SU652891A3 - Способ получени бензольного раствора надпропионовой кислоты - Google Patents
Способ получени бензольного раствора надпропионовой кислотыInfo
- Publication number
- SU652891A3 SU652891A3 SU762353640A SU2353640A SU652891A3 SU 652891 A3 SU652891 A3 SU 652891A3 SU 762353640 A SU762353640 A SU 762353640A SU 2353640 A SU2353640 A SU 2353640A SU 652891 A3 SU652891 A3 SU 652891A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- acid
- weight
- hydrogen peroxide
- obtaining
- perpropionic acid
- Prior art date
Links
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 title description 28
- 238000000034 method Methods 0.000 title description 12
- CZPZWMPYEINMCF-UHFFFAOYSA-N propaneperoxoic acid Chemical compound CCC(=O)OO CZPZWMPYEINMCF-UHFFFAOYSA-N 0.000 title 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 32
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 24
- 239000002253 acid Substances 0.000 description 16
- 235000019260 propionic acid Nutrition 0.000 description 12
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 8
- 238000004821 distillation Methods 0.000 description 7
- 239000000243 solution Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 229910052726 zirconium Inorganic materials 0.000 description 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- 229910052735 hafnium Inorganic materials 0.000 description 2
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- -1 19.7% by weight Chemical compound 0.000 description 1
- YEVQZPWSVWZAOB-UHFFFAOYSA-N 2-(bromomethyl)-1-iodo-4-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC=C(I)C(CBr)=C1 YEVQZPWSVWZAOB-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- YKYONYBAUNKHLG-UHFFFAOYSA-N n-Propyl acetate Natural products CCCOC(C)=O YKYONYBAUNKHLG-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229940090181 propyl acetate Drugs 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical group CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 description 1
- 239000006200 vaporizer Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/24—Peroxy compounds the —O—O— group being bound between a >C=O group and hydrogen, i.e. peroxy acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C07C407/003—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19752519288 DE2519288C2 (de) | 1975-04-30 | 1975-04-30 | Verfahren zur Herstellung von Percarbonsäurelösungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU652891A3 true SU652891A3 (ru) | 1979-03-15 |
Family
ID=5945440
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU762353640A SU652891A3 (ru) | 1975-04-30 | 1976-04-28 | Способ получени бензольного раствора надпропионовой кислоты |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5917110B2 (enExample) |
| BE (1) | BE841198A (enExample) |
| DE (1) | DE2519288C2 (enExample) |
| FR (1) | FR2309526A1 (enExample) |
| GB (1) | GB1550164A (enExample) |
| IE (1) | IE42801B1 (enExample) |
| NL (1) | NL7604540A (enExample) |
| SU (1) | SU652891A3 (enExample) |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE808108A (fr) * | 1972-12-22 | 1974-05-30 | Degussa | Procede pour la preparation de solutions d'acide percarboxylique dans des solvants organiques |
| DE2519287C3 (de) * | 1975-04-30 | 1979-04-19 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen Herstellung von wasserfreien oder weitgehend wasserfreien Percarbonsäurelösungen |
| DE2519301C2 (de) * | 1975-04-30 | 1984-12-13 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von Lösungen von Percarbonsäuren in organischen Lösungsmitteln |
-
1975
- 1975-04-30 DE DE19752519288 patent/DE2519288C2/de not_active Expired
-
1976
- 1976-04-28 FR FR7612603A patent/FR2309526A1/fr active Granted
- 1976-04-28 GB GB1718176A patent/GB1550164A/en not_active Expired
- 1976-04-28 SU SU762353640A patent/SU652891A3/ru active
- 1976-04-28 BE BE2054981A patent/BE841198A/xx unknown
- 1976-04-28 IE IE89376A patent/IE42801B1/en unknown
- 1976-04-28 NL NL7604540A patent/NL7604540A/xx active Search and Examination
- 1976-04-28 JP JP51047903A patent/JPS5917110B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| BE841198A (fr) | 1976-10-28 |
| NL7604540A (nl) | 1976-11-02 |
| FR2309526A1 (fr) | 1976-11-26 |
| DE2519288A1 (de) | 1976-11-11 |
| JPS51133223A (en) | 1976-11-18 |
| IE42801B1 (en) | 1980-10-22 |
| GB1550164A (en) | 1979-08-08 |
| FR2309526B1 (enExample) | 1980-08-22 |
| JPS5917110B2 (ja) | 1984-04-19 |
| DE2519288C2 (de) | 1982-09-16 |
| IE42801L (en) | 1976-10-30 |
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