFAOYSA-N 0.000 description 1
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- AKZWRTCWNXHHFR-PDIZUQLASA-N [(3S)-oxolan-3-yl] N-[(2S,3S)-4-[(5S)-5-benzyl-3-[(2R)-2-carbamoyloxy-2,3-dihydro-1H-inden-1-yl]-4-oxo-3H-pyrrol-5-yl]-3-hydroxy-1-phenylbutan-2-yl]carbamate Chemical compound NC(=O)O[C@@H]1Cc2ccccc2C1C1C=N[C@](C[C@H](O)[C@H](Cc2ccccc2)NC(=O)O[C@H]2CCOC2)(Cc2ccccc2)C1=O AKZWRTCWNXHHFR-PDIZUQLASA-N 0.000 description 1
- 125000003342 alkenyl group Chemical group 0.000 description 1
- 125000000304 alkynyl group Chemical group 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 125000000753 cycloalkyl group Chemical group 0.000 description 1
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000003457 sulfones Chemical class 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Plural Heterocyclic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US37133073A | 1973-06-18 | 1973-06-18 | |
| US37133273A | 1973-06-18 | 1973-06-18 | |
| US371329A US3897492A (en) | 1972-08-14 | 1973-06-18 | Method of making carbamoyl sulfoxide derivatives |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU673166A3 true SU673166A3 (ru) | 1979-07-05 |
Family
ID=27409012
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU731964954A SU673166A3 (ru) | 1973-06-18 | 1973-09-14 | Способ получени сульфоксидных или сульфоновых производных карбаматов |
| SU762322343A SU695521A3 (ru) | 1973-06-18 | 1976-02-16 | Гербицидна композици |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU762322343A SU695521A3 (ru) | 1973-06-18 | 1976-02-16 | Гербицидна композици |
Country Status (7)
| Country | Link |
|---|---|
| DD (1) | DD109217A5 (enrdf_load_stackoverflow) |
| HU (1) | HU168299B (enrdf_load_stackoverflow) |
| PH (1) | PH12123A (enrdf_load_stackoverflow) |
| PL (1) | PL89408B1 (enrdf_load_stackoverflow) |
| RO (1) | RO62922A (enrdf_load_stackoverflow) |
| SU (2) | SU673166A3 (enrdf_load_stackoverflow) |
| YU (1) | YU250673A (enrdf_load_stackoverflow) |
-
1973
- 1973-09-04 RO RO7598073A patent/RO62922A/ro unknown
- 1973-09-11 PL PL16515373A patent/PL89408B1/pl unknown
- 1973-09-14 SU SU731964954A patent/SU673166A3/ru active
- 1973-09-21 YU YU250673A patent/YU250673A/xx unknown
- 1973-10-01 DD DD17380573A patent/DD109217A5/xx unknown
- 1973-11-27 PH PH15265A patent/PH12123A/en unknown
-
1974
- 1974-08-24 HU HUSA002525 patent/HU168299B/hu unknown
-
1976
- 1976-02-16 SU SU762322343A patent/SU695521A3/ru active
Also Published As
| Publication number | Publication date |
|---|---|
| SU695521A3 (ru) | 1979-10-30 |
| DD109217A5 (enrdf_load_stackoverflow) | 1974-10-20 |
| PH12123A (en) | 1978-11-07 |
| RO62922A (fr) | 1978-05-15 |
| PL89408B1 (en) | 1976-11-30 |
| YU250673A (en) | 1982-05-31 |
| HU168299B (enrdf_load_stackoverflow) | 1976-03-28 |
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