SU435243A1 - - Google Patents
Info
- Publication number
- SU435243A1 SU435243A1 SU1852736A SU1852736A SU435243A1 SU 435243 A1 SU435243 A1 SU 435243A1 SU 1852736 A SU1852736 A SU 1852736A SU 1852736 A SU1852736 A SU 1852736A SU 435243 A1 SU435243 A1 SU 435243A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- mol
- solvent
- distilling
- tris
- dissolved
- Prior art date
Links
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 239000002904 solvent Substances 0.000 description 6
- 239000011541 reaction mixture Substances 0.000 description 5
- 239000007983 Tris buffer Substances 0.000 description 4
- PXAJQJMDEXJWFB-UHFFFAOYSA-N acetone oxime Chemical compound CC(C)=NO PXAJQJMDEXJWFB-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 229950011008 tetrachloroethylene Drugs 0.000 description 3
- 229910052725 zinc Inorganic materials 0.000 description 3
- 239000011701 zinc Substances 0.000 description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 239000005055 methyl trichlorosilane Substances 0.000 description 2
- UIUXUFNYAYAMOE-UHFFFAOYSA-N methylsilane Chemical compound [SiH3]C UIUXUFNYAYAMOE-UHFFFAOYSA-N 0.000 description 2
- JLUFWMXJHAVVNN-UHFFFAOYSA-N methyltrichlorosilane Chemical compound C[Si](Cl)(Cl)Cl JLUFWMXJHAVVNN-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 150000002923 oximes Chemical class 0.000 description 2
- -1 oxyl silyl ether Chemical compound 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000011135 tin Substances 0.000 description 2
- 229910052718 tin Inorganic materials 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- FYTPGBJPTDQJCG-UHFFFAOYSA-N Trichloro(chloromethyl)silane Chemical compound ClC[Si](Cl)(Cl)Cl FYTPGBJPTDQJCG-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- AZFVLHQDIIJLJG-UHFFFAOYSA-N chloromethylsilane Chemical compound [SiH3]CCl AZFVLHQDIIJLJG-UHFFFAOYSA-N 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 150000001367 organochlorosilanes Chemical class 0.000 description 1
- PARWUHTVGZSQPD-UHFFFAOYSA-N phenylsilane Chemical compound [SiH3]C1=CC=CC=C1 PARWUHTVGZSQPD-UHFFFAOYSA-N 0.000 description 1
- 239000005054 phenyltrichlorosilane Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000012262 resinous product Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- ORVMIVQULIKXCP-UHFFFAOYSA-N trichloro(phenyl)silane Chemical compound Cl[Si](Cl)(Cl)C1=CC=CC=C1 ORVMIVQULIKXCP-UHFFFAOYSA-N 0.000 description 1
- UKRDPEFKFJNXQM-UHFFFAOYSA-N vinylsilane Chemical compound [SiH3]C=C UKRDPEFKFJNXQM-UHFFFAOYSA-N 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1852736A SU435243A1 (enrdf_load_stackoverflow) | 1972-11-30 | 1972-11-30 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1852736A SU435243A1 (enrdf_load_stackoverflow) | 1972-11-30 | 1972-11-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU435243A1 true SU435243A1 (enrdf_load_stackoverflow) | 1974-07-05 |
Family
ID=20533828
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1852736A SU435243A1 (enrdf_load_stackoverflow) | 1972-11-30 | 1972-11-30 |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU435243A1 (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4400527A (en) | 1981-12-17 | 1983-08-23 | Allied Corporation | Producing oximinosilanes, oximinogermanes and oximinostannanes |
| DE3641756A1 (de) * | 1986-12-06 | 1988-08-11 | Huels Troisdorf | Verfahren zur herstellung von ketoximosilanen |
-
1972
- 1972-11-30 SU SU1852736A patent/SU435243A1/ru active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4400527A (en) | 1981-12-17 | 1983-08-23 | Allied Corporation | Producing oximinosilanes, oximinogermanes and oximinostannanes |
| DE3641756A1 (de) * | 1986-12-06 | 1988-08-11 | Huels Troisdorf | Verfahren zur herstellung von ketoximosilanen |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Rochow et al. | The Direct Synthesis of Phenylchlorosilanes | |
| EP3390410B1 (en) | Methods of making high purity trisilylamine | |
| US5387706A (en) | Process for preparing acyloxysilanes | |
| US2381000A (en) | Halogenated organosilicon compounds | |
| US4400527A (en) | Producing oximinosilanes, oximinogermanes and oximinostannanes | |
| SU435243A1 (enrdf_load_stackoverflow) | ||
| KR100219872B1 (ko) | 촉매혼합물로부터올리고머물질을분리하는방법 | |
| JPH0547552B2 (enrdf_load_stackoverflow) | ||
| JPH04235991A (ja) | シラシクロアルカンの調製方法 | |
| Kupchik et al. | Reaction of Triphenyltin Hydride with Some Organic Halides and Amines | |
| US4990642A (en) | Process for preparing oximosilanes | |
| US4026892A (en) | Process for the preparation of tetrachloropyrimidine | |
| JP2820554B2 (ja) | ジ−第３ブトキシジアセトキシシランの製造方法 | |
| US6777570B2 (en) | Process for producing norbornene derivative having organosilyl group | |
| US5403945A (en) | Cyclotrisiloxane and process for producing the same | |
| Breed et al. | Aryl and Alkylchlorodialkoxysilanes1 | |
| SU486511A3 (ru) | Способ получени моно- или дикремниевых соединений | |
| US3359186A (en) | Distillation of dimethylchlorosilane in presence of added hic | |
| US4855471A (en) | Process for the chlorodephenylation of phenyldisilanes | |
| JP2517783B2 (ja) | テキシルトリクロロシランの製造方法 | |
| US2735860A (en) | Dehydrochlorination of beta-chloro- | |
| SU374316A1 (ru) | Способ получения галоидсилилпроизводных бензотиофенов или хлорбеизотиофенов | |
| RU2299213C1 (ru) | Способ получения алкоксисиланов | |
| SU384807A1 (ru) | Способ получения арилметилированных ароматических углеводородов | |
| SU309521A1 (ru) | Способ получения алкилированных производных галогеисодержащих соединений кремния или олова |